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Chemical Health and Safety

Volumn 9, Issue 3, 2002, Pages 6-11

Safe handling of organolithium compounds in the laboratory

(3) Schwindeman, James A a,b Woltermann, Chris J a,b Letchford, Robert J a,b

a UNIVERSITY OF MIAMI (United States)

b NONE

Author keywords

[No Author keywords available]

Indexed keywords

ANION; ORGANOLITHIUM COMPOUND; REAGENT;

ACCIDENT PREVENTION; AIR; ARTICLE; CANNULA; CHEMICAL INDUSTRY; CONTAINER; CONTROLLED STUDY; EXPERIMENTATION; FLAMMABILITY; HUMAN; LABORATORY; LABORATORY PERSONNEL; MATERIALS HANDLING; MOISTURE; OCCUPATIONAL SAFETY; POLYMERIZATION; PROTECTIVE EQUIPMENT; STORAGE; SYNTHESIS; SYRINGE;

EID: 0036100252 PISSN: 10749098 EISSN: None Source Type: Journal
DOI: 10.1016/S1074-9098(02)00295-2 Document Type: Article

Times cited : (23)

References (23)

1
- 0003909903
- Pergamon: Oxford
- (1974) The Chemistry of Organolithium Compounds
- Wakefield, B.J.¹

2
- 0004174399
- Academic Press; London
- (1988) Organolithium Methods
- Wakefield, B.J.¹

3
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- Preparative Polar Organometallic Chemistry
- Springer-Verlag: Berlin
- (1987)
- Brandsma, L.¹ Verkruijsse, H.²

4
- 0003438023
- Springer-Verlag: Berlin
- (1990) Preparative Polar Organometallic Chemistry II
- Brandsma, L.¹

5
- 0004005191
- (For the application of organolithium reagents in organic synthesis) Wiley: New York, NY
- (1979) Carbanions in Organic Synthesis
- Stowell, J.C.¹

6
- 0004181038
- Marcel Dekker New York, NY (For an excellent overview of anionic polymerization)
- (1996) Anionic Polymerization
- Hsieh, H.L.¹ Quirk, R.P.²

7
- 0001630249
- (For example, the half-life of n-butyllithium in THF at 20°C is 1.78 hr. The half-lives of various alkyllithiums in ethereal solvents as a function of temperature)
- (1997) Org. Chem , vol.62 , pp. 1514
- Stanetty, P.¹ Mihovilovic M.D., J.²

8
- 0342322745
- 3rd ed.; Grayson, M., Ed.; Wiley: New York, NY
- (1981) Kirk-Othmer Encyclopedia of Chemical Technology , vol.16 , pp. 557-558
- Malpass, D.B.¹ Fannin, L.W.² Ligi, J.J.³

9
- 0003467672
- 5th ed.; Wiley: New York, NY
- (2001) Advanced Organic Chemistry , pp. 330
- March, J.¹

10
- 0006218943
- Pyrophoric is derived from the Greek word pyrophoros, which is a combination of pyr (fire) and pherein (to bear), in Webster's
- 3rd College ed.; Prentice Hall: New York, NY
- (1994) New World Dictionary of American English , pp. 1096

11
- 0006218614
- The official test for pyrophoricity is detailed in the Department of Transportation (DOT) regulations (49 CFR 173, Appendix E)

12
- 0004174399
- Academic Press: London
- (1988) Organolithium Methods , pp. 12
- Wakefield, B.J.¹

13
- 0006154050
- Schlosser M., Ed.; Wiley: Chichester
- (1994) Organometallics in Synthesis: A Manual , pp. 171-172
- Totter, F.¹ Rittmeyer, P.²

14
- 0006151509
- 4th ed.; Kroschwitz, J. I., Ed.; Wiley: New York, NY
- (1995) Kirk-Othmer Encyclopedia of Chemical Technology , vol.15 , pp. 453-454
- Kamienski, C.W.¹ McDonald, D.P.² Stark, M.W.³

15
- 0006182058
- (Winter) (for an excellent review of the various methods of analysis of organolithium compounds)
- (1994) Lithium Link
- Kamienski, C.W.¹

16
- 0006227122
- One brand of flame resistant fabric is Nomex®. A variety of clothing styles, including lab coats, coveralls, shirts and pants, is commercially available. Flame-resistant clothing is available from a number of vendors, including Aldrich, Fisher and VWR

17
- 0006198942
- One pair of Viton® gloves, size 9, is listed in the 2000-2001 Aldrich catalog for $57.60

18
- 0006155317
- One pair of nitrile gloves, size L, is listed in the 2000-2001 Aldrich catalog for $7.20

19
- 0006204560
- Ansul® Purple K is one popular choice for a Class B fire extinguisher

20
- 0006149438
- A number of bubbler designs are commercially available from laboratory glassware suppliers. A versatile bubbler design is Chemglass catalog number AF-0513-20

21
- 0006151510
- Butyllithium: Guidelines for Safe Handling a brochure available at no charge from FMC Lithium
- (For a more extensive discussion of these transfer techniques.)

22
- 0006148583
- Commercially available from FMC Lithium, 449 N. Cox Road, Gastonia, NC 28054

23
- 0006155318
- (Fall For an excellent review of t-butyllithium chemistry)
- (2000) Lithium Link
- Bailey, B.¹ Longstaff, S.²

* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.