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See Supporting Information for (further) experimental results and/or details
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See Supporting Information for (further) experimental results and/or details.
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Turnover frequency (TOF) is defined as mol of product per mol of catalyst per hour
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Turnover frequency (TOF) is defined as mol of product per mol of catalyst per hour.
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51
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79951828948
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note
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Similar hydrogenation using other protic solvents (MeOH, EtOH, i-PrOH, n-BuOH) were considerably slower requiring relatively long reaction times (>12ah) under analogous conditions.
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52
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For AH of simple ketones in toluene see.
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AH under analogous conditions using a toluene/(S)-1-phenylethanol 9:1 (v/v) mixture as solvent showed reduced activity (80% conv./2ah, 90% ee). The same inhibitory effect by product (S)-2 may lower TOF in toluene solvent at high conversions.
-
AH under analogous conditions using a toluene/(S)-1-phenylethanol 9:1 (v/v) mixture as solvent showed reduced activity (80% conv./2ah, 90% ee). The same inhibitory effect by product (S)-2 may lower TOF in toluene solvent at high conversions.
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