Evaluation of two sample treatment methodologies for large-scale pesticide residue analysis in olive oil by fast liquid chromatography-electrospray mass spectrometry

Journal of Chromatography A

Volumn 1217, Issue 24, 2010, Pages 3736-3747

  Gilbert López, Bienvenida ^a   García Reyes, Juan F ^a   Fernández Alba, Amadeo R ^b   Molina Díaz, Antonio ^a  

^a UNIVERSITY OF JAÉN   (Spain)

^b UNIVERSITY OF ALMERÍA   (Spain)

Author keywords

Liquid chromatography; Mass spectrometry; Matrix solid phase dispersion; Olive oil; Pesticides; QuEChERS; Sample treatment

Indexed keywords

AMINOPROPYL; ANALYTES; COMPREHENSIVE EVALUATION; DISPERSIVE SOLID PHASE EXTRACTION; ELECTROSPRAY MASS SPECTROMETRY; ELECTROSPRAYS; FLORISIL; GRAPHITIZED CARBON BLACK; LARGE-SCALE MULTI-RESIDUE METHOD; LC-MS METHODS; LIMITS OF DETECTION; LIQUID CHROMATOGRAPHY-MASS SPECTROMETRY; LIQUID PARTITIONING; LIQUID-LIQUIDS; MATRIX EFFECTS; MATRIX SOLID-PHASE DISPERSION; MULTI-CLASS; OLIVE OIL; PESTICIDE RESIDUE ANALYSIS; PETROLEUM ETHER; PHYSICOCHEMICAL PROPERTY; RECOVERY RATE; SAMPLE TREATMENT; SECONDARY AMINES; SIGNAL SUPPRESSION; SOLVENT CONSUMPTION; SORBENT MATERIALS; TARGET SPECIES; TIME OF FLIGHT MASS SPECTROMETRY; TRACE AMOUNTS; WASTE GENERATION;

ABILITY TESTING; ACETONITRILE; AGRICULTURAL CHEMICALS; BUBBLES (IN FLUIDS); CARBON BLACK; CHROMATOGRAPHY; DISPERSIONS; ETHERS; HIGH PRESSURE LIQUID CHROMATOGRAPHY; LIQUIDS; MASS SPECTROMETRY; PESTICIDES; PROJECTILES; RECOVERY; SORPTION; VEGETABLE OILS; WASTE TREATMENT;

EXTRACTION;

ACETONITRILE; OLIVE OIL; PESTICIDE;

ANALYTIC METHOD; ARTICLE; CHEMICAL ANALYSIS; CONTROLLED STUDY; ELECTROSPRAY MASS SPECTROMETRY; INTERMETHOD COMPARISON; LARGE SCALE PRODUCTION; LIQUID LIQUID EXTRACTION; PHYSICAL CHEMISTRY; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; REACTION TIME; RESIDUE ANALYSIS; SENSITIVITY ANALYSIS; SOLID PHASE EXTRACTION; TIME OF FLIGHT MASS SPECTROMETRY; ULTRA PERFORMANCE LIQUID CHROMATOGRAPHY; VALIDATION PROCESS;

CHROMATOGRAPHY, LIQUID; LINEAR MODELS; PESTICIDE RESIDUES; PLANT OILS; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SOLID PHASE EXTRACTION; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION;

EID: 77953579987     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2010.04.025     Document Type: Article

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