Characterization and optimization by experimental design of a liquid chromatographic method for the separation of hydroxylated polychlorinated biphenyls on a polar-embedded stationary phase

Journal of Chromatography A

Volumn 1217, Issue 46, 2010, Pages 7231-7241

  Quintanilla López, Jesús Eduardo ^a   Galindo Iranzo, Plácido ^b   Gómara, Belén ^a   Lebrón Aguilar, Rosa ^a  

^a INSTITUTO DE QUÍMICA ORGÁNICA GENERAL   (Spain)

^b INSTITUTO DE QUÍMICA FÍSICA ROCASOLANO   (Spain)

Author keywords

Experimental design; Hydroxylated polychlorinated biphenyls; Liquid chromatography; Polar embedded stationary phases; Retention modeling

Indexed keywords

ANALYSIS TIME; CENTRAL COMPOSITE; CHROMATOGRAPHIC METHODS; DERIVATIZATIONS; DISPERSION FORCE; EXPERIMENTAL DESIGN; EXPERIMENTAL PARAMETERS; GLOBAL OPTIMUM; GRADIENT TIME; HYDROGEN BONDINGS; HYDROXYLATED POLYCHLORINATED BIPHENYLS; ISOBARIC COMPOUNDS; METHANOL CONTENT; MOBILE PHASE; OCTADECYLSILANE; OH-PCBS; PH VALUE; RESPONSE SURFACE METHODOLOGY; RETENTION MODELING; SEPARATION PROCESS; STATIONARY PHASE; STATIONARY PHASIS;

AMIDES; CHROMATOGRAPHIC ANALYSIS; DESIGN; GAS CHROMATOGRAPHY; HYDROGEN; HYDROGEN BONDS; HYDROXYLATION; LIQUIDS; METHANOL; OPTIMIZATION; PH EFFECTS; POLYCHLORINATED BIPHENYLS; STATISTICS;

LIQUID CHROMATOGRAPHY;

AMIDE; BUFFER; METHANOL; OCTADECYLSILANE; POLYCHLORINATED BIPHENYL; SILANE DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL ANALYSIS; CHEMICAL INTERACTION; CONCENTRATION (PARAMETERS); CONTROLLED STUDY; DISPERSION; ELUTION; EXPERIMENTAL DESIGN; HYDROGEN BOND; HYDROXYLATION; LIQUID CHROMATOGRAPHY; PH; PRIORITY JOURNAL; PROCESS OPTIMIZATION; RESPONSE SURFACE METHOD; SENSITIVITY AND SPECIFICITY;

CHROMATOGRAPHY, LIQUID; HYDROGEN BONDING; HYDROGEN-ION CONCENTRATION; HYDROXYLATION; METHANOL; MODELS, CHEMICAL; POLYCHLORINATED BIPHENYLS; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; TIME FACTORS;

EID: 77958093423     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2010.09.032     Document Type: Article

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