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Volumn 48, Issue 7, 2009, Pages 3228-3238

Facile synthesis of bistridentate Ru II complexes based on 2,6-Di(quinolin-8-yl)pyridyl Ligands: Sensitizers with microsecond 3MLCT excited state lifetimes

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EID: 64349100823     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic802342t     Document Type: Article
Times cited : (69)

References (54)
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    • Encinas, S.; Flamigni, L.; Barigelletti, F.; Constable, E. C; Housecroft, C. E.; Schofield, E. R.; Figgemeier, E.; Fenske, D.; Neuburger, M.: Vos, J. G.; Zehnder, M. Chem.-Eur. J. 2002, δ, 137-150.
  • 29
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    • Constable, E. C; Cargill Thompson, A. M. W.; Tocher, D. A; Daniels. M. A. M. New J. Chem. 1992, 16, 855-867.
    • Constable, E. C; Cargill Thompson, A. M. W.; Tocher, D. A; Daniels. M. A. M. New J. Chem. 1992, 16, 855-867.
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    • 0031059866 scopus 로고    scopus 로고
    • Otwinowski, Z.; Minor, W. Processing of X-Ray Diffraction Data Collected in Oscillation Mode. In Methods in Enzymology; Carter, C. W., Sweet, R. M., Eds.; Academic Press: New York, 1997; 276, Macromolecular Crystallography, Part A, pp 307-326.
    • Otwinowski, Z.; Minor, W. Processing of X-Ray Diffraction Data Collected in Oscillation Mode. In Methods in Enzymology; Carter, C. W., Sweet, R. M., Eds.; Academic Press: New York, 1997; Vol. 276, Macromolecular Crystallography, Part A, pp 307-326.
  • 36
    • 84869268707 scopus 로고    scopus 로고
    • Sheldrick, G. M. SHELXL·97, Release 97-2; University of Göttingen: Göttingen, Germany, 1997.
    • Sheldrick, G. M. SHELXL·97, Release 97-2; University of Göttingen: Göttingen, Germany, 1997.
  • 41
    • 64349102605 scopus 로고    scopus 로고
    • In a previous report (ref 26, the presence of a 2-fold rotation axis in mer-1 through the pyridyl 4-positions was referred to as quasi-C2 symmetry in analogy to [Ru(tpy)2]2, However, the complex is best described by the symmetry label D2
    • 2.
  • 44
    • 84869265941 scopus 로고    scopus 로고
    • Only observed for H3 in mer-1 because of overlapping resonances for the H2 proton, see ref 38. A similar change in the 4J2,4 coupling constant upon coordination is also observed in all studied complexes Δ4J2,4, 0.3 Hz
    • 2,4 = -0.3 Hz).
  • 45
    • 84869270197 scopus 로고    scopus 로고
    • +].
    • +].
  • 46
    • 64349104328 scopus 로고    scopus 로고
    • The complexes are stable and can be stored under nitrogen for weeks without noticeable decomposition
    • The complexes are stable and can be stored under nitrogen for weeks without noticeable decomposition.
  • 51
    • 84869270198 scopus 로고    scopus 로고
    • II species upon column chromatography on silica and preparative HPLC. Attempted isomerization above 200 °C resulted in decomposition of the complexes.
    • II species upon column chromatography on silica and preparative HPLC. Attempted isomerization above 200 °C resulted in decomposition of the complexes.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.