Microwave-assisted synthesis of metal complexes

Mini-Reviews in Organic Chemistry

Volumn 8, Issue 3, 2011, Pages 315-333

  Abe, Taichi ^a   Miyazawa, Akira ^a   Kawanishi, Yuji ^a   Konno, Hideo ^a  

^a NATIONAL INSTITUTE OF ADVANCED INDUSTRIAL SCIENCE AND TECHNOLOGY AIST   (Japan)

Author keywords

Coordination compound; Metal complex; Microwave heating; Organometallic compound; Synthesis; Transition metal

Indexed keywords

COORDINATION REACTIONS; INORGANIC COMPOUNDS; METAL COMPLEXES; MICROWAVE HEATING; ORGANOMETALLICS; SYNTHESIS (CHEMICAL);

COORDINATION COMPOUNDS; INORGANIC CHEMISTRY; INORGANIC MATERIALS; MATERIAL SCIENCE; MICROWAVE ASSISTED SYNTHESIS; MICROWAVE CHEMISTRY; MICROWAVE TECHNIQUE; MICROWAVE-HEATING; ORGANOMETALLIC COMPOUNDS; SYNTHESISED;

TRANSITION METALS;

EID: 79960078596     PISSN: 1570193X     EISSN: None     Source Type: Journal    
DOI: 10.2174/157019311796197346     Document Type: Review

References (119)

1. Streitwieser, A.; Ward, H. R. Organic compounds in microwave discharge. J. Am. Chem. Soc., 1962, 84, 1065-1066.
2. Liu, S. W.; Wightman, J. P. Decomposition of simple alcohols, ethers and ketones in a microwave discharge. J. Appl. Chem. Biotechnol., 1971, 21, 168-172.
3. Hesek, J. A.; Wilson, R. C. Use of microwave oven in in-process control. Anal. Chem., 1974, 46, 1160.
4. Abu-Samra, A.; Morris, J. S.; Koirtyohann, S. R. Wet ashing of some biological samples in a microwave oven. Anal. Chem., 1975, 47, 1475-1477.
5. Barrett, P.; Davidowski, L. J.; Penaro, K. W.; Copeland, T. R. Microwave oven-based wet digestion technique. Anal. Chem., 1978, 50, 1021-1023.
6. Gedye, R.; Smith, F.; Westaway, K.; Ali, H.; Baldisera, L.; Laberge, L.; Rousell, J. The use of microwave ovens for rapid organic synthesis. Tetrahedron Lett., 1986, 27, 279-282.
7. Giguere, R. J.; Bray, T. L.; Duncan, S. M.; Majetich, G. Application of commercial microwave ovens to organic synthesis. Tetrahedron Lett., 1986, 27, 4945-4948.
8. Mingos, D. M. P.; Baghurst, D. R. Applications of microwave dielectric heating effects to synthetic problems in chemistry. Chem. Soc. Rev., 1991, 20, 1-47.
9. Galema, S. A. Microwave chemistry. Chem. Soc. Rev., 1997, 26, 233-238.
10. Gabriel, C.; Gabriel, S.; Grant, E. H.; Halstead, B. S. J.; Mingos, D. M. P. Dielectric parameters relevant to microwave dielectric heating. Chem. Soc. Rev., 1998, 27, 213-223.
11. de la Hoz, A.; Díaz-Ortiz, Á.; Moreno, A. Microwaves in organic synthesis. Thermal and non-thermal microwave effects. Chem. Soc. Rev., 2005, 34, 164-178.
12. Baghurst, D. R.; Mingos, D. M. P.; Watson, M. J. Application of microwave dielectric loss heating effects for the rapid and convenient synthesis of oraganometallic compounds. J. Organomet. Chem., 1989, 368, C43-C45.
13. Ali, M.; Bond, S. P.; Mbogo, S. A.; McWhinnie, W. R.; Watts, P. M. Use of a domestic microwave oven in organometallic chemistry. J. Organomet. Chem., 1989, 371, 11-13.
14. 2 films. Nature, 1991, 353, 737-740.
15. Fujita, E. Photochemical carbon dioxide reduction with metal complexes. Coord. Chem. Rev., 1999, 185, 373-384.
16. Abe, T.; Shinozaki, K. Tuning of luminescent spectra of neutral ruthenium(II) complexes by crystal waters. Inorg. Chem., 2005, 44, 849-851.
17. Abe, T.; Itakura, T.; Ikeda, N.; Shinozaki, K. Luminescence color change of a platinum(II) complex solid upon mechanical grinding. Dalton Trans., 2009, 711-715.
18. Abe, T.; Suzuki, T.; Shinozaki, K. Luminescence change by the solvent of crystallization, solvent reorganization and vapochromism of neutral dicyanoruthenium(II) complex in the solid state. Inorg. Chem., 2010, 49, 1794-1800.
19. +. Inorg. Chem., 2009, 48, 10138-10145.
20. Kobayashi, A.; Konno, H.; Sakamoto, K.; Sekine, A.; Ohashi, Y.; Iida, M.; Ishitani, O. Transition metal complexes coordinated by an NAD(P)H model compound and their enhanced hydride-donating abilities in the presence of a base. Chem. Eur. J., 2005, 11, 4219-4226.
21. 2. Inorg. Chim. Acta, 2000, 299, 155-163.
22. + model compounds: a model for enzymatic reactions by aldehyde dehydrogenases. Angew. Chem., Int. Ed., 2000, 39, 4061-4063.
23. Kobayashi, A.; Takatori, R.; Kikuchi, I.; Konno, H.; Sakamoto, K.; Ishitani, O. Formation of novel 1:1 adducts accompanied by regioselective hydride transfer from transition-metal hydrido complexes to NAD(P) models. Organometallics, 2001, 20, 3361-3363.
24. Konno, H.; Ishii, Y.; Sakamoto, K.; Ishitani, O. Synthesis, spectroscopic characterization, electrochemical and photochemical properties of ruthenium(II) polypyridyl complexes with a tertiary amine ligand. Polyhedron, 2002, 21, 61-68.
25. Kitamura, M.; Ohkuma, T.; Inoue, S.; Sayo, N.; Kumobayashi, H.; Akutagawa, S.; Ohta, T.; Takaya, H.; Noyori, R. Homogeneous asymmetric hydrogenation of functionalized ketones. J. Am. Chem. Soc., 1988, 110, 629-631.
26. Miyaura, N.; Suzuki, A. Palladium-catalyzed cross-coupling reactions of organoboron compounds. Chem. Rev., 1995, 95, 2457-2483.
27. Baldo, M. A.; O'Brien, D. F.; You, Y.; Shoustikov, A.; Sibley, S.; Thompson, M. E. Highly efficient phosphorescent emission from organic electroluminescent devices. Nature, 1998, 395, 151-154.
28. Baghurst D. R.; Mingos, D. M. P. A new reaction vessel for accelerated syntheses using microwave dielectric super-heating effects. J. Chem. Soc. Dalton Trans., 1992, 7, 1151-1155.
29. Baghurst. D. R.; Mingos, D. M. P. Design and application of a reflux modification for the synthesis of organometallic compounds using microwave dielectric loss heating effects. J. Organomet. Chem., 1990, 384, C57-C60.
30. Matsumura-Inoue, T.; Tanabe, M.; Minami, T.; Ohashi, T. A remarkably rapid synthesis of ruthenium(II) polypyridine complexes by microwave irradiation. Chem. Lett., 1994, 23, 2443-2446.
31. Whittaker, A. G.; Mingos, D. M. P. Synthetic reactions using metal powders under microwave irradiation. J. Chem. Soc. Dalton Trans., 2002, 3967-3970.
32. Ardon, M.; Hayes, P. D.; Hogarth, G. Microwave-assisted reflux in organometallic chemistry: synthesis and structural determination of molybdenum carbonyl complexes. J. Chem. Educ., 2002, 79, 1249-1251.
33. Broomhead, J. A.; Young, C. G. Tris(2,2'-bipyridine)ruthenium(II) dichloride hexahydrate. Inorg. Synth., 1982, 21, 127-128.
34. Johnson, S. R.; Westmoreland, T. D.; Caspar, J. V.; Barqawi, K. R.; Meyer, T. J. Influence of variations in the chromophoric ligand on the properties of metal-to-ligand charge-transfer excited states. Inorg. Chem., 1988, 27, 3195-3200.
35. Ott, C.; Wouters, D.; Thijs, H. M. L.; Schubert, U. S. New preparation and purification methods for metallo-supramolecular block copolymers. J. Inorg. Organomet. Polym., 2007, 17, 241-249.
36. Ardon, M.; Hogarth, G.; Oscroft, D. T. W. Organometallic chemistry in a conventional microwave oven: the facile synthesis of group 6 carbonyl complexes. J. Organomet. Chem., 2004, 689, 2429-2435.
37. Barnard, T. M. and Leadbeater, N. E. Real-time monitoring of microwavepromoted organometallic ligand substitution reactions using in situ Raman spectroscopy. Chem. Commun., 2006, 34, 3615-3616.
38. 4{ethyl[3-(2-pyridyl)-1-pyrazoyl]acetate}]. Molecules, 2006, 11, 940-952.
39. Amarante, T. R.; Paz, F. A. A.; Gago, S.; Gonçalves, I. S.; Pillinger, M.; Rodrigues, A. E.; Abrantes, M. Microwave-assisted synthesis and crystal structure of oxo(diperoxo)(4,4'-di-tert-butyl-2,2'-bipyridine)-molybdenum(VI). Molecules, 2009, 14, 3610-3620.
40. Adil, K.; Marrot, J.; Leblanc, M.; Maisonneuve, V. Bis[tris(2-aminoethyl)amine] bis(pentafluoridooxidomolybdate) difluoride monohydrate. Acta Cystallogr., Sect. E: Struct. Rep. Online, 2007, E63, m1511-m1513.
41. Artillo, A.; Sala, G. D.; De Santis, M.; Llordes, A.; Ricart, S.; Spinella, A. Preparation of organometallic uracil-analogue Fischer carbene complexes: comparative study of conventional heating vs microwave heating. J. Organomet. Chem., 2007, 692, 1277-1284.
42. 6] complexes with triphenylphosphine, tert-butylbenzenes and a sterically hindered phenol as arene ligands. J. Organomet. Chem., 1997, 542, 99-103.
43. III single-molecule magnet. Inorg. Chem., 2006, 45, 5272-5274.
44. Bhojak, N.; Gudasaria, D. D.; Khiwani, N.; Jain, R. Microwave assisted synthesis spectral and antibacterial investigations on complexes of Mn(II) with amide containing ligands. E-J. Chem., 2007, 4, 232-237.
45. Causey, P. W.; Besanger, T. R.; Schaffer, P.; Valliant, J. F. Expedient multistep synthesis of organometallic complexes of Tc and Re in high effective specific activity. A new platform for the production of molecular imaging and therapy agents. Inorg. Chem., 2008, 47, 8213-8221.
46. + (X = C1, ONO). Inorg. Chem., 1990, 29, 1693-1700.
47. n] (L= bidentate ligand, n = 0-3) types of complexes with polypyridyl ligands; another example of the synthetic utility of 'ruthenium-blue' solution. Inorg. Chim. Acta, 1992, 195, 221-225.
48. +
49. 3 complexes thereof. Z. Anorg. Allg. Chem., 2009, 635, 471-478.
50. 99mTc(I)-metallocarborane complexes. Inorg. Chem., 2006, 45, 5727-5729.
51. Armstrong, A. F.; Valliant, J. F. Microwave-assisted synthesis of tricarbonyl rhenacarboranes: steric and electronic effects on the 1,2 → 1,7 carborane cage isomerization. Inorg. Chem., 2007, 46, 2148-2158.
52. 2-cooled apparatus in an unmodified commercial microwave oven. J. Organomet. Chem., 1993, 460, C28-C29.
53. Dabirmanesh, Q.; Fernando, S. I. S.; Roberts, R. M. G. Synthesis and decomplexation of (η-arene)(η-cyclopentadienyl)iron(II) hexafluorophosphates using microwave dielectric heating. J. Chem. Soc. Perkin Trans. 1, 1995, 743-749.
54. 5-cyclopentadienyl) iron(II) complexes with heteroatom and carbonyl substituents. Part I: oxygen and carbonyl substituents. J. Organomet. Chem., 2006, 691, 2641-2647.
55. Garringer, S. M.; Hesse, A. J.; Magers, J. R.; Pugh, K. R.; O'Reilly, S. A.; Wilson, A. M. Microwave synthesis of benchmark organo-iron complexes. Organometallics, 2009, 28, 6841-6844.
56. Puciová, M.; Ertl, P.; Toma, Š. Synthesis of ferrocenyl-substituted heterocycles: the beneficial effect of the microwave irradiation. Collect. Czech. Chem. Commun., 1994, 59, 175-185.
57. Villemin, D.; Martin, B.; Puciova, M.; Toma, S. Dry synthesis under microwave irradiation: synthesis of ferrocenylenons. J. Organomet. Chem., 1994, 484, 27-31.
58. Janková, Š.; Císařová, I.; Uhlík, F.; Štepnička, P.; Kotora, M. Synthesis and characterisation of Dewar benzene-ferrocene conjugates. Dalton Trans., 2009, 17, 3137-3139.
59. Barghurst, D. R.; Mingos, D. M. P. Design and application of a reflux modification for the synthesis of organometallic compounds using microwave dielectric loss heating effects. J. Organomet. Chem., 1990, 384, C57-C60.
60. Kuhnert, N.; Danks, T. N. Microwave accelerated synthesis of cyclopentadienyl bis-phosphine ruthenium(II) thiolato complexes using focused microwave irradiation. J. Chem. Res. (S), 2002, 66-68.
61. 3RuCl(L-L')] complexes (L-L': chelate ligands with P-, N-, or S-donor atoms) by displacement of arene sssligands. Eur. J. Inorg. Chem., 2009, 8, 1003-1010.
62. Bolink, H. J.; Cappelli, L.; Coronado, E.; Grätzel, M.; Nazeeruddin, Md. K. Efficient and stable solid-state light-emitting electrochemical cell using tris(4,7-diphenyl-1,10-phenanthroline)ruthenium(II) hexafluorophosphate. J. Am. Chem. Soc., 2006, 128, 46-47.
63. Greene, D. L.; Mingos, D. M. P. Application of microwave dielectric loss heating effects for the rapid and convenient synthesis of ruthenium(II) polypyridine complexes. Trans. Met. Chem., 1991, 16, 71-72.
64. 6] with M = Fe and Ru. Inorg. Chem. Commun., 2008, 11, 1006-1008.
65. Martineau, D.; Beley, M.; Gros, P. C.; Cazzanti, S.; Caramori, S.; Bignozzi, C. A. Tuning of ruthenium complex properties using pyrrole-and pyrrolidine-containing polypyridine ligands. Inorg. Chem., 2007, 46, 2272-2277.
66. Jasimuddin, Sk.; Byabartta, P.; Mostafa, G.; Lu, T.-H.; Sinha, C. Synthesis, spectral studies, crystal structure and redox properties of homoleptic trischelated ruthenium(II)-arylazoimidazol. Polyhedron, 2004, 23, 727-733.
67. Grabulosa, A.; Beley, M.; Gros, P. C. Remarkable effect of 4-substituted 2,2'-bipyridine ligands on the stereochemistry of ruthenium(II) complexes. Eur. J. Inorg. Chem., 2008, 11, 1747-1751.
68. Wu, F.; Thummel, R. P. Ru(II) complexes of crowded delocalized diimine ligands. Inorg. Chim. Acta, 2002, 327, 26-30.
69. 4+ triple helicate and its interaction with DNA. Chem. Eur. J., 2008, 14, 10535-10538.
70. Xiao, X.; Sakamoto, J.; Tanabe, M.; Yamazaki, S.; Yamabe, S.; Matsumura-Inoue, T. Microwave synthesis and electrospectrochemical study on ruthenium(II) polypyridine complexes. J. Electroanal. Chem., 2002, 527, 33-40.
71. 2 by microwave-activated reactions (R: H, Me, tert-But) (L-L: substituted bibenzimidazoles, bipyrimidine, and phenanthroline). Inorg. Chim. Acta, 2004, 357, 4496-4503.
72. Schwalbe, M.; Schäfer, B.; Görls, H.; Rau, S.; Tschierlei, S.; Schmitt, M.; Popp, J.; Vaughan, G.; Henry, W.; Vos, J. G. Synthesis and characterisation of poly(bipyridine)ruthenium complexes as building blocks for heterosupramolecular arrays. Eur. J. Inorg. Chem., 2008, 21, 3310-3319.
73. Abrahamsson, M.; Jäger, M.; Österman, T.; Eriksson, L.; Persson, P.; Becker, H. C.; Johansson, O.; Hammarström, L. A 3.0Bs room temperature excited state lifetime of a bistridentate RuII-polypyridine complex for rodlike molecular arrays. J. Am. Chem. Soc., 2006, 128, 12616-12617.
74. 3MLCT state lifetimes: sensitizers for rod-like molecular arrays. J. Am. Chem. Soc., 2008, 130, 15533-15542.
75. 3MLCT excited state lifetimes. Inorg. Chem., 2009, 48, 3228-3238.
76. Sasaki, I.; Daran, J. C.; Aït-Haddou, H.; Balavoine, G. G. A. New annelated 2,2':6',2''-terpyridines and their Ru(II) complexes: synthesis and characterization. Inorg. Chem. Commun., 1998, 1, 354-357.
77. Ziegler, M.; Monney, V.; Stoeckli-Evans, H.; Von Zelewsky, A.; Sasaki, I.; Dupic, G.; Daran, J. C.; Balavoine, G. G. A. Complexes of new chiral terpyridyl ligands. Synthesis and characterization of their ruthenium(II) and rhodium(III) complexes. J. Chem. Soc. Dalton Trans., 1999, 667-675.
78. Funaki, T.; Yanagida, M.; Onozawa-Komatsuzaki, N.; Kasuga, K.; Kawanishi, Y.; Kurashige, M.; Sayama, K.; Sugihara, H. Synthesis of a new class of cyclometallated ruthenium(II) complexes and their application in dyesensitized solar cells. Inorg. Chem. Commun., 2009, 12, 842-845.
79. Pezet, F.; Daran, J. C.; Sasaki, I.; Aït-Haddou, H.; Balavoine, G. G. A. Highly diastereoselective preparation of ruthenium bis(diimine) sulfoxide complexes: new concept in the preparation of optically active octahedral ruthenium complexes. Organometallics, 2000, 19, 4008-4015.
80. Munery, S.; Jaud, J.; Bonvoisin, J. Synthesis and characterization of bis(bipyridine)ruthenium(II) complexes with bromo or protected ethynyl β-diketonato ligands. Inorg. Chem. Commun., 2008, 11, 975-977.
81. Díaz-Valenzuela, M. B.; Phillips, S. D.; France, M. B.; Gunn, M. E.; Clarke, M. L. Enantioselective hydrogenation and transfer hydrogenation of bulky ketones catalyzed by a ruthenium complex of a chiral tridentate ligand. Chem. Eur. J., 2009, 15, 1227-1232.
82. Bashilov, A. V.; Fedorova, A. A.; Runov, V. K. Reduction of ruthenium(IV) to ruthenium(III) in aqueous alcohol solutions of hydrochloric acid under microwave radiation. J. Anal. Chem., 2000, 55, 1123-1155.
83. 3 with microwave sample preparation. J. Anal. Chem., 2004, 59, 296-298.
84. Leadbeater, N. E.; Shoemaker, K. M. Preparation of ruthenium and osmium carbonyl complexes using microwave hating: demonstrating the use of a gasloading accessory and real-time reaction monitoring by means of a digital camera. Organometallics, 2008, 27, 1254-1258.
85. 6]Cl, featuring the first reported X-ray crystal structure. Inorg. Chem. Commun., 2008, 11, 44-46.
86. 3. J. Organomet. Chem., 2009, 694, 3526-3528.
87. Harcourt, E. M.; Yonis, S. R.; Lynch, D. E.; Hamilton, D. G. Microwaveassisted synthesis of cyclopentadienyl-cobalt sandwich complexes from diaryl acetylenes. Organometallics, 2008, 27, 1653-1656.
88. Tan, N. Y.; Xiao, X. M.; Li, Z. L.; Matsumura-Inoue, T. Microwave synthesis, characterization and DNA-binding properties of a new cobalt(II) complex with 2,6-bis(benzimidazol-2-yl)pyridine. Chin. Chem. Lett., 2004, 15, 687-690.
89. Murugavel, R.; Davis, P.; Walawalkar, M. G. First examples of metal cyclohexylphosphonates: influence of the choice of synthetic route on the product. Z. Anorg. Allg. Chem., 2005, 631, 2806-2811.
90. Amarante, D.; Cherian, C.; Emmel, C.; Chen, H.-Y.; Dayal, S.; Koshy, M.; Megehee, E. G. Improved synthetic routes to rhodium bipyridine complexes: comparison of microwave vs. conventional synthesis. Inorg. Chim. Acta, 2005, 358, 2231-2238.
91. 211At complexes as potential precursors for astatine radiopharmaceuticals. Part I: synthesis. Bioconjug. Chem., 2008, 19, 958-965.
92. Yoshikawa, N.; Sakamoto, J.; Matsumura-Inoue, T.; Takashima, H.; Tsukahara, K.; Kanehisa, N.; Kai, Y. Electrochemical and phosphorescent properties of new Ir(III) complexes coordinated by various bipyridine derivatives. Anal. Sci., 2004, 20, 711-716.
93. Yoshikawa, N.; Matsumura-Inoue, T. Electrochemical and phosphorescent properties of new mixed-ligand Ir(III) complexes coordinated with both terpyridine and various bipyridine derivatives. Anal. Sci., 2003, 19, 761-765.
94. IIItolylterpyridine complexes. Eur. J. Inorg. Chem., 2007, 13, 1911-1919.
95. Konno, H.; Sasaki, Y. Selective one-pot synthesis of facial tris-orthometalated iridium(III) complexes using microwave irradiation. Chem. Lett., 2003, 32, 252-253.
96. Saito, K.; Matsusue, N.; Kanno, H.; Hamada, Y.; Takahashi, H.; Matsumura, T. Microwave synthesis of iridium(III) complexes: synthesis of highly efficient orange emitters in organic light-emitting devices. Jpn. J. Appl. Phys., 2004, 43, 2733-2734.
97. Barghurst, D. R.; Cooper, S. R.; Greene, D. L.; Mingos, D. M. P.; Reynolds, S. M. Application of microwave dielectric loss heating effects for the rapid and convenient synthesis of coordination compounds. Polyhedron, 1990, 9, 893-895.
98. Buslaeva, T. M.; Kravchenko, V. V.; Kopylova, E. V.; Kashiricheva, I. I.; Alekseeva, O. A.; Kazantsev, S. S. Synthesis and structure of iridium complex with thiocarbamide. Crystallogr. Rep., 2008, 53, 775-780.
99. Zhang, S.-H.; Tang, M.-F.; Ge, C.-M. Microwave synthesis, crystal structure and magnetic behavior of a Schiff base trinuclear nickel cluster. Z. Anorg. Allg. Chem., 2009, 635, 1442-1446.
100. II. J. Organomet. Chem., 1994, 479, 153-157.
101. Gosiewska, S.; Herreras, S. M.; Lutz, M.; Spek, A. L.; Havenith, R. W. A.; van Klink, G. P. M.; van Koten, G.; Klein Gebbink, R. J. M. Synthesis, structure, and catalytic performance of diasteropure five-coordinated NCN-pincer palladium(II) complexes bearing bulky amino acid substituents. Organometallics, 2008, 27, 2549-2559.
102. Tu, T.; Malineni, J.; Dötz, K. H. A novel pyridine-bridged bisbenzimidazolylidene pincer palladium complex: synthesis and catalytic properties. Adv. Synth. Catal., 2008, 350, 1791-1795.
103. Shoemaker, K. A.; Leadbeater, N. E. A fast and easy approach to the synthesis of Zeise's salt using microwave heating. Inorg. Chem. Commun., 2009, 12, 341-342.
104. Januário-Charmier, M. A.; Kukushkin, V. Yu.; Pomberio, A. J. L. Microwave-assisted [2 + 3] cycloaddition of nitrones to platinum-(II) and-(IV) bound organonitriles. Dalton Trans., 2003, 2540-2543.
105. 2]. Selective formation of mono-oxadiazoline and mixed bis-oxadiazoline complexes under thermal and microwave conditions. Dalton Trans., 2004, 166-171.
106. Lasri, J.; Januário-Charmier, M. A.; Haukka, M.; Pombeiro, A. J. L. Stereospecific synthesis of polysubstituted E-olefins by reaction of acyclic nitrones with free and platinum(II) coordinated organonitriles. J. Org. Chem., 2006, 72, 750-755.
107. Lasri, J.; Januário-Charmier, M. A.; Guedes da Silva, M. F. C.; Pombeiro, A. J. L. Direct synthesis of (imine)platinum(II) complexes by iminoacylation of ketoximes with activated organonitrile ligands. Dalton Trans., 2006, 5062-5067.
108. Mukhopadhyay, S.; Lasri, J.; Januário-Charmier, M. A.; Guedes da Silva, M. F. C.; Pombeiro, A. J. L. Microwave synthesis of mono-and bis-tetrazolato complexes via 1,3-dipolar cycloaddition of organonitriles with platinum(II)-bound azides. Dalton Trans., 2007, 5297-5304.
109. Mukhopadhyay, S.; Lasri, J.; Guedes da Silva, M. F. C.; Januário-Charmier, M. A.; Pombeiro, A. J. L. Trans-bis[5-(4-fluorophenyl)tetrazolato] bis(triphenylphosphine)platinum(II). Acta Cystallogr., Sect. E: Struct. Rep. Online, 2007, E63, m2656.
110. Smoleński, P.; Mukhopadhyay, S.; Guedes da Silva, M. F. C.; Januário-Charmier, M. A.; Pombeiro, A. J. L. New water-soluble azido-and derived tetrazolato-platinum(II) complexes with PTA. Easy metal-mediated synthesis and isolation of 5-substituted tetrazoles. Dalton Trans., 2008, 6546-6555.
111. Godbert, N.; Pugliese, T.; Aiello, I.; Bellusci, A.; Crispini, A.; Ghedini, M. Efficient, ultrafast, microwave-assisted syntheses of cycloplatinated complexes. Eur. J. Inorg. Chem., 2007, 32, 5105-5111.
112. Lombard, C. K.; Myers, K. L.; Platt, Z. H.; Holland, A. W. Kinetics of reductive elimination from platinum(IV) as a probe for nonthermal effects in microwave-heating reactions. Organometallics, 2009, 28, 3303-3306.
113. Carlsson, M.; Eliasson, B. One-pot synthesis of trans mono-or diarylalkynyl substituted platinum(II) compounds with tertiary phosphine or phosphite ligands. Organometallics, 2006, 25, 5500-5502.
114. Singh, R. V.; Chaudhary, P.; Chauhan, S.; Swami, M. Microwave-assisted synthesis, characterization and biological activities of organotin(IV) complexes with some thio Schiff bases. Spectrochim. Acta, Part A, 2009, 72, 260-268.
115. Hegedus, L. S.; Sundermann, M. J.; Dorhout, P. K. Synthesis, complexation, and coordination oligomerization of 1,8-pyrazine-capped 5,12-dioxocyclams. Inorg. Chem., 2003, 42, 4346-4354.
116. n complex. Inorg. Chim. Acta, 2009, 362, 2435-2439.
117. Carballo, R.; Covelo, B.; Fernández-Hermida, N.; García-Martínez, E.; Lago, A. B.; Vázquez-López, E. M. Anion effect on the construction of copper(II) coordination polymers with the twisted ligand bis(4-pyridylthio)methane. Polyhedron, 2008, 27, 3247-3254.
118. Mohanan, K.; Kumari, B. S.; Rijulal, G. Microwave assisted synthesis, spectroscopic, thermal, and antifungal studies of some lanthanide(III) complexes with a heterocyclic bishydrazone. J. Rare Earths, 2008, 26, 16-21.
119. 3) (Ln = Ho, Er, Tm, Yb, Lu, Y). J. Solid State Chem., 2008, 181, 3065-3070.