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Yields achieved on addition of various ligands: Triethylamine<1%; N,N,N',N'-tetramethylethylendiamine<1%; urotropine<1%; 2,2,6,6-tetramethylpiperidine<1%; N,N,N',N'-tetramethylguanidine<1%; N,N'-diphenyl urea16%; pyridine19%; N,N-dimethylpyridine<1%; 4-methylpyridine28%; 4-hydroxypyridine18%; 2,6-dimethylpyridine5%; 2,2'-bipyridine12%; indazole41%; pyridazine46%; pyrazine17%; phenanzine36%; acridine45%; imidazole7%; phenol20%; 2,4,6-tri-tert-butylphenol5%; 1,1,1,3,3,3-hexafluoropropanol46%. Reactions were carried out for 1h at 60°C, as described in Table1, entry1. In the case of monodentate systems, a metal/ligand ratio of 1:2 was used, whereas for polydentate systems the ratio was 1:1.
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