Analysing organochlorine pesticides in strawberry jams using GC-ECD, GC-MS/MS and QuEChERS sample preparation

Food Additives and Contaminants - Part A

Volumn 29, Issue 7, 2012, Pages 1074-1084

  Fernandes, V C ^a,b   Domingues, V F ^a   Mateus, N ^b   Delerue Matos, C ^a  

^a INSTITUTO SUPERIOR DE ENGENHARIA DO PORTO   (Portugal)

^b UNIVERSITY OF PORTO   (Portugal)

Author keywords

Chromatography GC; Cooked foods; Extraction; Fruit; GC MS; Organic foods; Pesticide residues; Pesticides organochlorine; Processed foods

Indexed keywords

EXTRACTION; FRUITS; GAS CHROMATOGRAPHY; MASS SPECTROMETRY; PESTICIDES; PROCESSED FOODS; ULTRASONIC APPLICATIONS;

CHROMATOGRAPHY - GC; COOKED FOOD; GC/MS; ORGANIC FOODS; ORGANOCHLORINES; PESTICIDE RESIDUE;

CHEMICAL CONTAMINATION;

ORGANOCHLORINE PESTICIDE; CHLORINATED HYDROCARBON; PESTICIDE;

ARTICLE; CHEMICAL ANALYSIS; CHROMATOGRAPHY; COOKED FOOD; GAS CHROMATOGRAPHY; ION TRAP MASS SPECTROMETRY; LIMIT OF DETECTION; MASS FRAGMENTOGRAPHY; ORGANIC FOOD; PRIORITY JOURNAL; RESIDUE ANALYSIS; STRAWBERRY; TANDEM MASS SPECTROMETRY; TIME OF FLIGHT MASS SPECTROMETRY; CHEMISTRY; FRAGARIA; MASS SPECTROMETRY; METHODOLOGY; REPRODUCIBILITY; STANDARD; VALIDATION STUDY;

FRAGARIA X ANANASSA;

CHROMATOGRAPHY, GAS; FRAGARIA; HYDROCARBONS, CHLORINATED; LIMIT OF DETECTION; MASS SPECTROMETRY; PESTICIDES; REFERENCE STANDARDS; REPRODUCIBILITY OF RESULTS;

EID: 84866759645     PISSN: 19440049     EISSN: 14645122     Source Type: Journal    
DOI: 10.1080/19440049.2012.682319     Document Type: Article

References (42)

1. Anastassiades M. 2008. QuEChERS: a mini-multiresidue method for the analysis of pesticide residues in low-fat products. Stuttgart (Germany). [cited 2012 Apr 24]. Available from: http://quechers.cvua-stuttgart.de/pdf/reality.pdf
2. Anastassiades M, Lehotay SJ, Stajnbaher D, Schenck FJ. 2003. Fast and easy multiresidue method employing acetonitrile extraction/partitioning and 'dispersive solid-phase extraction' for the determination of pesticide residues in produce. J AOAC Int. 86:412-431.
3. Barriada-Pereira M, Concha-Grana E, Gonzalez-Castro MJ, Muniategui-Lorenzo S, Lopez-Mahia P, Prada-Rodriguez D, Fernandez-Fernandez E. 2003. Microwave-assisted extraction versus Soxhlet extraction in the analysis of 21 organochlorine pesticides in plants. J Chromatogr A. 1008:115-122.
4. Barriada-Pereira M, Gonzalez-Castro MJ, Muniategui-Lorenzo S, Lopez-Mahia P, Prada-Rodriguez D, Fernandez-Fernandez E. 2005. Determination of organo-chlorine pesticides in horticultural samples by microwave assisted extraction followed by GC-ECD. Int J Environ Anal Chem. 85:325-333.
5. Barriada-Pereira M, Gonzalez-Castro MJ, Muniategui-Lorenzo S, Lopez-Mahia P, Prada-Rodriguez D, Fernandez-Fernandez E. 2007. Comparison of pressurized liquid extraction and microwave assisted extraction for the determination of organochlorine pesticides in vegetables. Talanta. 71:1345-1351.
6. Beltran J, Peruga A, Pitarch E, Lopez FJ, Hernandez F. 2003. Application of solid-phase microextraction for the determination of pyrethroid residues in vegetable samples by GC-MS. Anal Bioanal Chem. 376:502-511.
7. Berrada H, Fernandez M, Ruiz MJ, Molto JC, Manes J, Font G. 2010. Surveillance of pesticide residues in fruits from Valencia during twenty months (2004/05). Food Control. 21:36-44.
8. Bolanos PP, Moreno JLF, Shtereva DD, Frenich AG, Vidal JLM. 2007. Development and validation of a multiresidue method for the analysis of 151 pesticide residues in strawberry by gas chromatography coupled to a triple quadrupole mass analyzer. Rapid Commun Mass Spectrom. 21:2282-2294.
9. Colume A, Cardenas S, Gallego M, Valcarcel M. 2001. Multiresidue screening of pesticides in fruits using an automatic solid-phase extraction system. J Agric Food Chem. 49:1109-1116.
10. Correia M, Delerue-Matos C, Alves A. 2000. Multi-residue methodology for pesticide screening in wines. J Chromatogr A. 889:59-67.
11. Cortes-Aguado S, Sanchez-Morito N, Arrebola FJ, Frenich AG, Vidal JLM. 2008. Fast screening of pesticide residues in fruit juice by solid-phase microextraction and gas chromatography-mass spectrometry. Food Chem. 107:1314-1325.
12. Da Silva RL, Da Silva CP, Navickiene S. 2010. Multiresidue determination of carbamate, organochlorine, organophosphorus, and dicarboximide pesticides in lettuce by GC/MS. J Environ Sci Hlth B. 45:589-594.
13. Dasgupta S, Banerjee K, Patil SH, Ghaste M, Dhumal KN, Adsule PG. 2010. Optimization of two-dimensional gas chromatography time-of-flight mass spectrometry for separation and estimation of the residues of 160 pesticides and 25 persistent organic pollutants in grape and wine. J Chromatogr A. 1217:3881-3889.
14. Di Muccio A, Fidente P, Barbini DA, Dommarco R, Seccia S, Morrica P. 2006. Application of solid-phase extraction and liquid chromatography-mass spectrometry to the determination of neonicotinoid pesticide residues in fruit and vegetables. J Chromatogr A. 1108:1-6.
15. Dubois N, Elbaz A, Charlier C. 2010. Quantitative determination of eight organochlorine pesticides in serum by GC coupled to tandem mass spectrometry. Acta Clin Belgica. 65:58-64.
16. European Union. EU database [Internet]. [cited 2012 Apr 24]. Available from: http://ec.europa.eu/sanco_pesticides/public/index.cfm?event=substance.selection/
17. Feo ML, Eljarrat E, Barcelo D. 2010. Determination of pyrethroid insecticides in environmental samples. Trends Analyt Chem. 29:692-705.
18. Fernandes VC, Domingues VF, Mateus N, Delerue-Matos C. 2011. Determination of pesticides in fruit and fruit juices by chromatographic methods. An overview. J Chromatogr Sci. 49:715-730.
19. Fernandes VC, Domingues VF, Mateus N, Delerue-Matos C. 2011. Organochlorine pesticide residues in strawberries from integrated pest management and organic farming. J Agric Food Chem. 59:7582-7591.
20. Fernandes VC, Pestana D, Monteiro R, Faria G, Meireles M, Correia-Sa L, Teixeira D, Faria A, Calhau C, Domingues VF, et al. 2012. Optimization and validation of organochlorine compounds in adipose tissue by SPE-gas chromatography. Biomed Chromatogr. DOI: 10.1002/bmc.2723 (in press).
21. Fontcuberta M, Arques JF, Villalbi JR, Martinez M, Centrich F, Serrahima E, Pineda L, Duran J, Casas C. 2008. Chlorinated organic pesticides in marketed food: Barcelona, 2001-06. Sci Total Environ. 389:52-57.
22. Fugel R, Carle R, Schieber A. 2005. Quality and authenticity control of fruit purees, fruit preparations and jams - a review. Trends Food Sci Technol. 16:433-441.
23. Holland PT, Hamilton D, Ohlin B, Skidmore MW. 1994. IUPAC Reports on Pesticides 31. Effects of storage and processing on pesticide residues in plant-products. Pure Appl Chem. 66:335-356.
24. ICH (European Agency for the Evaluation of Medicinal Products, Human Medicines Evaluation Unit). 1996. Validation of analytical procedures: methodology. ICH Topic Q 2B. [Internet]. [cited 2012 Apr 24]. http://www.uam.es/personal_pas/txrf/MU5.pdf
25. Kaushik G, Satya S, Naik SN. 2009. Food processing a tool to pesticide residue dissipation - a review. Food Res Int. 42:26-40.
26. Keikotlhaile BM, Spanoghe P, Steurbaut W. 2010. Effects of food processing on pesticide residues in fruits and vegetables: a meta-analysis approach. Food Chem Toxicol. 48:1-6.
27. Koesukwiwat U, Lehotay SJ, Miao S, Leepipatpiboon N. 2010. High throughput analysis of 150 pesticides in fruits and vegetables using QuEChERS and low-pressure gas chromatography-time-of-flight mass spectrometry. J Chromatogr A. 1217:6692-6703.
28. Lambropoulou DA, Albanis TA. 2003. Headspace solid-phase microextraction in combination with gas chromatography-mass spectrometry for the rapid screening of organophosphorus insecticide residues in strawberries and cherries. J Chromatogr A. 993:197-203.
29. Lehotay SJ, Gates RA. 2009. Blind analysis of fortified pesticide residues in carrot extracts using GC-MS to evaluate qualitative and quantitative performance. J Sep Sci. 32:3706-3719.
30. Lehotay SJ, Son KA, Kwon H, Koesukwiwat U, Fu WS, Mastovska K, Hoh E, Leepipatpiboon N. 2010. Comparison of QuEChERS sample preparation methods for the analysis of pesticide residues in fruits and vegetables. J Chromatogr A. 1217:2548-2560.
31. Mansilha C, Melo A, Rebelo H, Ferreira IMPLVO, Pinho O, Domingues V, Pinho C, Gameiro P. 2010. Quantification of endocrine disruptors and pesticides in water by gas chromatography-tandem mass spectrometry. Method validation using weighted linear regression schemes. J Chromatogr A. 1217:6681-6691.
32. Medina CM, Pitarch E, Portoles T, Lopez FJ, Hernandez F. 2009. GC-MS/MS multi-residue method for the determi nation of organochlorine pesticides, polychlorinated biphenyls and polybrominated diphenyl ethers in human breast tissues. J Sep Sci. 32:2090-2102.
33. Navickiene S, Polese L, Minelli EV, Ribeiro ML. 1999. A simplified method for the determination of fenpropathrin residues in fruits. Chromatographia. 49:212-214.
34. Perez-Serradilla JA, Mata-Granados JM, De Castro MDL. 2010. Low-level determination of organochlorine pesti cides in wines by automatic preconcentration and GC-MS- MS detection. Chromatographia. 71:899-905.
35. Rashid A, Nawaz S, Barker H, Ahmad I, Ashraf M. 2010. Development of a simple extraction and clean-up procedure for determination of organochlorine pesticides in soil using gas chromatography-tandem mass spectrometry. J Chromatogr A. 1217:2933-2939.
36. SANCO. 2009. SANCO/10684/2009. Method validation and quality control procedures for pesticides residues analysis in food and feed. European Commission [Internet]. [cited 2012 Apr 24]. Available from: http://www.crl-pesticides.eu/library/docs/allcrl/AqcGuidance_Sanco_2009_10684.pdf
37. Sannino A. 1995. Investigation into contamination of processed fruit products by carbendazim, methyl thiophanate and thiabendazole. Food Chem. 52:57-61.
38. Sannino A, Bolzoni L, Bandini M. 2004. Application of liquid chromatography with electrospray tandem mass spectrometry to the determination of a new generation of pesticides in processed fruits and vegetables. J Chromatogr A. 1036:161-169.
39. Sanusi A, Guillet V, Montury M. 2004. Advanced method using microwaves and solid-phase microextraction coupled with gas chromatography-mass spectrometry for the determination of pyrethroid residues in strawberries. J Chromatogr A. 1046:35-40.
40. Tao CJ, Hu JY, Li JZ, Zheng SS, Liu W, Li CJ. 2009. Multi-residue determination of pesticides in vegetables by gas chromatography/ion trap mass spectrometry. Bull Environ Contam Toxicol. 82:111-115.
41. Wennrich L, Popp B, Breuste J. 2001. Determination of organochlorine pesticides and chlorobenzenes in fruit and vegetables using subcritical water extraction combined with sorptive enrichment and CGC-MS. Chromatographia. 53:S380-S386.
42. Wong JW, Zhang K, Tech K, Hayward DG, Krynitsky AJ, Cassias I, Schenck FJ, Banerjee K, Dasgupta S, Brown D. 2010. Multiresidue pesticide analysis of ginseng powders using acetonitrile-or acetone-based extraction, solid-phase extraction cleanup, and gas chromatography-mass spectrometry/ selective ion monitoring (GC-MS/SIM) or -tandem mass spectrometry (GC-MS/MS). J Agric Food Chem. 58:5884-5896.