High yield of graphene by dispersant-free liquid exfoliation of mechanochemically delaminated graphite

Journal of Nanoparticle Research

Volumn 15, Issue 11, 2013, Pages

  Posudievsky, Oleg Yu ^a   Khazieieva, Oleksandra A ^a   Koshechko, Vyacheslav G ^a   Pokhodenko, Vitaly D ^a   Cherepanov, Vsevolod V ^b  

^a L V PISARZHEVSKII INSTITUTE OF PHYSICAL CHEMISTRY   (Ukraine)

^b INSTITUTE OF PHYSICS   (Ukraine)

Author keywords

Dispersant free solvent exfoliation; Ethanol; Graphene; Mechanochemical delamination of graphite; Nanofabrication; Nanolayer

Indexed keywords

DISINTEGRATION; DISPERSIONS; ETHANOL; EXFOLIATION (MATERIALS SCIENCE); GRAPHENE; GRAPHITE; NANOPARTICLES; NANOTECHNOLOGY; ULTRASONICS;

FEW-LAYER GRAPHENE; FREE SOLVENTS; FUNCTIONAL PERFORMANCE; LIQUID EXFOLIATIONS; MECHANOCHEMICAL TREATMENT; MECHANOCHEMICALS; NANO LAYERS; NANOSTRUCTURED GRAPHITE;

ORGANIC SOLVENTS;

GRAPHENE; GRAPHITE; NANOPARTICLE; ORGANIC SOLVENT; SODIUM CHLORIDE;

ARTICLE; CONCENTRATION (PARAMETERS); CONTROLLED STUDY; DISPERSION; PARTICLE SIZE; PRIORITY JOURNAL; SURFACE PROPERTY; SYNTHESIS; X RAY DIFFRACTION;

EID: 84892660672     PISSN: 13880764     EISSN: 1572896X     Source Type: Journal    
DOI: 10.1007/s11051-013-2046-y     Document Type: Article

References (43)

1. Allen MJ, Tung VC, Kaner RB (2010) Honeycomb carbon: a review of graphene. Chem Rev 110:132-145
2. Bonaccorso F, Sun Z, Hasan T, Ferrari AC (2010) Graphene photonics and optoelectronics. Nat Photon 4:611-622
3. Bonaccorso F, Lombardo A, Hasan T et al (2012) Production and processing of graphene and 2d crystals. Mater Today 15:564-589
4. Bourlinos AB, Georgakilas V, Zboril R et al (2009) Liquid-phase exfoliation of graphite towards solubilized graphenes. Small 5:1841-1845
5. Brownson DAC, Kampouris DK, Banks CE (2011) An overview of graphene in energy production and storage applications. J Power Sources 196:4873-4885
6. Cançado LG, Jorio A, Ferreira EHM et al (2011) Quantifying defects in graphene via Raman spectroscopy at different excitation energies. Nano Lett 11:3190-3196
7. Chang H, Wu H (2013) Graphene-Based Nanomaterials: synthesis, properties, and optical and optoelectronic applications. Adv Funct Mater 23:1984-1997
8. Choucair M, Thordarson P, Stride JA (2009) Gram-scale production of graphene based on solvothermal synthesis and sonication. Nat Nanotechnol 4:30-33
9. Coleman JN (2009) Liquid-phase exfoliation of nanotubes and graphene. Adv Funct Mater 19:3680-3695
10. Coleman JN (2013) Liquid exfoliation of defect-free graphene. Acc Chem Res 46:14-22
11. Eckmann A, Felten A, Mishchenko A et al (2012) Probing the nature of defects in graphene by Raman spectroscopy. Nano Lett 12:3925-3930
12. Edwards RS, Coleman KS (2013) Graphene synthesis: relationship to applications. Nanoscale 5:38-51
13. Gokus T, Nair RR, Bonetti A et al (2009) Making graphene luminescent by oxygen plasma treatment. ACS Nano 3:3963-3968
14. Gómez-Navarro C, Weitz RT, Bittner AM et al (2007) Electronic transport properties of individual chemically reduced graphene oxide sheets. Nano Lett 7:3499-3503
15. Hernandez Y, Nicolosi V, Lotya M et al (2008) High-yield production of graphene by liquid-phase exfoliation of graphite. Nat Nanotechnol 3:563-568
16. Horcas I, Fernández R, Gómez-Rodríguez JM et al (2007) WSXM: A software for scanning probe microscopy and a tool for nanotechnology. Rev Sci Instrum 78:13705-13712
17. Kamat PV (2011) Graphene-based nanoassemblies for energy conversion. J Phys Chem Lett 2:242-251
18. Khan U, O'Neill A, Lotya M et al (2010) High-concentration solvent exfoliation of graphene. Small 6:864-871
19. Knieke C, Berger A, Voigt M et al (2010) Scalable production of graphene sheets by mechanical delamination. Carbon 48:04-3196
20. León V, Quintana M, Herrero MA et al (2011) Few-layer graphenes from ball-milling of graphite with melamine. Chem Commun 47:10936-10938
21. Li B, Cao H (2011) ZnO@graphene composite with enhanced performance for the removal of dye from water. J Mater Chem 21:3346-3349
22. Lotya M, King PJ, Khan U et al (2010) High-concentration, surfactant-stabilized graphene dispersions. ACS Nano 4:3155-3162
23. Luo D, Zhang G, Liu J, Sun X (2011) Evaluation criteria for reduced graphene oxide. J Phys Chem C 115:11327-11335
24. Malard LM, Pimenta MA, Dresselhaus G, Dresselhaus MS (2009) Raman spectroscopy in graphene. Phys Rep 473: 51-87
25. Marcano DC, Kosynkin DV, Berlin JM et al (2010) Improved synthesis of graphene oxide. ACS Nano 4:4806-4814
26. Nguyen DD, Tai NH, Chueh YL et al (2011) Synthesis of ethanol-soluble few-layer graphene nanosheets for flexible and transparent conducting composite films. Nanotechnol 22:295606 8pp
27. Ni Z, Wang Y, Yu T, Shen Z (2008) Raman spectroscopy and imaging of graphene. Nano Res 1:273-291
28. Novoselov KS, Fal'ko VI, Colombo L et al (2012) A roadmap for graphene. Nature 490:192-200
29. Pang S, Hernandez Y, Feng X, Müllen K (2011) Graphene as transparent electrode material for organic electronics. Adv Mater 23:2779-2795
30. Park S, Ruoff RS (2009) Chemical methods for the production of graphenes. Nat Nanotechnol 4:217-224
31. Posudievsky OYu, Khazieieva OA, Koshechko VG, Pokhodenko VD (2012) Preparation of graphene oxide by solvent-free mechanochemical oxidation of graphite. J Mater Chem 22:12465-12467
32. Posudievsky OYu, Kozarenko OA, Khazieieva OA et al (2013) Ultrasound-free preparation of graphene oxide from mechanochemically oxidized graphite. J. Mater Chem A 1:6658-6663
33. Schwierz F (2010) Graphene transistors. Nat Nanotechnol 5: 487-496
34. Singh V, Joung D, Zhai L et al (2011) Graphene based materials: past, present and future. Prog Mater Sci 56:1178-1271
35. Subrahmanyam KS, Vivekchand SRC, Govindaraj A, Rao CNR (2008) A study of graphenes prepared by different methods: characterization, properties and solubilization. J Mater Chem 18:1517-1523
36. Tung VC, Allen MJ, Yang Y, Kaner RB (2009) High-throughput solution processing of large-scale graphene. Nat Nanotechnol 4:25-29
37. Yang H, Hernandez Y, Schlierf A et al (2013) A simple method for graphene production based on exfoliation of graphite in water using 1-pyrenesulfonic acid sodium salt. Carbon 53:357-365
38. Zhamu A, Jang BZ (2012) Mass production of pristine nano graphene materials. US Patent 8,226,801 B2
39. Zhang W, Cui J, Tao C-A et al (2009) A strategy for producing pure single-layer graphene sheets based on a confined selfassembly approach. Angew Chem Int Ed 48:1-6
40. Zhang X, Coleman AC, Katsonis N et al (2010) Dispersion of graphene in ethanol using a simple solvent exchange method. Chem Commun 46:7539-7541
41. Zhao W, Fang M, Wu F et al (2010) Preparation of graphene by exfoliation of graphite using wet ball milling. J Mater Chem 20:5817-5819
42. Zhu Y, Murali S, Cai W et al (2010) Graphene and graphene oxide: synthesis, properties, and applications. Adv Mater 22:3906-3924
43. Zhu Y, James DK, Tour JM (2012) New routes to graphene, graphene oxide and their related applications. Adv Mater 24:4924-4955