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DILBERT. Copyright 1996, Scott Adams. Used with permission of UNIVERSAL UCLICK. All rights reserved
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DILBERT. Copyright 1996, Scott Adams. Used with permission of UNIVERSAL UCLICK. All rights reserved.
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2
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Researcher Dies After Lab Fire
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accessed May 15, 2014
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(a) Kemsley, J. Researcher Dies After Lab Fire. Chem. Eng. News [Online] 2009, http://cen.acs.org/articles/87/web/2009/01/Researcher-Dies-Lab-Fire.html (accessed May 15, 2014).
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(b) http://www.chemistry-blog.com/2009/01/20/tert-butyllithium-claims-fellow-chemist-at-ucla/ (accessed June 30, 2014).
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Chapter 1: Organoalkali Chemistry
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Baldwin, J. E., Williams, R. M., Eds.; Elsevier: Oxford
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(f) Clayden, J. In Organolithiums: Selectivity for Synthesis, Vol. 23; Baldwin, J. E., Williams, R. M., Eds.; Elsevier: Oxford, 2002.
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Rappoport, Z., Marek, I., Eds.; John Wiley & Sons: New York
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(g) The chemistry of organolithium compounds. In The Chemistry of Organolithium Compounds ; Rappoport, Z., Marek, I., Eds.; John Wiley & Sons: New York, 2004.
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Brochure available at no charge from Rockwood Lithium April
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Butyllithium. Brochure available at no charge from Rockwood Lithium, April 2012; http://www.rockwoodlithium.com/products/butyllithium/.
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(2012)
Butyllithium
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13
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84908010029
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Brochure available at no charge from FMC Corporation, May Permission was granted to use drawing in Figure 6, Laboratory apparatus for cannula transfer
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Butyllithium Safe Handling Guide. Brochure available at no charge from FMC Corporation, May 2005; http://www.fmclithium.com/. Permission was granted to use drawing in Figure 6, Laboratory apparatus for cannula transfer.
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Butyllithium Safe Handling Guide
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14
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84907982739
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One such video is available from Yale University Environmental Health and Safety Department at the following link accessed May 16, 2014
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(a) One such video is available from Yale University Environmental Health and Safety Department at the following link: http://ehs.yale.edu/training/organolithium-compounds-training (accessed May 16, 2014).
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15
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84907982738
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Dartmouth University also has a video available, which emphasizes the cannula transfer technique accessed May 16, 2014
-
(b) Dartmouth University also has a video available, which emphasizes the cannula transfer technique: http://www.youtube.com/watch?v=gi-ODNJCbqY (accessed May 16, 2014).
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17
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84907996681
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Contact manufacturers for product inquiries and large scale handling advice. See the Supporting Information.
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Contact manufacturers for product inquiries and large scale handling advice. See the Supporting Information.
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Various grades of hexanes and heptanes are used
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Various grades of hexanes and heptanes are used.
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84907997570
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Method for Producing Alkyl Lithium Compounds and Aryl Lithium Compounds by Monitoring the Reaction by Means of IR-Spectroscopy
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Although conducted under an inert atmosphere, experience in handling pyrophoric solids is required. This procedure was only used at the laboratory bench scale.21
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Although conducted under an inert atmosphere, experience in handling pyrophoric solids is required. This procedure was only used at the laboratory bench scale.21
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The use of 2 equiv of n-BuLi to prepare the MeLi-LiI complex was not explored, nor was the use of methyl bromide instead of methyl iodide investigated
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The use of 2 equiv of n-BuLi to prepare the MeLi-LiI complex was not explored, nor was the use of methyl bromide instead of methyl iodide investigated.
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One brand of flame-resistant fabric is Nomex. A variety of Nomex clothing styles, including lab coats, coveralls, shirts, and pants, is commercially available. Flame-resistant clothing is available from a number of laboratory supply vendors, including Fisher Scientific, Sigma-Aldrich, and VWR
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One brand of flame-resistant fabric is Nomex. A variety of Nomex clothing styles, including lab coats, coveralls, shirts, and pants, is commercially available. Flame-resistant clothing is available from a number of laboratory supply vendors, including Fisher Scientific, Sigma-Aldrich, and VWR.
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