Size and spatial distribution of micropores in SBA-15 using CM-SANS

Chemistry of Materials

Volumn 23, Issue 17, 2011, Pages 3828-3840

  Pollock, Rachel A ^a   Walsh, Brenna R ^a   Fry, Jason ^a   Ghampson, I Tyrone ^b   Melnichenko, Yuri B ^c   Kaiser, Helmut ^a   Pynn, Roger ^a,c   Desisto, William J ^b   Wheeler, M Clayton ^b   Frederick, Brian G ^a  

^a INDIANA UNIVERSITY   (United States)

^b University of Maine   (United States)

^c OAK RIDGE NATIONAL LABORATORY   (United States)

Author keywords

Mesoporous silica; micropore structure; neutron scattering; SBA 15

Indexed keywords

DIFFRACTION INTENSITY; DIRECT PROBE; MESO-PORES; MESOPORE; MESOPORE STRUCTURES; MESOPOROUS SILICA; MICRO-PORE STRUCTURES; MICROPORE-SIZE DISTRIBUTION; MICROPORES; NITROGEN DESORPTION; NON-LOCAL DENSITY FUNCTIONAL THEORIES; POLYMER TEMPLATES; SBA-15; SCATTERING LENGTH DENSITY; SMALL-ANGLE NEUTRON SCATTERING MEASUREMENTS; SURFACE HYDROXYL;

DENSITY FUNCTIONAL THEORY; DESORPTION; MESOPOROUS MATERIALS; NEUTRON SCATTERING; NEUTRONS; PARAFFINS; PORE SIZE; SILICA; SIZE DISTRIBUTION;

MICROPOROSITY;

EID: 80052428100     PISSN: 08974756     EISSN: 15205002     Source Type: Journal    
DOI: 10.1021/cm200707y     Document Type: Article

References (83)

1. Zhao, D.; Feng, J.; Huo, Q.; Melosh, N.; Fredrickson, G. H.; Chmelka, B. F.; Stucky, G. D. Science 1998, 279 (5350) 548-552
2. Melosh, N. A.; Lipic, P.; Bates, F. S.; Wudl, F.; Stucky, G. D.; Fredrickson, G. H.; Chmelka, B. F. Macromolecules 1999, 32 (13) 4332-4342
3. Zhao, D.; Sun, J.; Li, Q.; Stucky, G. D. Chem. Mater. 2000, 12, 275-279
4. Celer, E. B.; Kruk, M.; Zuzek, Y.; Jaroniec, M. J. Mater. Chem. 2006, 16 (27) 2824-2833
5. Jaroniec, M.; Solovyov, L. A. Chem. Commun. 2006, 2006, 2242-2244
6. Ryoo, R.; Ko, C. H.; Kruk, M.; Antochshuk, V.; Jaroniec, M. J. Phys. Chem. B 2000, 104, 11465-11471
7. Shin, H. J.; Ryoo, R.; Kruk, M.; Jaroniec, M. Chem. Commun. 2001, 349-350
8. Kruk, M.; Jaroniec, M.; Ko, C. H.; Ryoo, R. Chem. Mater. 2000, 12, 1961-1968
9. Linton, P.; Alfredsson, V. Chem. Mater. 2008, 20, 2878-2880
10. Galarneau, A.; Cambon, N.; Di Renzo, F.; Ryoo, R.; Choi, M.; Fajula, F. New J. Chem. 2003, 27 (1) 73-79
11. Albouy, P.-A.; Ayral, A. Chem. Mater. 2002, 14, 3391-3397
12. Schreiber, A.; Ketelsen, I.; Findenegg, G. H.; Hoinkis, E. Stud. Surf. Sci. Catal. 2007, 160, 17-24
13. Shin, T.; Findenegg, G. H.; Brandt, A. Prog. Colloid Polym. Sci. 2006, 133, 116-122
14. Zickler, G. A.; Jähnert, S.; Wagermaier, W.; Funari, S. S.; Findenegg, G. H.; Paris, O. Phys. Rev. B 2006, 73, 184109-1-184109-10
15. Selvam, P.; Bhatia, S. K.; Sonwane, C. G. Ind. Eng. Chem. Res. 2001, 40, 3237-3261
16. Xiao, F.-S. Top. Catal. 2005, 35 (1-2) 9-24
17. Ravikovitch, P. I.; Haller, G. L.; Neimark, A. V. Adv. Colloid Interface Sci. 1998, 76-77, 203-226
18. Imperor-Clerc, M.; Davidson, P.; Davidson, A. J. Am. Chem. Soc. 2000, 122, 11925-11933
19. Silvestre-Albero, A.; Jardim, E. O.; Bruijn, E.; Meynen, V.; Cool, P.; Sepulveda-Escribano, A.; Silvestre-Albero, J.; Rodriguez-Reinoso, F. Langmuir 2009, 25 (2) 939-943
20. Sonwane, C. G.; Ludovice, P. J. J. Mol. Catal. A: Chem. 2005, 238 (1-2) 135-137
21. Vradman, L.; Titelman, L.; Herskowitz, M. Microporous Mesoporous Mater. 2006, 93 (1-3) 313-317
22. Pollock, R. A.; Walsh, B. R.; Fry, J. A.; Ghampson, I. T.; Kaiser, H.; Pynn, R.; Melnichencko, Y.; Wheeler, M. C.; DeSisto, W. J.; Frederick, B. G. 2011, in press.
23. Baker, E. G.; Elliott, D. C., Catalytic Hydrotreating of Biomass-Derived Oils. In Pyrolysis Oils from Biomass: Producing, Analyzing and Upgrading; Soltes, E. J.; Milne, T. A., Eds. American Chemical Society: Washington, D.C., 1988; pp 228-240.
24. Churin, E.; Maggi, R.; Grange, P.; Delmon, B. Characterization and Upgrading of a Bio-Oil Produced by Pyrolysis of Biomass. In Proceedings of the International Conference on Thermochemical Biomass Conversion; Phoenix, AZ, 1988; Bridgwater, A. V.; Kuester, J. L., Eds.; Elsevier Applied Science: London, 1988; pp 896-909.
25. DeSisto, W. J.; Hill, N.; Beis, S. H.; Mukkamala, S.; Joseph, J.; Baker, C.; Ong, T.-H.; Stemmler, E. A.; Wheeler, M. C.; Frederick, B. G.; Heiningen, A. v. Energy Fuels 2010, 24, 2642-2651
26. Garcia-Perez, M.; Chaala, A.; Pakdel, H.; Kretschmer, D.; Roy, C. Biomass Bioenergy 2007, 31, 222-242
27. Ingram, L.; Mohan, D.; Bricka, M.; Steele, P.; Strobel, D.; Crocker, D.; Mitchell, B.; Mohammad, J.; Cantrell, K.; Pittman, C. U. Energy Fuels 2008, 22 (1) 614-625
28. Mullen, C. A.; Strahan, G. D.; Boateng, A. A. Energy Fuels 2009, 23 (5) 2707-2718
29. Huber, G. W.; Iborra, S.; Corma, A. Chem. Rev. 2006, 4044-4098
30. Ghampson, I. T.; Newman, C.; Kong, L.; Pier, E.; Hurley, K. D.; Pollock, R. A.; Walsh, B. R.; Goundi, B.; Wright, J.; Wheeler, M. C.; Meulenberg, R.; DeSisto, W. J.; Frederick, B. G.; Austin, R. N. Appl. Catal., A 2010, 388 (1-2) 57-67
31. Hoang, V.-T.; Huang, Q.; Ei, M.; Do, T.-O.; Kaliaguine, S. Langmuir 2005, 21, 2051-2057
32. Cassiers, K.; Linssen, T.; Mathieu, M.; Benjelloun, M.; Schrijnemakers, K.; Van Der Voort, P.; Cool, P.; Vansant, E. F. Chem. Mater. 2002, 14 (5) 2317-2324
33. Fulvio, P. F.; Pikus, S.; Jaroniec, M. J. Mater. Chem. 2005, 15, 5049-5053
34. Kruk, M.; Jaroniec, M.; Sayari, A. Langmuir 1997, 13, 6267-6273
35. Ojeda, M. L.; Esparza, J. M.; Campero, A.; Cordero, S. Phys. Chem. Chem. Phys. 2003, 5, 1859-1866
36. Ravikovitch, P. I.; Neimark, A. V. J. Phys. Chem. B 2001, 105, 6817-6823
37. Thommes, M.; Smarsly, B.; Groenewolt, M.; Ravitovitch, P. I.; Neimark, A. V. Langmuir 2006, 22, 756-764
38. van Grieken, R.; Calleja, G.; Stucky, G. D.; Melero, J. A.; Garcia, R. A.; Iglesias, J. Langmuir 2003, 19 (9) 3966-3973
39. De Paul, S. M.; Zwanziger, J. W.; Ulrich, R.; Wiesner, U.; Spiess, H. W. J. Am. Chem. Soc. 1999, 121 (24) 5727-5736
40. Nossov, A.; Haddad, E.; Guenneau, F.; Galarneau, A.; Di Renzo, F.; Fajula, F.; Gedeon, A. J. Phys. Chem. B 2003, 107 (45) 12456-12460
41. Chen, F.; Zhang, M. J.; Han, Y.; Xiao, F. S.; Yue, Y.; Ye, C. H.; Deng, F. J. Phys. Chem. B 2004, 108 (12) 3728-3734
42. Bhattacharya, S.; Coasne, B.; Hung, F. R.; Gubbins, K. E. Langmuir 2009, 25 (10) 5802-5813
43. Luan, A.; Hartmann, M.; Zhao, D.; Zhou, W.; Kevan, L. Chem. Mater. 1999, 11, 1621-1627
44. Zhang, F.; Yan, Y.; Yang, H.; Meng, Y.; Yu, C.; Tu, B.; Zhao, D. J. Phys. Chem. B 2005, 109 (18) 8723-8732
45. Smarsly, B.; Göltner, C.; Antonietti, M.; Ruland, W.; Hoinkis, E. J. Phys. Chem. B 2001, 105, 831-840
46. Esparza, J. M.; Ojeda, M. L.; Campero, A.; Domínguez, A.; Kornhauser, I.; Rojas, F.; Vidales, A. M.; López, R. H.; Zgrablich, G. Colloids Surf., A 2004, 241, 35-45
47. Vinh-Thang, H.; Huang, Q.; Eic, M.; Trong-On, D.; Kaliaguine, S. Langmuir 2005, 21 (11) 5094-5101
48. Brunauer, S.; Emmett, P. H.; Teller, E. J. Am. Chem. Soc. 1938, 60, 309-319
49. Neimark, A. V.; Ravikovitch, P. I. Microporous Mesoporous Mater. 2001, 44-45, 697-707
50. Neimark, A. V. Private communication, June 28, 2011.
51. Horvath, G.; Kawazoe, K. J. Chem. Eng. Jpn. 1983, 16 (6) 470-475
52. Saito, A.; Foley, H. C. AIChE J. 1991, 37 (3) 429-436
53. Cheng, L. S.; Yang, R. T. Chem. Eng. Sci. 1994, 49 (16) 2599-2609
54. Barrett, E. P.; Joyner, L. G.; Halenda, P. P. J. Am. Chem. Soc. 1951, 73, 373-380
55. Galarneau, A.; Lefevre, B.; Cambon, H.; Coasne, B.; Vallange, S.; Gabelica, Z.; Bellat, J. P.; Di Renzo, F. J. Phys. Chem. C 2008, 112 (33) 12921-12927
56. Schemmel, S.; Rother, G.; Eckerlebe, H.; Findenegg, G. H. J. Chem. Phys. 2005, 122 (24), 244718-1-244718-10.
57. Thommes, M.; Kohn, R.; Froba, M. J. Phys. Chem. B 2000, 104 (33) 7932-7943
58. Bao, X.; Zhao, X. S.; Li, X.; Li, J. Appl. Surf. Sci. 2004, 237 (1-4) 380-386
59. Jaroniec, M.; Solovyov, L. A. Langmuir 2006, 22 (16) 6757-6760
60. Wignall, G. D.; Bates, F. S. J. Appl. Crystallogr. 1987, 20, 28-40
61. McCool, B.; Murphy, L.; Tripp, C. P. J. Colloid Interface Sci. 2006, 295, 294-298
62. Escax, V.; Delahaye, E.; Imperor-Clerc, M.; Beaunier, P.; Appay, M.-D.; Davidson, A. Microporous Mesoporous Mater. 2007, 102 (1-3) 234-241
63. Marler, B.; Oberhagemann, U.; Vortmann, S.; Gies, H. Microporous Mater. 1996, 6, 375-383
64. Sonwane, C. G.; Bhatia, S. K.; Calos, N. Ind. Eng. Chem. Res. 1998, 37, 2271-2283
65. Kruk, M.; Jaroniec, M.; Sayari, A. Chem. Mater. 1999, 11, 492-500
66. Storck, S.; Bretinger, H.; Maier, W. F. Appl. Catal. A 1998, 174 (1-2) 137-146
67. Ehrburger-Dolle, F.; Morfin, I.; Geissler, E.; Bley, F.; Livet, F.; Vix-Guterl, C.; Saadallah, S.; Parmentier, J.; Reda, M.; Patarin, J.; Iliescu, M.; Werckmann, J. Langmuir 2003, 19, 4303-4308
68. Dierker, S. B.; Wiltzius, P. Phys. Rev. Lett. 1991, 66 (9) 1185-1188
69. Lin, M. Y.; Sinha, S. K.; Drake, J. M.; Wu, X. I.; Thiyagarajan, P.; Stanley, H. B. Phys. Rev. Lett. 1994, 72 (14) 2207-2210
70. Wiltzius, P.; Bates, F. S.; Dierker, S. B.; Wignall, G. D. Phys. Rev. A 1987, 36 (6) 2991-2994
71. Sinha, S. K., Small-angle scattering from porous materials. In Methods in the Physics of Porous Media; Wong, P.-Z., Ed.; Academic Press: San Diego, 1999; Vol. 35, pp 223-262.
72. Svehla, R. A. Estimated Viscosities and Thermal Conductivities of Gases at High Temperatures; NASA Lewis Research Center: Cleveland, OH, 1962; Vol. TR R-132, pp 1-120.
73. Grosman, A.; Ortega, C. Langmuir 2005, 21, 10515-10521
74. Galarneau, A.; Cambon, N.; Martin, T.; De Menorval, L. C.; Brunel, D.; Di Renzo, F.; Fajula, F. Stud. Surf. Sci. Catal. 2002, 141, 395-402
75. Reid, R. C.; Prausnitz, J. M.; Poling, B. E., The Properties of Gases and Liquids; McGraw-Hill: New York, 1987.
76. Zhuravlev, L. T. Langmuir 1987, 3, 316-318
77. Melnichenko, Y. B.; Wignall, G. D. J. Appl. Phys. 2007, 102, 021101-1-021101-24
78. Roe, R.-J., Methods of X-ray and Neutron Scattering in Polymer Science. Oxford University Press: New York, 2000.
79. Zholobenko, V. L.; Khodakov, A. Y.; Durand, D. Microporous Mesoporous Mater. 2003, 66, 297-302
80. Pikus, S.; Celer, E. B.; Jaroniec, M.; Solovyov, L. A.; Kozak, M. Appl. Surf. Sci. 2010, 256 (17) 5311-5315
81. Morishige, K.; Tateishi, M. Langmuir 2006, 22, 4165-4169
82. Diaz, M. C.; Hall, P. J.; Snape, C. E.; Brown, S. D.; Hughes, R. Ind. Eng. Chem. Res. 2002, 41, 6566-6571
83. Kim, M.-H.; Glinka, C. J.; Carter, R. N. Rev. Sci. Instrum. 2005, 76, 113904-1-113904-10