Determination of chloropropanols in foods by one-step extraction and derivatization using pressurized liquid extraction and gas chromatography-mass spectrometry

Journal of Chromatography A

Volumn 1218, Issue 39, 2011, Pages 6878-6883

  Racamonde, I ^a   Gonzalez P ^a   Lorenzo, R A ^a   Carro, A M ^a  

^a UNIVERSITY OF SANTIAGO DE COMPOSTELA   (Spain)

Author keywords

Bakery foods; BSTFA; Chloropropanols; Pressurized liquid extraction; Simultaneous extraction and derivatization, GC MS

Indexed keywords

1 ,3-DICHLORO-2-PROPANOL; 3-CHLOROPROPANE-1 ,2-DIOL; ANALYTES; ANALYTICAL METHOD; BOX-BEHNKEN DESIGN; BSTFA; CALIBRATION CURVES; CELL EXTRACTION; CHLOROPROPANOLS; DERIVATIZATIONS; DIATOMACEOUS EARTH; DISPERSANTS; DOEHLERT; ETHYL ACETATES; EXTRACTION PROCESS; EXTRACTION TIME; FLORISIL; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; GC-MS ANALYSIS; IN-SITU DERIVATIZATION; LIMITS OF QUANTIFICATION; NUMBER OF CYCLES; OPTIMUM CONDITIONS; PARTICULATE MATTER; PORE VOLUME; PRESSURIZED LIQUID EXTRACTION; RELATIVE STANDARD DEVIATIONS; RESPONSE SURFACE DESIGNS; SCREENING DESIGN; SILYLATIONS; SIMULTANEOUS EXTRACTION AND DERIVATIZATION, GC-MS; TRIFLUOROACETAMIDES; TRIMETHYLSILYL;

ADSORPTION; BAKERIES; CHEMICAL CONTAMINATION; DESIGN; GAS CHROMATOGRAPHY; LIQUID CHROMATOGRAPHY; LIQUIDS; MASS SPECTROMETRY; SODIUM; SODIUM SULFATE; VOLATILE FATTY ACIDS;

SOLVENT EXTRACTION;

1,3 DICHLORO 2 PROPANOL; ACETIC ACID ETHYL ESTER; ADSORBENT; ALPHA CHLOROHYDRIN; DISPERSANT; INFUSORIAL EARTH; MAGNESIUM TRISILICATE; PROPANOL; SODIUM SULFATE; UNCLASSIFIED DRUG;

ACCURACY; ANALYTIC METHOD; ANALYTICAL PARAMETERS; ARTICLE; BREAD; CALIBRATION; CEREAL; CONCENTRATION (PARAMETERS); DERIVATIZATION; DISPERSION; EXPERIMENTAL DESIGN; EXTRACTION; FAST FOOD; FOOD ANALYSIS; LIMIT OF QUANTITATION; MASS FRAGMENTOGRAPHY; ONE STEP EXTRACTION; PRESSURIZED LIQUID EXTRACTION; PRIORITY JOURNAL; PROCESS OPTIMIZATION; RESPONSE SURFACE METHOD; SENSITIVITY ANALYSIS; TIME PERCEPTION;

ALPHA-CHLOROHYDRIN; ANALYSIS OF VARIANCE; BREAD; CEREALS; CHEMICAL FRACTIONATION; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; GLYCEROL; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; TEMPERATURE; TRIMETHYLSILYL COMPOUNDS;

EID: 80052314293     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2011.08.004     Document Type: Article

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