In-house validation for the determination of honey adulteration with plant sugars (C4) by Isotope Ratio Mass Spectrometry (IR-MS)

LWT

Volumn 57, Issue 1, 2014, Pages 9-15

  Cengiz, Mehmet Fatih ^a   Durak, M Zeki ^b   Ozturk, Musa ^a  

^a AKDENIZ UNIVERSITY   (Turkey)

^b YILDIZ TECHNICAL UNIVERSITY   (Turkey)

Author keywords

Extraction; IR MS; Isotopic analysis; Method validation; Optimization

Indexed keywords

FOOD PRODUCTS; ISOTOPES; MASS SPECTROMETRY;

ANALYTICAL METHOD; HONEY ADULTERATION; HONEY SAMPLES; IN-HOUSE VALIDATIONS; ISOTOPE-RATIO MASS SPECTROMETRY; ISOTOPIC ANALYSIS; LIMIT OF DETECTION; LIMIT OF QUANTIFICATIONS; METHOD VALIDATIONS; OPTIMISATIONS;

RECOVERY;

EID: 84894269843     PISSN: 00236438     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.lwt.2013.12.032     Document Type: Article

References (35)

1. Anklam E. Areview of the analytical methods to determine the geographical and botanical origin of honey. Food Chemistry 1998, 63:549-562.
2. AOAC Official methods of analysis method 998.12: C-4 plant sugars in honey. Internal standard stable carbon isotope ratio method. AOAC International 1998, 44:27-30.
3. Bertelli D., Lolli M., Papotti G., Bortolotti L., Serra G., Plessi M. Detection of honey adulteration by sugar syrups using one-dimensional and two-dimensional high-resolution nuclear magnetic resonance. Journal of Agricultural and Food Chemistry 2010, 58:8495-8501.
4. Cabanero A.I., Recio J.L., Ruperez M. Liquid chromatography coupled to isotope ratio mass spectrometry: a new perspective on honey adulteration detection. Journal of Agricultural and Food Chemistry 2006, 54:9719-9727.
5. Cai J., Wu X., Yuan L., Han E., Zhou L., Zhou A. Determination of Chinese Angelica honey adulterated with rice syrup by an electrochemical sensor and chemometrics. Analytical Methods 2013, 5:2324-2328.
6. Carter J., Barwick V. Good practise guide for isotope ratio mass spectrometry 2011, FIRMS, UK. 1st ed.
7. Carter J.F., Fry B. Ensuring the reliability of stable isotope ratio data-beyond the principle of identical treatment. Analytical and Bioanalytical Chemistry 2013, 405:2799-2814.
8. Chen L., Xue X., Ye Z., Zhou J., Chen F., Zhao J. Determination of Chinese honey adulterated with high fructose corn syrup by near infrared spectroscopy. Food Chemistry 2011, 128:1110-1114.
9. Codex Standard Codex standard for honey. Rev. 2 2001, Codex Alimentarius Commission. http://www.codexalimentarius.net/standard_list.asp.
10. Cordella C., Militão J.S.L.T., Clément M.-C., Drajnudel P., Cabrol-Bass D. Detection and quantification of honey adulteration via direct incorporation of sugar syrups or bee-feeding: preliminary study using high-performance anion exchange chromatography with pulsed amperometric detection (HPAEC-PAD) and chemometrics. Analytica Chimica Acta 2005, 531:239-248.
11. Cotte J.F., Casabianca H., Lheritier J., Perrucchietti C., Sanglar C., Waton H., et al. Study and validity of 13C stable carbon isotopic ratio analysis by mass spectrometry and 2H site-specific natural isotopic fractionation by nuclear magnetic resonance isotopic measurements to characterize and control the authenticity of honey. Analitica Chimica Acta 2007, 582:125-136.
12. EURACHEM The fitness for purpose of analytical methods. A laboratory guide to method validation and related topics 1998, EURACHEM Guide.
13. Green J.M. Peer reviewed: a practical guide to analytical method validation. Analytical Chemistry 1996, 68:305A-309A.
14. ISO General requirements for the competence of testing and calibration laboratories 2005, International Standards Organization, ISO/IEC 17025.
15. Keck B.D., Ognibene T., Vogel J.S. Analytical validation of accelerator mass spectrometry for pharmaceutical development. Bioanalysis 2010, 2:469-485.
16. Kelly J.D., Petisco C., Downey G. Potential of near infrared transflectance spectroscopy to detect adulteration of Irish honey by beet invert syrup and high fructose corn syrup. Journal of Near Infrared Spectroscopy 2006, 14:139-146.
17. Kracht O., Hilkert A. Detection of honey adulteration with FlashEA elemental analyzer and DELTA V isotope ratio mass spectrometer 2009, Thermo Fisher Scientific Application, Application Note: 30177.
18. Li S., Shan Y., Zhu X., Zhang X., Ling G. Detection of honey adulteration by high fructose corn syrup and maltose syrup using Raman spectroscopy. Journal of Food Composition and Analysis 2012, 28:69-74.
19. Morales V., Corzo N., Sanz M.L. HPAEC-PAD oligosaccharide analysis to detect adulterations of honey with sugar syrups. Food Chemistry 2008, 107:922-928.
20. Ouchemoukh S., Schweitzer P., Bachir Bey M., Djoudad-Kadji H., Louaileche H. HPLC sugar profiles of Algerian honeys. Food Chemistry 2010, 121:561-568.
21. Padovan G.J., De Jong D., Rodrigues L.P., Marchini J.S. Detection of adulteration of commercial honey samples by the 13C/12C isotopic ratio. Food Chemistry 2003, 82:633-636.
22. Perna A., Intaglietta I., Simonetti A., Gambacorta E. Acomparative study on phenolic profile, vitamin C content and antioxidant activity of Italian honeys of different botanical origin. International Journal of Food Science & Technology 2013, 48:1899-1908.
23. Puscas A., Hosu A., Cimpoiu C. Application of a newly developed and validated high-performance thin-layer chromatographic method to control honey adulteration. Journal of Chromatography A 2013, 1272:132-135.
24. Ruiz-Matute A.I., Soria A.C., Martinez-Castro I., Sanz M.L. Anew methodology based on GC-MS to detect honey adulteration with commercial syrups. Journal of Agricultural and Food Chemistry 2007, 55:7264-7269.
25. Ruiz-Matute A.I., Weiss M., Sammataro D., Finely J., Sanz M.L. Carbohydrate composition of high-fructose corn syrups (HFCS) used for bee feeding: effect on honey composition. Journal of Agricultural and Food Chemistry 2010, 58:7317-7322.
26. Sanz M.L., Polemis N., Morales V., Corzo N., Drakoularakou A., Gibson G.R., et al. Invitro investigation into the potential prebiotic activity of honey oligosaccharides. Journal of Agricultural and Food Chemistry 2005, 53:2914-2921.
27. Sanz M.L., Sanz J., Martínez-Castro I. Gas chromatographic-mass spectrometric method for the qualitative and quantitative determination of disaccharides and trisaccharides in honey. Journal of Chromatography A 2004, 1059:143-148.
28. SAS The SAS system for windows. Release 7.00 TS Level 00P1 1998, SAS Institute, Inc, Cary, NC, USA.
29. Simsek A., Bilsel M., Goren A.C. 13C/12C pattern of honey from Turkey and determination of adulteration in commercially available honey samples using EA-IRMS. Food Chemistry 2012, 130:1115-1121.
30. Sivakesava S., Irudayaraj J. Classification of simple and complex sugar adulterants in honey by mid-infrared spectroscopy. International Journal of Food Science & Technology 2002, 37:351-360.
31. Tosun M. Detection of adulteration in honey samples added various sugar syrups with 13C/12C isotope ratio analysis method. Food Chemistry 2013, 138:1629-1632.
32. Turkis Food Codex Türk Gida Kodeksi-Bal Tebligi 2005, Tebliǧ No: 2005/49 (in Turkish). http://www.kkgm.gov.tr/TGK/Teblig/2005-49.html.
33. Wang X.H., Andrae L., Engeseth N.J. Antimutagenic effect of various honeys and sugars against Trp-p-1. Journal of Agricultural and Food Chemistry 2002, 50:6923-6928.
34. Weston R.J., Brocklebank L.K. The oligosaccharide composition of some New Zealand honeys. Food Chemistry 1999, 64:33-37.
35. White J.W., Winters K. Honey protein as internal standard for stable carbon isotope ratio detection of adulteration of honey. Journal of the Association of Official Analytical Chemists 1989, 72:907-911.