Development and validation of an accurate and rapid LC-ESI-MS/MS method for the simultaneous quantification of aflatoxin B 1, B 2, G 1 and G 2 in lotus seeds

Food Control

Volumn 29, Issue 1, 2013, Pages 156-161

  Liu, Shuyu ^a   Qiu, Feng ^a   Kong, Weijun ^a   Wei, Jianhe ^a   Xiao, Xiaohe ^b   Yang, Meihua ^a  

^a BEIJING UNIVERSITY OF POSTS AND TELECOMMUNICATIONS   (China)

^b BEIJING 302 HOSPITAL   (China)

Author keywords

Aflatoxins; Determination; LC ESI MS MS; Lotus seeds; Method validation

Indexed keywords

EID: 84862993624     PISSN: 09567135     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.foodcont.2012.05.069     Document Type: Article

References (28)

1. 2 in spices using a multifunctional column clean-up. Journal of Chromatography A 2001, 932:153-157.
2. 1 levels in deep-red ground pepper (isot) using immunoaffinity column combined with ELISA. Food and Chemical Toxicology 2008, 46:1596-1599.
3. Bacaloni A., Cavaliere C., Cucci F., Foglia P., Samperi R., Laganà A. Determination of aflatoxins in hazelnuts by various sample preparation methods and liquid chromatography-tandem mass spectrometry. Journal of Chromatography A 2008, 1179:182-189.
4. Bradburn N., Jewers K., Jones B.D., Tomlins I.I. Rapid method for the clean-up of extracts of cottonseed prior to aflatoxin determination by bi-directional HPTLC. Chromatographia 1989, 28:541-544.
5. Cavaliere C., Foglia P., Guarino C., Nazzari M., Samperi R., Laganà A. Determination of aflatoxins in olive oil by liquid chromatography-tandem mass spectrometry. Analytical Chimica Acta 2007, 596:141-148.
6. Diana Di Mavungu J., Monbaliu S., Scippo M.L., Maghuin-Rogister G., Schneider Y.J., Larondelle Y., et al. LC-MS/MS multi-analyte method for mycotoxin determination in food supplements. Food Additives and Contaminants. Part A 2009, 26:885-895.
7. 1 in sidestream cigarette smoke by immunoaffinity column extraction coupled with liquid chromatography/mass spectrometry. Journal of Chromatography A 2005, 1083:127-132.
8. Fedorowski J., LaCourse W.R. A review of post-column photochemical reaction systems coupled to electrochemical detection in HPLC. Analytical Chimica Acta 2010, 657:1-8.
9. Ferrer A.C., Unterluggauer H., Fischer R.J., Fernández-Alba A.R., Masselter S. Development and validation of a LC-MS/MS method for the simultaneous determination of aflatoxins, dyes and pesticides in spices. Analytical and Bioanalytical Chemistry 2010, 397:93-107.
10. Garon D., Richard E., Sage L., Bouchart V., Pottier D., Lebailly P. Mycoflora and multimycotoxin detection in corn silage: experimental study. Journal of Agricultural and Food Chemistry 2006, 54:3479-3484.
11. Guo H.B. Cultivation of lotus (Nelumbo nucifera Gaertn. ssp. nucifera) and its utilization in China. Genetic Resources and Crop Evolution 2009, 3:323-330.
12. 2 in traditional Chinese medicines. Analytical Chimica Acta 2010, 664:165-171.
13. Lattanzio V.M.T., Solfrizzo M., Powers S., Visconti A. Simultaneous determination of aflatoxins, ochratoxin A and Fusarium toxins in maize by liquid chromatography/tandem mass spectrometry after multitoxin immunoaffinity cleanup. Rapid Communications in Mass Spectrometry 2007, 21:3253-3261.
14. Logrieco A., Bottalico A., Mulé G., Moretti A., Perrone G. Epidemiology of toxigenic fungi and their associated mycotoxins for some Mediterranean crops. European Journal of Plant Pathology 2003, 109:645-667.
15. Mani S.S., Subramanian I.P., Pillai S.S., Muthusamy K. Evaluation of hypoglycemic activity of inorganic constituents in Nelumbo nucifera seeds on streptozotocin-induced diabetes in rats. Biological Trace Element Research 2010, 138:226-237.
16. Quinto M., Spadaccino G., Palermo C., Centonze D. Determination of aflatoxins in cereal flours by solid-phase microextraction coupled with liquid chromatography and post-column photochemical derivatization-fluorescence detection. Journal of Chromatography A 2009, 1216:8636-8641.
17. Rai S.,A., Mukherjee W.K., Saha B.P., Mukherjee P.K. Antioxidant activity of Nelumbo nucifera (sacred lotus) seeds. Journal of Ethnopharmacology 2006, 3:322-327.
18. 1 in rice in India. Food Microbiology 2009, 26:27-31.
19. Sridhar K.R., Bhat R. Lotus-A potential nutraceutical source. Journal of Agricultural Technology 2007, 3:143-155.
20. 1 in different food and feed matrices. Food Additives and Contaminats 1999, 16:331-338.
21. Stroka J., Van Otterdijk R., Anklam E. Immunoaffinity column clean-up prior to thin-layer chromatography for the determination of aflatoxins in various food matrices. Journal of Chromatography A 2000, 904:251-256.
22. Sulyok M., Krska R., Schuhmacher R. Application of a liquid chromatography-tandem mass spectrometric method to multi-mycotoxin determination in raw cereals and evaluation of matrix effects. Food Additives and Contaminants. Part A 2007, 24:1184-1195.
23. Tanaka H., Takino M., Sugita-Konishi Y., Tanaka T. Development of a liquid chromatography/time-of-flight mass spectrometric method for the simultaneous determination of trichothecenes, zearalenone and aflatoxins in foodstuffs. Rapid Communications in Mass Spectrometry 2006, 20:1422-1428.
24. Trucksess M.W., Weaver C.,M., Oles C.J., Rump L.V., White K.D., Betz J.M., et al. Use of multitoxin immunoaffinity columns for determination of aflatoxins and ochratoxin A in ginseng and ginger. Journal of AOAC International 2007, 90:1042-1049.
25. Vahl M., Jørgensen K. Determination of aflatoxins in food using LC/MS/MS. Zeitschrift für Lebensmittel-untersuchung und -Forschung A 1998, 206:243-245.
26. 2 in medicinal herbs by liquid chromatography-tandem mass spectrometry. Journal of Chromatography A 2004, 1048:25-29.
27. 2 in Brizail nuts. International Journal of Environmental Analytical Chemistry 2008, 88:425-433.
28. Yang M.H., Chen J.M., Zhang X.H. Immunoaffinity column clean-up and liquid chromatography with post-column derivatization for analysis of aflatoxins in traditional Chinese medicine. Chromatographia 2005, 62:499-504.