Dispersive cleanup of acetonitrile extracts of tea samples by mixed multiwalled carbon nanotubes, primary secondary amine, and graphitized carbon black sorbents

Journal of Agricultural and Food Chemistry

Volumn 60, Issue 16, 2012, Pages 4026-4033

  Zhao, Pengyue ^a   Wang, Lei ^a   Jiang, Yaping ^a   Zhang, Fengzu ^a   Pan, Canping ^a  

^a CHINA AGRICULTURAL UNIVERSITY   (China)

Author keywords

multiwalled carbon nanotubes; pesticide multiresidue analysis; reversed dispersive solid phase extraction; tea

Indexed keywords

ACETONITRILE SOLUTIONS; ANALYTES; CONCENTRATION LEVELS; EXTRACTION SOLVENTS; GRAPHITIZED CARBON BLACK; GREEN TEA; LIMITS OF QUANTIFICATION; MAGNESIUM SULFATE; MULTI-RESIDUE ANALYSIS; OOLONG TEA; ORGANIC PHASE; PESTICIDE RESIDUE; PUER TEA; RELATIVE STANDARD DEVIATIONS; SAMPLE PREPARATION; SECONDARY AMINES; SOLID-PHASE EXTRACTION; TANDEM MASS SPECTROMETRY; TEA; TEA SAMPLES;

ACETONITRILE; CARBON BLACK; GRAPHITIZATION; LIQUID CHROMATOGRAPHY; MAGNESIUM; MASS SPECTROMETRY; MULTIWALLED CARBON NANOTUBES (MWCN); ORGANIC SOLVENTS; PESTICIDES; PHASE SEPARATION; SODIUM CHLORIDE;

SOLVENT EXTRACTION;

ACETONITRILE; ACETONITRILE DERIVATIVE; AMINE; CARBON NANOTUBE; PESTICIDE RESIDUE;

ADSORPTION; ARTICLE; CHEMISTRY; EVALUATION; FOOD CONTAMINATION; INSTRUMENTATION; ISOLATION AND PURIFICATION; MASS FRAGMENTOGRAPHY; METHODOLOGY; SOLID PHASE EXTRACTION; SOOT; TEA;

ACETONITRILES; ADSORPTION; AMINES; CAMELLIA SINENSIS; FOOD CONTAMINATION; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; NANOTUBES, CARBON; PESTICIDE RESIDUES; SOLID PHASE EXTRACTION; SOOT; TEA;

EID: 84860351031     PISSN: 00218561     EISSN: 15205118     Source Type: Journal    
DOI: 10.1021/jf205351t     Document Type: Article

References (38)

1. Dufresne, C. J.; Farnworth, E. R. A review of latest research findings on the health promotion properties of tea J. Nutr. Biochem. 2001, 12, 404-421 (Pubitemid 32633828)
2. Dufresne, C.; Farnworth, E. Tea, kombucha, and health: a review Food Res. Int. 2000, 33, 409-421 (Pubitemid 30427822)
3. Chen, G.; Cao, P.; Liu, R. A multi-residue method for fast determination of pesticides in tea by ultra performance liquid chromatography-electrospray tandem mass spectrometry combined with modified QuEChERS sample preparation procedure Food Chem. 2011, 125, 1406-1411
4. Lu, C.; Liu, X.; Dong, F.; Xu, J.; Song, W.; Zhang, C.; Li, Y.; Zheng, Y. Simultaneous determination of pyrethrins residues in teas by ultra-performance liquid chromatography/tandem mass spectrometry Anal. Chim. Acta 2010, 678, 56-62
5. Commission Directive 2000/42/EC of 22 June 2000 amending the Annexes to Council Directives 86/362/EEC.86/363/EEC and 90/642/EEC on the fixing of maximum levels for pesticide residues in and on cereals, foodstuffs of animal origin and certain products of plant origin, including fruit and vegetables respectively (text with EEA relevance). Off. J. Eur. Communites: Legis. 2000, 158, 51-75.
6. Huang, Z.; Li, Y.; Chen, B.; Yao, S. Simultaneous determination of 102 pesticide residues in Chinese teas by gas chromatography-mass spectrometry J. Chromatogr., B 2007, 853, 154-162 (Pubitemid 46891348)
7. Ji, J.; Deng, C.; Zhang, H.; Wu, Y.; Zhang, X. Microwave-assisted steam distillation for the determination of organochlorine pesticides and pyrethroids in Chinese teas Talanta 2007, 71, 1068-1074 (Pubitemid 46161617)
8. Liu, S.; Zheng, Z.; Wei, F.; Ren, Y.; Gui, W.; Wu, H.; Zhu, G. Simultaneous determination of seven neonicotinoid pesticide residues in food by ultraperformance liquid chromatography tandem mass spectrometry J. Agric. Food Chem. 2010, 58, 3271-3278
9. Hu, B.; Song, W.; Xie, L.; Shao, T. Determination of 33 pesticides in tea using accelerated solvent extraction/gel permeation chromatography and solid phase extraction/gas chromatography-mass spectrometry Chin. J. Chromatogr. 2008, 26, 22-28
10. Schurek, J.; Portoles, T.; Hajslova, J.; Riddellova, K.; Hernandez, F. Application of head-space solid-phase microextraction coupled to comprehensive two-dimensional gas chromatography-time-of-flight mass spectrometry for the determination of multiple pesticide residues in tea samples Anal. Chim. Acta 2008, 611, 163-172
11. Wu, F.; Lu, W.; Chen, J.; Liu, W.; Zhang, L. Single-walled carbon nanotubes coated fibers for solid-phase microextraction and gas chromatography-mass spectrometric determination of pesticides in tea samples Talanta 2010, 82, 1038-1043
12. Hou, Y.; Cao, Q.; Xie, X.; Wang, B.; Xu, J.; Yang, L.; Yang, Y.; Yang, Y. Determination of pyrethroid pesticide residues in tobacco leaves and tea using stir bar sorptive extraction-thermal desorption and gas chromatography-mass spectrometry Chin. J. Chromatogr. 2007, 25, 25-29
13. Bicchi, C.; Cordero, C.; Iori, C.; Rubiolo, P.; Sandra, P.; Yariwake, J. H.; Zuin, V. G. SBSE-GC-ECD/FPD in the analysis of pesticide residues in Passiflora alata dryander herbal teas J. Agric. Food Chem. 2003, 51, 27-33
14. Moinfar, S.; Hosseini, M.-R. M. Development of dispersive liquid-liquid microextraction method for the analysis of organophosphorus pesticides in tea J. Hazard. Mater. 2009, 169, 907-911
15. Anastassiades, M.; Maštovská, K.; Lehotay, S. J. Evaluation of analyte protectants to improve gas chromatographic analysis of pesticides J. Chromatogr., A 2003, 1015, 163-184 (Pubitemid 37163515)
16. Anastassiades, M.; Lehotay, S. J.; Stajnbaher, D.; Schenck, F. J. Fast and easy multiresidue method employing acetonitrile extraction/partitioning and "dispersive solid-phase extraction" for the determination of pesticide residues in produce J. AOAC Int. 2003, 86, 412-431
17. Lehotay, S. J.; Son, K. A.; Kwon, H.; Koesukwiwat, U.; Fu, W.; Mastovska, K.; Hoh, E.; Leepipatpiboon, N. Comparison of QuEChERS sample preparation methods for the analysis of pesticide residues in fruits and vegetables J. Chromatogr., A 2010, 1217, 2548-2560
18. Wilkowska, A.; Biziuk, M. Determination of pesticide residues in food matrices using the QuEChERS methodology Food Chem. 2011, 125, 803-812
19. Iijiama, S. Helical microtubules of graphitic carbon Nature 1991, 354, 56-58
20. Wang, S.; Zhao, P.; Min, G.; Fang, G. Multi-residue determination of pesticides in water using multi-walled carbon nanotubes solid-phase extraction and gas chromatography-mass spectrometry J. Chromatogr., A 2007, 1165, 166-171 (Pubitemid 47313426)
21. Zhou, Q.; Wang, W.; Xiao, J. Preconcentration and determination of nicosulfuron, thifensulfuron-methyl and metsulfuron-methyl in water samples using carbon nanotubes packed cartridge in combination with high performance liquid chromatography Anal. Chim. Acta 2006, 559, 200-206 (Pubitemid 43220439)
22. Zhou, Q.; Xiao, J.; Wang, W.; Liu, G.; Shi, Q.; Wang, J. Determination of atrazine and simazine in environmental water samples using multiwalled carbon nanotubes as the adsorbents for preconcentration prior to high performance liquid chromatography with diode array detector Talanta 2006, 68, 1309-1315 (Pubitemid 43088706)
23. El-Sheikh, A. H.; Sweileh, J. A.; Al-Degs, Y. S.; Insisi, A. A.; Al-Rabady, N. Critical evaluation and comparison of enrichment efficiency of multi-walled carbon nanotubes, C18 silica and activated carbon towards some pesticides from environmental waters Talanta 2008, 74, 1675-1680
24. El-Sheikh, A. H.; Insisi, A. A.; Sweileh, J. A. Effect of oxidation and dimensions of multi-walled carbon nanotubes on solid phase extraction and enrichment of some pesticides from environmental waters prior to their simultaneous determination by high performance liquid chromatography J. Chromatogr., A 2007, 1164, 25-32 (Pubitemid 47284108)
25. Cai, Y.; Cai, Y.; Mou, S.; Lu, Y. Multi-walled carbon nanotubes as a solid-phase extraction adsorbent for the determination of chlorophenols in environmental water samples J. Chromatogr., A 2005, 1081, 245-247 (Pubitemid 40848409)
26. Du, D.; Wang, M.; Zhang, J.; Cai, J.; Tu, H.; Zhang, A. Application of multiwalled carbon nanotubes for solid-phase extraction of organophosphate pesticide Electrochem. Commun. 2008, 10, 85-89 (Pubitemid 50008399)
27. Ravelo-Pérez, L. M.; Hernández-Borges, J.; Rodríguez-Delgado, M. Multi-walled carbon nanotubes as efficient solid-phase extraction materials of organophosphorus pesticides from apple, grape, orange and pineapple fruit juices J. Chromatogr., A 2008, 1211, 33-42
28. Wang, L.; Zhao, H.; Qiu, Y.; Zhou, Z. Determination of four benzodiazepine residues in pork using multiwalled carbon nanotube solid-phase extraction and gas chromatography-mass spectrometry J. Chromatogr., A 2006, 1136, 99-105 (Pubitemid 44767886)
29. Su, R.; Wang, X.; Xu, X.; Wang, Z.; Li, D.; Zhao, X.; Li, X.; Zhang, H.; Yu, A. Application of multiwall carbon nanotubes-based matrix solid phase dispersion extraction for determination of hormones in butter by gas chromatography mass spectrometry J. Chromatogr., A 2010, 1218, 5047-5054
30. Fang, G.; Min, G.; He, J.; Zhang, C.; Qian, K.; Wang, S. Multiwalled carbon nanotubes as matrix solid-phase dispersion extraction absorbents to determine 31 pesticides in agriculture samples by gas chromatography-mass spectrometry J. Agric. Food Chem. 2009, 57, 3040-3045
31. Asensio-Ramos, M.; D'Orazio, G.; Hernandez-Borges, J.; Rocco, A.; Fanali, S. Multi-walled carbon nanotubes-dispersive solid-phase extraction combined with nano-liquid chromatography for the analysis of pesticides in water samples Anal. Bioanal. Chem. 2011, 400, 1113-1123
32. European Council 2002/657/EC Implementing Council Directive 96/23/EC Concerning the Performance of Analytical Methods and the Interpretation of Results; European Council: Brussels, Belgium, 2002.
33. Kolberg, D. I.; Prestes, O. D.; Adaime, M. B.; Zanella, R. Development of a fast multiresidue method for the determination of pesticides in dry samples (wheat grains, flour and bran) using QuEChERS based method and GC-MS Food Chem. 2011, 125, 1436-1442
34. Pareja, L.; Cesio, V.; Heinzen, H.; Fernández-Alba, A. R. Evaluation of various QuEChERS based methods for the analysis of herbicides and other commonly used pesticides in polished rice by LC-MS/MS. Talanta 83 (5), 1613-1622.
35. González-Curbelo, M. A.; Hernández-Borges, J.; Ravelo-Pérez, L. M.; Rodríguez-Delgado, M. á. Insecticides extraction from banana leaves using a modified QuEChERS method Food Chem. 2011, 125, 1083-1090
36. Xu, R.; Wu, J.; Liu, Y.; Zhao, R.; Chen, B.; Yang, M.; Chen, J. Analysis of pesticide residues using the quick easy cheap effective rugged and safe (QuEChERS) pesticide multiresidue method in traditional Chinese medicine by gas chromatography with electron capture detection Chemosphere 2011, 84, 908-912
37. European Commission, Directorate General Health and Consumer Protection. Guidance Document on Method Validation and Quality Control Procedures for Pesticide Residues Analyses in Food and Feed; SANCO/10684/2009; European Commission: Brussels, Belgium, Jan 1, 2010.
38. Zhang, X.; Mobley, N.; Zhang, J.; Zheng, X.; Lu, L.; Ragin, O.; Smith, C. J. Analysis of agricultural residues on tea using d-SPE sample preparation with GC-NCI-MS and UHPLC-MS/MS J. Agric. Food Chem. 2010, 58, 11553-11560