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Volumn 10, Issue 11, 2010, Pages 4689-4692

A novel ring-shaped phosphovanadomolybdate built by bicapped Pseudo-Keggin clusters and copper(II) complexes

Author keywords

[No Author keywords available]

Indexed keywords

BIPYRIDINES; COPPER COMPLEXES; DIAMINOPROPANE; ELEMENTAL ANALYSIS; HYDROGEN BONDING INTERACTIONS; HYDROTHERMALLY SYNTHESIZED; ORGANIC-INORGANIC HYBRID; SINGLE CRYSTAL X-RAY DIFFRACTION; SUPRAMOLECULAR STRUCTURE; X-RAY POWDER;

EID: 78149343223     PISSN: 15287483     EISSN: 15287505     Source Type: Journal    
DOI: 10.1021/cg100864m     Document Type: Conference Paper
Times cited : (17)

References (59)
  • 50
    • 78149346013 scopus 로고    scopus 로고
    • 4 (0.5 mL, 50%), and distilled water (12 mL) at pH 7.0 was stirred for 20 min. The mixture was then transferred to a Teflon-lined stainless steel autoclave (30 mL) and kept at 170 °C for 6 days. After being slowly cooled to room temperature, block-shaped black crystals (Figure S17) were isolated (42% based on Mo) and then washed with distilled water and air-dried at room temperature. Elemental analysis (%). Calcd: C, 12.76; H, 2.79; N, 7.44. Found: C, 12.88; H, 2.67; N, 7.31
    • 4 (0.5 mL, 50%), and distilled water (12 mL) at pH 7.0 was stirred for 20 min. The mixture was then transferred to a Teflon-lined stainless steel autoclave (30 mL) and kept at 170 °C for 6 days. After being slowly cooled to room temperature, block-shaped black crystals (Figure S17) were isolated (42% based on Mo) and then washed with distilled water and air-dried at room temperature. Elemental analysis (%). Calcd: C, 12.76; H, 2.79; N, 7.44. Found: C, 12.88; H, 2.67; N, 7.31.
  • 52
    • 78149301553 scopus 로고    scopus 로고
    • 2) = 0.0891(0.2062) [ I > 2σ(I)]. Intensity data of 1 were collected on a Bruker CCD Apex-II diffractometer using graphite-monochromated Mo Kα radiation (λ = 0.71073 Å), respectively. Routine Lorentz and polarization corrections were applied, and an absorption correction was performed using the SADABS program
    • 2 using the SHELXTL-97 program package. (12) All non-hydrogen atoms were refined anisotropically. CCDC 782335 for 1 contains the crystallographic data for this paper.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.