Development and optimization of an LC-MS/MS-based method for simultaneous quantification of vitamin D2, vitamin D3, 25-hydroxyvitamin D2 and 25-hydroxyvitamin D3

Journal of Separation Science

Volumn 34, Issue 1, 2011, Pages 11-20

  Adamec, Jiri ^a   Jannasch, Amber ^a   Huang, Jianjie ^a   Hohman, Emily ^a   Fleet, James C ^a   Peacock, Munro ^b   Ferruzzi, Mario G ^a   Martin, Berdine ^a   Weaver, Connie M ^a  

^a PURDUE UNIVERSITY   (United States)

^b INDIANA UNIVERSITY   (United States)

Author keywords

Cholecalciferol; Ergocalciferol; LC MS MS; Vitamin D

Indexed keywords

ACCURATE MEASUREMENT; ANALYTES; ATMOSPHERIC PRESSURE PHOTO IONIZATION; BIOLOGICAL SAMPLES; CHOLECALCIFEROL; ERGOCALCIFEROL; LC-MS METHODS; LC-MS/MS; LIQUID-LIQUID EXTRACTION; REVERSED PHASE; SIMULTANEOUS DETECTION; TECHNOLOGY STANDARDS; TRIPLE QUADRUPOLE; VITAMIN D;

ACETONE; ATMOSPHERIC IONIZATION; ATMOSPHERIC PRESSURE; HYDROXYLATION; LIQUIDS; MASS SPECTROMETRY; MOLECULES; OPTIMIZATION; SOLVENT EXTRACTION;

QUALITY CONTROL;

25 HYDROXYERGOCALCIFEROL; CALCIFEDIOL; COLECALCIFEROL; ERGOCALCIFEROL;

ACCURACY; ARTICLE; ATMOSPHERIC PRESSURE; HYDROXYLATION; IONIZATION; LIQUID CHROMATOGRAPHY; LIQUID LIQUID EXTRACTION; MASS SPECTROMETRY; PRIORITY JOURNAL; QUALITY CONTROL; QUANTITATIVE ANALYSIS; TANDEM MASS SPECTROMETRY; TECHNOLOGY; VALIDATION PROCESS;

25-HYDROXYVITAMIN D 2; CALCIFEDIOL; CHOLECALCIFEROL; CHROMATOGRAPHY, LIQUID; ERGOCALCIFEROLS; HUMANS; MOLECULAR STRUCTURE; REFERENCE STANDARDS; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; TANDEM MASS SPECTROMETRY;

EID: 78650425264     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.201000410     Document Type: Article

References (28)

1. Holick, M. F., Nutr. Rev. 2008, 66, S182-S194.
2. Jenab, M., Bueno-de-Mesquita, H. B., Ferrari, P., van Duijnhoven, F. J., Norat, T., Pischon, T., Jansen, E. H., Slimani, N., Byrnes, G., Rinaldi, S., Tjonneland, A., Olsen, A., Overvad, K., Boutron-Ruault, M. C., Clavel-Chapelon, F., Morois, S., Kaaks, R., Linseisen, J., Boeing, H., Bergmann, M. M., Trichopoulou, A., Misirli, G., Trichopoulos, D., Berrino, F., Vineis, P., Panico, S., Palli, D., Tumino, R., Ros, M. M., van Gils, C. H., Peeters, P. H., Brustad, M., Lund, E., Tormo, M. J., Ardanaz, E., Rodriguez, L., Sanchez, M. J., Dorronsoro, M., Gonzalez, C. A., Hallmans, G., Palmqvist, R., Roddam, A., Key, T. J., Khaw, K. T., Autier, P., Hainaut, P., Riboli, E., BMJ 2010, 340.
3. Carter, G. D., Clin. Chem. 2009, 55, 1300-1302.
4. Goltzman, D., Ann. N. Y. Acad. Sci. 2010, 1192, 145-152.
5. Binkley, N., Krueger, D., Cowgill, C. S., Plum, L., Lake, E., Hansen, K. E., DeLuca, H. F., Drezner, M. K., J. Clin. Endocrinol. Metab. 2004, 89, 3152-3157.
6. Hollis, B. W., J. Clin. Endocrinol. Metab. 2004, 89, 3149-3151.
7. Lensmeyer, G. L., Wiebe, D. A., Binkley, N., Drezner, M. K., Clin. Chem. 2006, 52, 1120-1126.
8. Blake, C. J., J. AOAC Int. 2007, 90, 897-910.
9. Byrdwell, W. C., Devries, J., Exler, J., Harnly, J. M., Holden, J. M., Holick, M. F., Hollis, B. W., Horst, R. L., Lada, M., Lemar, L. E., Patterson, K. Y., Philips, K. M., Tarrago-Trani, M. T., Wolf, W. R., Am. J. Clin. Nutr. 2008, 88, 554S-557S.
10. Yeung, B., Vouros, P., Siu-Caldera, M. L., Reddy, G. S., Biochem. Pharmacol. 1995, 49, 1099-1710.
11. Huang, M., LaLuzerne, P., Winters, D., Sullivan, D., J. AOAC Int. 2009, 92, 1327-1335.
12. Chen, H., McCoy, L. F., Schleicher, R. L., Pfeiffer, C. M., Clin. Chim. Acta 2008, 391, 6-12.
13. Maunsell, Z., Wright, D. J., Rainbow, S. J., Clin. Chem. 2005, 51, 1683-1690.
14. Saenger, A. K., Laha, T. J., Bremner, D. E., Sadrzadeh, S. M., Am. J. Clin. Pathol. 2006, 125, 914-920.
15. Singh, R. J., Taylor, R. L., Reddy, G. S., Grebe, S. K., J. Clin. Endocrinol. Metab. 2006, 91, 3055-3061.
16. Taylor, R. L., Grebe, S. K., Singh, R. J., Clin. Chem. 2005, 51, A231-A232.
17. Tsugawa, N., Suhara, Y., Kamao, M., Okano, T., Anal. Chem. 2005, 77, 3001-3007.
18. Vogeser, M., Kyriatsoulis, A., Huber, E., Kobold, U., Clin. Chem. 2004, 50, 1415-1417.
19. Duan, X., Weinstock-Guttman, B., Wang, H., Bang, E., Li, J., Ramanathan, M., Qu, J., Anal. Chem. 2010, 82, 2488-2497.
20. Eyles, D., Anderson, C., Ko, P., Jones, A., Thomas, A., Burne, T., Mortensen, P. B., Norgaad-Pedersen, B., Hougaard, D. M., McGrath, J., Clin. Chim. Acta 2009, 403, 145-151.
21. Phinney, K. W., Am. J. Clin. Nutr. 2008, 88, 511S-512S.
22. Dimartino, G., J. AOAC Int. 2009, 92, 511-517.
23. Knox, S., Harris, J., Calton, L., Wallace, A. M., Ann. Clin. Biochem. 2009, 46, 226-230.
24. Cai, S. S., Syage, J. A., Anal. Chem. 2006, 78, 1191-1199.
25. Cai, S. S., Syage, J. A., J. Chromatogr. A 2006, 1110, 15-26.
26. Nerin, C., Salafranca, J., Aznar, M., Batlle, R., Anal. Bioanal. Chem. 2009, 393, 809-833.
27. Higashi, T., Shibayama, Y., Fuji, M., Shimada, K., Anal. Bioanal. Chem. 2008, 391, 229-238.
28. Jiang, L., He, L., Fountoulakis, M., J. Chromatogr. A 2004, 1023, 317-320.