4′-Chloro-2,2′:6′,2″-terpyridine (L): ethyl sulfate salts of [H2L]2+ and the single crystal structures of [H2L][EtOSO3]Cl · H2O and [ML2][PF6]2 with M = Fe and Ru

Inorganic Chemistry Communications

Volumn 11, Issue 9, 2008, Pages 1006-1008

  Beves, Jonathon E ^a   Constable, Edwin C ^a   Housecroft, Catherine E ^a   Neuburger, Markus ^a   Schaffner, Silvia ^a   Zampese, Jennifer A ^a  

^a UNIVERSITY OF BASEL   (Switzerland)

Author keywords

4 Chloro 2,2 :6 ,2 terpyridine; Coordination; Heterocyclic; Iron; Ruthenium

Indexed keywords

EID: 50249090958     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2008.04.026     Document Type: Article

References (48)

1. Constable E.C., and Ward M.D. J. Chem. Soc., Dalton Trans. (1990) 1405
2. Constable E.C., Cargill Thompson A.M.W., Tocher D.A., and Daniels M.A.M. New J. Chem. 16 (1992) 855
3. See for example:. Constable E.C., Housecroft C.E., and Schneider A. J. Organomet. Chem. 573 (1999) 101
4. Constable E.C., Housecroft C.E., and Tao Y. Synthesis (2004) 869
5. Schubert U.S., Eschbaumer C., Hien O., and Andres P.R. Tetrahedron Lett. 42 (2001) 4705
6. Zhang Z., Mikkola S., and Lonnberg H. Tetrahedron 63 (2007) 11716
7. Chow H.S., Constable E.C., Housecroft C.E., Neuburger M., and Schaffner S. Dalton Trans. (2006) 2881
8. Sénéchal-David K., Leonard J.P., Plush S.E., and Gunnlaugsson T. Org. Lett. 8 (2006) 2727
9. Veauthier J.M., Carlson C.N., Collis G.E., Kiplinger J.L., and John K.D. Synthesis (2005) 2683
10. Sakamoto S., Tamura T., Furukawa T., Komatsu Y., Ohtsuka E., Kitamura M., and Inoue H. Nucleic Acids Res. 31 (2003) 1416
11. Liu X., McInnes E.J.L., Kilner C.A., Thornton-Pett M., and Halcrow M.A. Polyhedron 20 (2001) 2889
12. Wang J., Fang Y.-Q., Hanan G.S., Loiseau F., and Campagna S. Inorg. Chem. 44 (2005) 5
13. Chambers J., Eaves B., Parker D., Claxton R., Ray P.S., and Slattery S.J. Inorg. Chim. Acta 359 (2006) 2400
14. See for example. Chow H.S., Constable E.C., Housecroft C.E., and Neuburger M. Dalton Trans. (2003) 4568
15. Constable E.C., Housecroft C.E., Neuburger M., Schaffner S., and Smith C.B. Dalton Trans. (2005) 2259
16. Constable E.C., Hermann B.A., Housecroft C.E., Neuburger M., Schaffner S., and Scherer L.J. New J. Chem. 29 (2005) 1475
17. See for example:. Constable E.C., Handel R.W., Housecroft C.E., Morales A.F., Ventura B., Flamigni L., and Barigelletti F. Chem. Eur. J. 11 (2005) 4024
18. Constable E.C., and Harverson P. Inorg. Chim. Acta 252 (1996) 9
19. Constable E.C., Harverson P., and Housecroft C.E. J. Chem. Soc., Dalton Trans. (1999) 3693
20. Borgström M., Ott S., Lomoth R., Bergquist J., Hammarström L., and Johansson O. Inorg. Chem. 45 (2006) 4820
21. Newkome G.R., Cardullo F., Constable E.C., Moorefield C.N., and Cargill Thompson A.M.W. J. Chem. Soc., Chem. Commun. (1993) 925
22. Burazerovic S., Gradinaru J., Pierron J., and Ward T.R. Angew. Chem. Int. Ed. 46 (2007) 5510
23. See for example:. Weidl C.H., Precup A.A., Eschbaumer C., and Schubert U.S. Polym. Mater. Sci. Eng. 84 (2001) 937
24. Ott C., Wouters D., Thijs H.M.L., and Schubert U.S. J. Inorg. Organomet. Polym. Mater. 17 (2007) 241
25. Shunmugam R., and Tew G.N. J. Am. Chem. Soc. 127 (2005) 13567
26. Schubert U.S., Schmatloch S., and Precup A.A. Des. Monomers Polym. 5 (2002) 211
27. Schubert U.S., Hien O., and Eschbaumer C. Macromol. Rapid Commun. 21 (2000) 1156
28. Meier M.A.R., Wouters D., Ott C., Guillet P., Fustin C.-A., Gohy J.-F., and Schubert U.S. Macromolecules 39 (2006) 1569
29. Andres P.R., and Schubert U.S. Synthesis (2004) 1229
30. Beves J.E., Constable E.C., Housecroft C.E., Neuburger M., and Schaffner S. Acta Crystallogr., Sect. E 62 (2006) o2497
31. You W., Yang X.Y., Yao C., and Huang W. Acta Crystallogr., Sect. E 64 (2008) m79
32. Huang W., and Qian H. J. Mol. Struct. 874 (2008) 64
33. Huang W., and Qian H. J. Mol. Struct. 832 (2007) 108
34. J.E. Beves, E.C. Constable, C.E. Housecroft, M. Neuburger, S. Schaffner, Polyhedron, in press.
35. J.E. Beves, E.C. Constable, C.E. Housecroft, M. Neuburger, S. Schaffner, J.A. Zampese, Eur. J. Org. Chem., doi: 10.1002/ejoc.200800301.
36. +.
37. -1, T = 173 K, 4629 reflections collected. Refinement of 3351 reflections (254 parameters) with I > 3σ (I) converged at final R1 = 0.0312 (R1 all data = 0.0462), wR2 = 0.0326 (wR2 all data = 0.0485), gof = 1.106.
38. Drew M.G.B., Hudson M.J., Iveson P.B., Russell M.L., Liljenzin J.-O., Skålberg M., Spjuth L., and Madic C. J. Chem. Soc., Dalton Trans. (1998) 2973
39. Kepert C.J., Skelton B.W., and White A.H. Aust. J. Chem. 47 (1994) 391
40. Berthon C., and Grigoriev M.S. Acta Crystallogr., Sect. E 61 (2005) o1216
41. Charushnikova I.A., and Den Auwer C. Russ. J. Coord. Chem. 30 (2004) 511
42. Robertson K.N., Bakshi P.K., Lantos S.D., Cameron T.S., and Knop O. Can. J. Chem. 76 (1998) 583
43. Drew M.G.B., Iveson P.B., Hudson M.J., Liljenzin J.-O., Spjuth L., Cordier P.-Y., Enarsson A., Hill C., and Madic C. J. Chem. Soc., Dalton Trans. (2000) 821
44. 2Ru requires C 38.89, H 2.18, N 9.07%.
45. 2 requires C 40.89, H 2.29, N 9.54%.
46. -1, T = 173 K, 1944 reflections collected. Refinement of 1430 reflections (123 parameters) with I > 3σ (I) converged at final R1 = 0.0245 (R1 all data = 0.0341), wR2 = 0.0273 (wR2 all data = 0.0312), gof = 1.102.
47. 2 converged at final R1 = 0.0231 (R1 all data = 0.0236), wR2 = 0.0588 (wR2 all data = 0.0594), gof = 1.172.
48. McMurtrie J., and Dance I. CrystEngComm 7 (2005) 216