A method to determine volatile contaminants in polyethylene terephthalate (PET) packages by HDC-GC-FID and its application to post-consumer materials;Determinação de contaminantes voláteis em embalagens de polietileno terefalato (PET) por CDEL-CG-DIC e sua aplicação a materiais pós-consumo

Ciencia e Tecnologia de Alimentos

Volumn 30, Issue 4, 2010, Pages 1046-1055

  Fabris, Samanta ^a   Freire, Maria Teresa de Alvarenga ^b   Wagner, Roger ^a   Reyes, Felix Guillermo ^a  

^a UNIVERSITY OF CAMPINAS   (Brazil)

^b UNIVERSITY OF SÃO PAULO   (Brazil)

Author keywords

Extraction; Gas chromatography; PET packaging; Validation

Indexed keywords

EID: 79952330638     PISSN: 01012061     EISSN: 1678457X     Source Type: Journal    
DOI: 10.1590/S0101-20612010000400033     Document Type: Article

References (49)

1. ADAMS, R. P. Identifcation of essential oil components by gas chromatography/ mass spectrometry. Carol Stream: Allured, 1995. 698 p.
2. BAYER, F. L. Polyethylene terephthalate recycling for food contact applications: testing, safety and technologies: a global perspective. Food Additives and Contaminants, v. 19, p. 111-134, 2002. Supplement.
3. BRASIL. Portaria SVS/MS no 987, de 8 de dezembro de 1998. Regulamento Técnico para embalagens descartáveis de polietileno terefalato - PET - multicamada destinadas ao acondicionamento de bebidas não alcoólicas carbonatadas. Diário Ofcial [da] República Federativa do Brasil, Brasília, DF, 9 dez. 1998. Available from: http://www.anvisa.gov.br/e-legis/. Access in: 16 Oct. 2008.
4. BRASIL. Resolução da Diretoria Colegiada - RDC no 20, de 26 de março de 2008. Dispõe sobre o Regulamento Técnico sobre embalagens de polietilenotereftalato (PET) pós-consumo reciclado grau alimentício (PET-PCR grau alimentício) destinados a entrar em contato com alimentos. Diário Ofcial [da] República Federativa do Brasil, Brasília, DF, 2008. Available from: http://www.anvisa.gov.br/e-legis/. Access in: 16 Oct. 2008.
5. BRUCE, P.; MINKKINEN, P.; RIEKKOLA, M.L. Practical method validation sufcient for in analysis method. Mickrochimica Acta, v. 128, n. 1-2, p. 93-106, 1998.
6. CAVA, D. et al. Testing limonene difusion through food contact polyethylene by FT-IR spectroscopy: Film thickness, permeant concentration and outer medium efects. Polymer Testing, v. 24, n. 4, p. 483-489, 2005.
7. DZIECIOL, M.; TRZESZCZYNSKI, J. Volatile products of poly(ethylene terephthalate) thermal degradation in nitrogen atmosphere. Journal of Applied Polymer Science, v. 77, n. 9, p. 1894-1901, 2000.
8. DZIECIOL, M.; ZIECIOL, M.; TRZESZCZYNSKI, J. Studies of temperature infuence on volatile thermal degradation products of poly(ethylene terephthalate). Journal of Applied Polymer Science, v. 69, n. 12, p. 2377-2381, 1998.
9. EZQUERRO, O.; PONS, B.; TENA M. T. Multiple headspace solid-phase microextraction for the quantitative determinantion of volatile organic compounds in multilayer packagings. Journal of Chromatography A, v. 999, n. 1-2, p. 155-164, 2003.
10. FAYOUX, S. C.; SEUVRE, A.; VOILLEY, A. J. Aroma transfers in and through plastic packagings: orange juice and d-limonene: a review. Part I: orange juice aroma sorption. Packaging Technology and Science, v. 10, n. 2, p. 69-82, 1997.
11. FOOD AND AGRICULTURE ORGANIZATION OF THE UNITED NATIONS - FAO. Validation of analytical methods for food control. A report of a joint FAO/IAEA expert consultation 2-4 December 1997 Vienna, Austria. Rome: FAO, 1998. 19 p. Available from: fp://fp.fao.org/docrep/fao/007/w8420e/w8420e00.pdf. Access in: 16 Oct. 2008. Fao Food and Nutrition Paper 68.
12. FRANCO, M. R. B.; RODRIGUEZ, D. B.A. Trapping of soursop (Annona muricata) juice volatiles on porapak Q by suction. Journal of the Science of Food and Agriculture, v. 34, n. 3, p. 293-299, 1983.
13. FRANZ, R. Programme on the recyclability of food-packaging materials with respect to food safety considerations: polyethylene terephthalate (PET), paper and board, and plastics covered by functional barriers. Food Additives and Contaminants, v. 19, p. 93-110, 2002. Supplement.
14. FRANZ, R.; MAUER, A.; WELLE, F. European survey on post-consumer poly(ethylene terephthalate) (PET) materials to determine contamination levels and maximum consumer exposure from food packages made from recycled PET. Food Additives and Contaminants, v. 21, n. 3, p. 265-286, 2004.
15. FRANZ, R.; WELLE, F. Recycled poly (ethylene terephthalate) for direct food contact applications: challenge test of an inline recycling process. Food Additives and Contaminants, v. 19, n. 5, p. 502-511, 2002.
16. FREIRE, M. T. A. et al. Termal stability of polyethylene terephthalate food contact material: formation of volatiles from retail samples and implications for recycling. Food Additives and Contaminants, v. 1, n. 4, p. 473-480, 1998.
17. FREIRE, M. T. A.; REYES F. G.R. A importância do polietileno tereftalato (PET) na indústria de embalagens para alimentos. Boletim SBCTA, v. 31, n. 12, p. 129-136, 1997.
18. GARCÍA, R. S. et al. Revision of analytical strategies to evaluate diferent migrants from food packaging materials. Trends in Food Science & Technology, v. 17, n. 7, p. 354-366, 2006.
19. HAKKARAINEN, M.; GRONING, M.; ALBERTSSON, A. Solid-phase microextraction (SPME) in polymer characterization: long-term properties and quality control of polymeric materials. Journal of Applied Polymer Science, v. 89, n. 3, p. 867-873, 2003.
20. HUBER, L. Validation of analytical methods: review and strategy. LC/ GC International, v. 11, p. 96-105, 1998.
21. INTERNATIONAL LIFE SCIENCES INSTITUTE - ILSI EUROPE. Report on Packaging Materials 1: polyethylene terephathalate (PET) for food packaging applications. Brussels: ILSI Europe Packaging Material Task Force, 2000.
22. KALJURAND, M.; SMIT, H.C. Comparison of sample concentration methods and correlation chromatography for polymer dynamic head-space studies. Chromatographia, v. 39, n. 3-4, 210-215, 1994.
23. KONKOL, L. M. et al. Contaminants and levels of occurrence in washed and shredded poly (ethylene terephthalate) from curbide collection. Part 1: extraction conditions. Food Additives and Contaminants, v. 20, n. 9, p. 859-874, 2003.
24. KUZNESOF, P. M.; VANDERVEER, M. C. Recycled plastics for food-contact applications: science, policy and regulation. In: RADER, C. P. et al. (Eds.). Plastics, rubber and paper recycling: a pragmatic approach. Washington: American Chemical Society, 1995. p. 390-403.
25. LANÇAS, F. M. Cromatografa em fase gasosa. São Carlos: Acta Eventos, 1993. p. 240.
26. LEBOSSÉ, R.; DUCRUET, V.; FEIGENBAUM, A. Interactions between reactive aroma compounds from model citrus juice with polypropylene packaging flm. Journal of Agricultural and Food Chemistry, v. 45, n. 8, p. 2836-2842, 1997.
27. LIN, C.-E. et al. Migration behavior and selectivity of sulfonamides in capillary electrophoresis. Journal of Chromatography A, v. 792, n. 1-2, p. 37-47, 1997.
28. MILLER, J. C.; MILLER, J. N. Statistics for analytical chemistry. 3rd ed. New York: Ellis Horwood, 1993. 232 p.
29. NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY - NIST. Chemistry Webbook. NIST Standard Reference Database 69. 2005. Available from: http://webbook.nist.gov/chemistry/. Access in: 16 Oct. 2008.
30. NERÍN, C. et al. Evaluation of some screening methods for the analysis of contaminants in recycled polyethylene terephthalate fakes. Food Additives and Contaminants, v. 20, n. 7, p. 668-677, 2003.
31. NIELSEN, T.; DAMANT, A. P.; CASTLE, L. Validation studies of a quick test for predicting the sorption and washing properties of refllable plastic bottles. Food Additives and Contaminants, v. 14, n. 6-7, p. 685-693, 1997.
32. NONGONIERMA, A. et al. Mechanims of extraction of aroma compounds from foods, using adsorvents. Effect of various parameters. Food Reviews International, v. 22, n. 1, p. 51-94, 2006.
33. PAIK, J.S. Comparison of sorption in orange favor components by packaging flms using the headspace technique. Journal of Agricultural and Food Chemistry, v. 40, n. 10, p. 1822-1825, 1992.
34. PAWLISZYN, J. Solid phase microextraction: theory and practice. New York: Wiley-VHC, 1997. 245 p.
35. PIERCE, D. E.; KING, D. B.; SADLER, G. D. Analysis of contaminants in recycled poly(ethylene terephtalate) by thermal-extraction gas chromatography-mass spectroscopy. In: RADER, C. P. et al. (Eds.). Plastics, rubber and paper recycling: a pragmatic approach. Washington: American Chemical Society, 1995. p. 458-471.
36. REYNIER, A. et al. Stabilization of aroma compounds through sorption-release by packaging polymers. Journal of Agricultural and Food Chemistry, v. 52, n. 18, p. 5653-5662, 2004.
37. RIBANI, M. et al. Validação em métodos cromatográficos e eletroforéticos. Química Nova, v. 27, n. 5, p. 771-780, 2004.
38. SADLER, G. D. Recycling of polymers for food use: a current perspective. In: RADER, C. P. et al. (Eds.). Plastics, rubber and paper recycling: a pragmatic approach. Washington: American Chemical Society, 1995. p. 380-388.
39. Soto-Valdez H.; Gramshaw, J. W.; Vandengurg, H. J. Determination of potencial migrants present in Nylon 'microwave and roasting bags' and migration into olive oil. Food Additives and Contaminants, v. 14, n. 3, p. 309-318, 1997.
40. TRIANTAFYLLOU, V. et al. Studies on the usability of recycled PET for food packaging applications. European Food and Research Technology, v. 215, n. 3, p. 243-248, 2002.
41. US FOOD AND DRUG ADMINISTRATION - FDA. CFSAN/Ofce of Food Additive Safety. Guidance for industry. Use of recycled plastics in food packaging: chemistry considerations. Available from: http:// www.cfsan.fda.gov/~dms/opa2cg3b.html. Access in: 16 Oct. 2008.
42. Valente Soares, L.M. Como obter resultados confáveis em cromatografia. Revista do Instituto Adolfo Lutz, v. 60, n. 1, p. 79-84, 2001.
43. VAN WILLIGE, R. W. G. et al. Infuence of favour absorption by food-packaging materials (low-density polyethylene, polycarbonate and polyethylene terephthalate) on taste perception of a model solution and orange juice. Food Additives and Contaminants, v. 20, n. 1, p. 84-91, 2003.
44. VILLBERG, K.; VEIJANEN, A.; GUSTAFSSON, I. Identifcation of of-favour compounds in high-density polyethylene (HDPE) with diferent amounts of abscents. Polymer Engineering and Science, v. 38, n. 6, p. 922-925, 1998.
45. von Kovats E. Gas-chromatographische charakterisierung organischer verbindungen, Teil 1: retentions indices aliphatischer halogenide, alkohole, aldehyde und ketone. Helvetica Chimica Acta, v. 10, p. 1915-1932, 1958.
46. WEZL, T.; LANKMAYR, E. P. Comparative studies of the static and dynamic headspace extraction of saturated short chain aldehydes from cellulose-based packaging materials. Analytical and Bioanalytical Chemistry, v. 372, n. 5, p. 649-653, 2002.
47. WIDÉN, H.; LEUFVÉN, A.; NIELSEN, T. Identifcation of chemicals, possibly originating from misuse of refillable PET bottles, responsable for consumer complaints about of-odours in water and sof drinks. Food Additives and Contaminants, v. 22, n. 7, p. 681-692, 2005.
48. WIDÉN, H.; LEUFVÉN, A.; NIELSEN, T. Migration of model contaminants from PET bottles: influence of temperature, food stimulant and functional barrier. Food Additives and Contaminants, v. 21, p. 993-1006, 2004.
49. ZHANG, Z.; PAWLISZYN, J. Headspace solid-phase microextraction. Analytical Chemistry, v. 65, n. 14, p. 1843-1852, 1993.