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Volumn , Issue 12, 2002, Pages 1238-1239

[{(H2O)Ni(enMe)2 MoV4MoVI4VIV 8(VVO4)O40}2{Ni(enMe) 2}][Ni(enMe)2]4·8H2O: The first dimer of polyoxometalates linked through coordination fragment

Author keywords

[No Author keywords available]

Indexed keywords

CHEMICAL COMPOUND; COORDINATION COMPOUND; DIMER; POLYANION; POLYOXOMETALATE; PROPANE; TRANSITION ELEMENT; UNCLASSIFIED DRUG;

EID: 0037028347     PISSN: 03667022     EISSN: None     Source Type: Journal    
DOI: 10.1246/cl.2002.1238     Document Type: Article
Times cited : (12)

References (10)
  • 8
    • 0012971556 scopus 로고    scopus 로고
    • note
    • -1, Mo Kα radiation, λ = 0.71073 ////. A black block crystal with dimensions of 0.28 × 0.20 × 0.16 mm was mounted on a glass fiber. Data collection was performed on a Bruker Smart CCD diffractometer at 298 K in the range of 1.67 < θ < 25.05 using ω and φ scan. A total of 26009 data were collected and were merged to give 12422 unique reflections of which 7777 were considered to be observed [I > 2σ(I)]. The structure was solved by direct methods and refined using SHELXL 97 software. All the non-hydrogen atoms except C(21) were refined anisotropically. Final R values (R = 0.0780, wR = 0.1303, and S = 1.083) were obtained for 7777 reflections with I > 2σ(I) and a total 937 of parameters. Atomic coordinates, bond lengths and angles, and the terminal parameters have been deposited at the Cambridge Crystallographic Data Center (CCDC 189963).


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.