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41
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64349102605
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In a previous report (ref 26, the presence of a 2-fold rotation axis in mer-1 through the pyridyl 4-positions was referred to as quasi-C2 symmetry in analogy to [Ru(tpy)2]2, However, the complex is best described by the symmetry label D2
-
2.
-
-
-
-
43
-
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0001219771
-
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Jahng, Y.; Thummel, R. P.; Bott, S. G. Inorg. Chem. 1997, 36, 3133-3138.
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-
44
-
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84869265941
-
-
Only observed for H3 in mer-1 because of overlapping resonances for the H2 proton, see ref 38. A similar change in the 4J2,4 coupling constant upon coordination is also observed in all studied complexes Δ4J2,4, 0.3 Hz
-
2,4 = -0.3 Hz).
-
-
-
-
45
-
-
84869270197
-
-
+].
-
+].
-
-
-
-
46
-
-
64349104328
-
-
The complexes are stable and can be stored under nitrogen for weeks without noticeable decomposition
-
The complexes are stable and can be stored under nitrogen for weeks without noticeable decomposition.
-
-
-
-
47
-
-
64349116330
-
-
Johansson, K. O.; Lotoski, J. A.; Tong, C. C; Hanan, G. S. Chem. Commun. 2000, 819, 820.
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Hanan, G.S.4
-
51
-
-
84869270198
-
-
II species upon column chromatography on silica and preparative HPLC. Attempted isomerization above 200 °C resulted in decomposition of the complexes.
-
II species upon column chromatography on silica and preparative HPLC. Attempted isomerization above 200 °C resulted in decomposition of the complexes.
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-
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