Electrochemical surface structuring with palladium nanoparticles for signal enhancement

Langmuir

Volumn 26, Issue 14, 2010, Pages 12293-12299

  Soreta, Tesfaye Refera ^a   Strutwolf, Jörg ^a,c   Henry, Olivier ^a   O'Sullivan, Ciara K ^a,b  

^a UNIVERSITAT ROVIRA I VIRGILI   (Spain)

^b INSTITUCIÓ CATALANA DE RECERCA I ESTUDIS AVANÇATS ICREA   (Spain)

^c UNIVERSITY COLLEGE CORK   (Ireland)

Author keywords

[No Author keywords available]

Indexed keywords

ANODIC PEAKS; ELECTROACTIVE; ELECTROCHEMICAL DEPOSITION; ELECTROCHEMICAL SURFACES; GC ELECTRODE; GLASSY CARBON ELECTRODES; GOLD NPS; METAL NANOPARTICLES; NANO SCALE; NANOSTRUCTURED SURFACE; NARROW SIZE DISTRIBUTIONS; NUMBER DENSITY; PALLADIUM ELECTRODES; PALLADIUM NANOPARTICLES; PHYSICOCHEMICAL PROPERTY; SECONDARY NUCLEATION; SEM; SEM IMAGE ANALYSIS; SENSOR SIGNALS; SEQUENTIAL DEPOSITION; SIGNAL ENHANCEMENT; SPATIAL DISTRIBUTION; SURFACE NANOSTRUCTURING; TRANSDUCER SURFACE;

ELECTRODES; GLASS MEMBRANE ELECTRODES; GLASSY CARBON; GOLD COATINGS; GOLD DEPOSITS; IMAGE ANALYSIS; NANOPARTICLES; NANOSTRUCTURED MATERIALS; REDUCTION; SCANNING ELECTRON MICROSCOPY; SIZE DISTRIBUTION;

PALLADIUM;

CARBON; GLASS; METAL NANOPARTICLE; PALLADIUM;

ARTICLE; CHEMISTRY; ELECTROCHEMISTRY; ELECTRODE; PARTICLE SIZE; SCANNING ELECTRON MICROSCOPY; SURFACE PROPERTY;

CARBON; ELECTROCHEMISTRY; ELECTRODES; GLASS; METAL NANOPARTICLES; MICROSCOPY, ELECTRON, SCANNING; PALLADIUM; PARTICLE SIZE; SURFACE PROPERTIES;

EID: 77956686256     PISSN: 07437463     EISSN: 15205827     Source Type: Journal    
DOI: 10.1021/la101398g     Document Type: Article

References (61)

1. Kenneth J. Klabunde, R. S. M. Chemical and Catalytic Aspects of Nanocrystals. In Nanoscale Materials in Chemistry; Klabunde, K. J., Ed.; John Wiley: New York, 2001; pp 238-239.
2. Durand, J.; Teuma, E.; Gomez, M. An overview of palladium nanocatalysts: Surface and molecular reactivity. Eur. J. Inorg. Chem. 2008, 3577-3586.
3. Roduner, E. Size matters: Why nanomaterials are different. Chem. Soc. Rev. 2006, 35, 583-592.
4. Arvia, A. J.; Salvarezza, R. C.; Triaca, W. E. Noble metal surfaces and electrocatalysis. Review and perspectives. J. New Mater. Electrochem. Syst. 2004, 7, 133-143.
5. Aiken, J. D.; Finke, R. G. Areview of modern transition-metal nanoclusters: Their synthesis, characterization, and applications in catalysis. J. Mol. Catal A: Chem. 1999, 145, 1-44.
6. El-Deab, M. S.; Okajima, T.; Ohsaka, T. Fabrication of phase-separated multicomponent self-assembled monolayers at gold nanoparticles electrodeposited on glassy carbon electrodes. J. Electrochem. Soc. 2006, 153, E201-E206.
7. Su, L.; Mao, L. Gold nanoparticle/alkanedithiol conductive films selfassembled onto gold electrode: Electrochemistry and electroanalytical application for voltammetric determination of trace amount of catechol. Talanta 2006, 70 68-74.
8. Klabunde, K. J. Introduction to Nanotechnology. In Nanoscale Materials in Chemistry; Klabunde, K. J., Ed.; John Wiley and Sons: New York, 2001; p 7.
9. Paunovic, M.; Schlesinger, M. Fundamentals of Electrochemical Deposition, 2nd ed.; John Wiley & Sons: Hoboken, NJ, 2006.
10. Gorer, S.; Liu, H.; Stiger, R. M.; Zach, M. P.; Zoval, J. V.; Penner, R. M. Electrodeposition of Metal Nanoparticles on Graphite and Silicon. In Metal Nanoparticles: Synthesis, Characterization, and Applications; Feldheim, D. L., Foss, C. A., Jr., Eds.; Marcel Dekker: New York, 2002; pp 237-259.
11. Milchev, A.; Zapryanova, T. Nucleation and growth of copper under combined charge transfer and diffusion limitations - part II. Electrochim. Acta 2006, 51, 4916-4921. (Pubitemid 43765920)
12. Zoval, J. V.; Lee, J.; Gorer, S.; Penner, R. M. Electrochemical preparation of platinum nanocrystallites with size selectivity on basal plane oriented graphite surfaces. J. Phys. Chem. B 1998, 102, 1166-1175.
13. Zoval, J. V.; Stiger, R. M.; Biernacki, P. R.; Penner, R. M. Electrochemical deposition of silver nanocrystallites on the atomically smooth graphite basal plane. J. Phys. Chem. 1996, 100 (2), 837-844.
14. Penner, R. M. Metal Deposition; Elsevier: Amsterdam, 2007; pp 661-709.
15. Giersig, M.; Mulvaney, P., Preparation of ordered colloid monolayers by electrophoretic deposition. Langmuir 1993, 9, 3408-3413.
16. Teranishi, T.; Hosoe, M.; Miyake, M. Formation of monodispersed ultrafine platinum particles and their electrophoretic deposition on electrodes. Adv. Mater. 1997, 9 (1), 65-67.
17. Rozenberg, B. A.; Tenne, R. Polymer-assisted fabrication of nanoparticles and nanocomposites. Prog. Polym. Sci. 2008, 33, 40-112.
18. Katz, E.; Willner, I.; Wang, J. Electroanalytical and bioelectroanalytical systems based on metal and semiconductor nanoparticles. Electroanalysis 2004, 16, 19-44.
19. Sadik, O. A.; Aluoch, A. O.; Zhou, A. Status of biomolecular recognition using electrochemical techniques. Biosens. Bioelectron. 2009, 24, 2749-2765.
20. Luo, X.; Morrin, A.; Killard, A. J.; Smyth, M. R. Application of nanoparticles in electrochemical sensors and biosensors. Electroanalysis 2006, 18, 319-326.
21. El-Deab, M. S.; Sotomura, T.; Ohsaka, T. Oxygen reduction at Au nanoparticles electrodeposited on different carbon substrates. Electrochim. Acta 2006, 52, 1792-1798. (Pubitemid 44791295)
22. Zhang, Y.; Asahina, S.; Yoshihara, S.; Shirakashi, T. Oxygen reduction on Au nanoparticle deposited boron-doped diamond films. Electrochim. Acta 2003, 48, 741-747.
23. Rajalakshmi, N.; Dhathathreyan, K. S. Nanostructured platinum catalyst layer prepared by pulsed electrodeposition for use in PEM fuel cells. Int. J. Hydrogen Energy 2008, 33, 5672-5677.
24. Wei, Z. D.; Chan, S. H.; Li, L. L.; Cai, H. F.; Xia, Z. T.; Sun, C. X. Electrodepositing Pt on a Nafion-bonded carbon electrode as a catalyzed electrode for oxygen reduction reaction. Electrochim. Acta 2005, 50, 2279-2287.
25. Diculescu, V. C.; Chiorcea-Paquim, A. M.; Corduneanu, O.; Oliveira- Brett, A. M. Palladium nanoparticles and nanowires deposited electrochemically: AFM and electrochemical characterization. J. Solid State Electrochem. 2007, 11, 887-898.
26. Gimeno, Y.; Creus, A. H.; Carro, P.; Gonzalez, S.; Salvarezza, R. C.; Arvia, A. J. Electrochemical formation of palladium islands on HOPG: Kinetics, morphology, and growth mechanisms. J. Phys. Chem. B 2002, 106, 4232-4244.
27. Soreta, T. R.; Strutwolf, J.; O'Sullivan, C. K. Electrochemically deposited palladium as a substrate for self-assembled monolayers. Langmuir 2007, 23, 10823-10830.
28. Liu, H.; Favier, F.; Ng, K.; Zach, M. P.; Penner, R. M. Size-selective electrodeposition of meso-scale metal particles: a general method. Electrochim. Acta 2001, 47, 671-677.
29. Penner, R. M. Mesoscopic Metal particles and wires by electrodeposition. J. Phys. Chem. B 2002, 106, 3339-3353.
30. Walter, E. C.; Murray, B. J.; Favier, F.; Kaltenpoth, G.; Grunze, M.; Penner, R. M. Noble and coinage metal nanowires by electrochemical step edge decoration. J. Phys. Chem. B 2002, 106, 11407-11411.
31. Lubert, K.-H.; Guttmann, M.; Beyer, L. Electrode reactions and accumulation of hydrogen at carbon paste electrodes in the presence of tetrachloropalladate. J. Electroanal. Chem. 1999, 462, 174-180.
32. Lubert, K.-H.; Guttmann, M.; Beyer, L.; Kalcher, K. Experimental indications for the existence of different states of palladium(0) at the surface of carbon paste electrodes. Electrochem. Commun. 2001, 3, 102-106.
33. Li, F.; Zhang, B.; Dong, S.; Wang, E. A novel method of electrodepositing highly dispersed nano palladium particles on glassy carbon electrode. Electrochim. Acta 1997, 42, 2563-2568.
34. Batchelor-McAuley, C. ; Banks, C. E.; Simm, A. O.; Jones, T. G. J.; Compton, R. G. Nano-electrochemical detection of hydrogen or protons using palladiumnanoparticles: distinguishing surface and bulk hydrogen. ChemPhysChem 2006, 7, 1081-1085.
35. Fournée, V.; Barrow, J. A.; Shimoda, M.; Ross, A. R.; Lograsso, T. A.; Thiel, P. A.; Tsai, A. P. Palladium clusters formed on the complex pseudo-10-fold surface of the [xi]'-Al77.5Pd19Mn3.5 approximant crystal. Surf. Sci. 2003, 541, 147-159.
36. Ji, X.; Banks, C. E.; Xi, W.; Wilkins, S. J.; Compton, R. G. Edge plane sites on highly ordered pyrolytic graphite as templates for making palladium nanowires via electrochemical decoration. J. Phys. Chem. B 2006, 110, 22306-22309.
37. Atashbar,M. Z.; Banerji, D.; Singamaneni, S.; Bliznyuk, V. Deposition of parallel arrays of palladium nanowires and electrical characterization using microelectrode contacts. Nanotechnology 2004, 15, 374-378.
38. Gimeno, Y.; Hernandez Creus, A.; Gonzalez, S.; Salvarezza, R. C.; Arvia, A. J. Preparation of 100-160-nm-sized branched palladium islands with enhanced electrocatalytic properties on HOPG. Chem. Mater. 2001, 13, 1857-1864.
39. Gao, G.-Y.; Guo, D.-J.; Li, H.-L. Electrocatalytic oxidation of formaldehyde on palladium nanoparticles supported on multi-walled carbon nanotubes. J. Power Sources 2006, 162, 1094-1098.
40. Safavi, A.; Maleki, N.; Farjami, F.; Farjami, E. Electrocatalytic oxidation of formaldehyde on palladium nanoparticles electrodeposited on carbon ionic liquid composite electrode. J. Electroanal. Chem. 2009, 626, 75-79.
41. Teschner, D.; Vass, E.; Hävecker, M.; Zafeiratos, S.; Schnörch, P.; Sauer, H.; Knop-Gericke, A.; Schlögl, R.; Chamam, M.; Wootsch, A.; Canning, A. S.; Gamman, J. J.; Jackson, S. D.; McGregor, J.; Gladden, L. F. Alkyne hydrogenation over Pd catalysts: A new paradigm. J. Catal. 2006, 242, 26-37.
42. Trapp, O.; Weber, S. K.; Bauch, S.; Backer, T.; Hofstadt, W.; Spliethoff, B. High-throughput kinetic study of hydrogenation over palladium nanoparticles: Combination of reaction and analysis. Chem.;Eur. J. 2008, 14, 4657-4666.
43. Mukherjee, D. Potential application of palladium nanoparticles as selective recyclable hydrogenation catalysts. J. Nanopart. Res. 2008, 10, 429-436.
44. Yang C.-C.; Senthil Kumar, A.; Zen, J. M. Electrocatalytic reduction and determination of dissolved oxygen at a preanodized screen-printed carbon electrode modified with palladium nanoparticles. Electroanalysis 2006, 18, 64-69.
45. Chen, J.; Zhang, Q.; Wang, Y.; Wan, H. Size-dependent catalytic activity of supported palladium nanoparticles for aerobic oxidation of alcohols. Adv. Synth. Catal. 2008, 350, 453-464.
46. Bianchi, C. L.; Canton, P.; Dimitratos, N.; Porta, F.; Prati, L. Selective oxidation of glycerol with oxygen using mono and bimetallic catalysts based on Au, Pd and Pt metals. Catal. Today 2005, 102-103, 203-212.
47. Choudhary, V. R.; Samanta, C. Role of chloride or bromide anions and protons for promoting the selective oxidation of H2 by O2 to H2O2 over supported Pd catalysts in an aqueous medium. J. Catal. 2006, 238, 28-38.
48. Nishihata, Y.; Mizuki, J.; Akao, T.; Tanaka, H.; Uenishi, M.; Kimura, M.; Okamoto, T.; Hamada, N. Self-regeneration of a Pd-perovskite catalyst for automotive emissions control. Nature 2002, 418, 164-167.
49. Santhosh, P.; Manesh, K. M.; Uthayakumar, S.; Komathi, S.; Gopalan, A. I.; Lee, K. P. Fabrication of enzymatic glucose biosensor based on palladium nanoparticles dispersed onto poly(3,4-ethylenedioxythiophene) nanofibers. Bioelectrochemistry 2009, 75, 61-66.
50. Thiagarajan, S.; Yang, R.-F.; Chen, S.-M. Palladium nanoparticles modified electrode for the selective detection of catecholamine neurotransmitters in presence of ascorbic acid. Bioelectrochemistry 2009, 75, 163-169.
51. Chang, Z.; Pan, H.; Zhao, K.; Chen, M.; He, P. G.; Fang, Y. Z. Electrochemical DNA biosensors based on palladium nanoparticles combined with carbon nanotubes. Electroanalysis 2008, 20, 131-136.
52. Hammer, B.; Nørskov, J. K.; Bruce, C. G. a. H. K. Theoretical Surface Science and Catalysis: Calculations and Concepts. In Advances in Catalysis; Academic Press: San Diego, CA, 2000; Vol.45, pp 71-129.
53. Sánchez, C. G.; Leiva, E. P. M.; Schmickler, W. On the catalytic activity of palladium clusters generated with the electrochemical scanning tunnelling microscope. Electrochem. Commun. 2003, 5, 584-586.
54. Corthey, G. n.; Rubert, A. A.; Benitez,G. A.; Fonticelli, M. H.; Salvarezza, R. C. Electrochemical and X-ray photoelectron spectroscopy characterization of alkanethiols adsorbed on palladium surfaces. J. Phys. Chem. C 2009, 113, 6735-6742.
55. Carvalho, A.; Geissler, M.; Schmid, H.; Michel, B.; Delamarche, E. Selfassembled monolayers of eicosanethiol on palladium and their use in microcontact printing. Langmuir 2002, 18, 2406-2412.
56. Love, J. C.; Wolfe, D. B.; Chabinyc, M. L.; Paul, K. E.; Whitesides, G. M. Self-assembled monolayers of alkanethiolates on palladium are good etch resists. J. Am. Chem. Soc. 2002, 124, 1576-1577.
57. Soreta, T. R.; Strutwolf, J.; O'Sullivan, C. K., Electrochemical fabrication of nanostructured surfaces for enhanced response. ChemPhysChem 2008, 9, 920-927.
58. Rasband, W. S. ImageJ. http://rsb.info.nih.gov/ij/
59. A.J. Bard, L. R. F. Electrochemical Methods: Fundamentals and Applications, 2nd ed.; John Wiley & Sons: New York, 2001.
60. Rand, D. A. J.; Woods, R. Determination of surface composition of smooth noble-metal alloys by cyclic voltammetry. J. Electroanal. Chem. 1972, 36 (1), 57-69.
61. Bartlett, P. N.; Gollas, B.; Guerin, S.; Marwan, J. The preparation and characterisation of H-1-e palladium films with a regular hexagonal nanostructure formed by electrochemical deposition from lyotropic liquid crystalline phases. Phys. Chem. Chem. Phys. 2002, 4, 3835-3842