Optimization of the GC method for routine analysis of the fatty acid profile in several food samples

Food Chemistry

Volumn 122, Issue 1, 2010, Pages 285-291

  Petrović, Marinko ^a   Kezić, Nataša ^a   Bolanča, Vesna ^a  

^a UNIVERSITY OF ZAGREB   (Croatia)

Author keywords

Fatty acids; Gas chromatography (GC); Method optimization

Indexed keywords

FATTY ACID; POTASSIUM HYDROXIDE; TRIACYLGLYCEROL;

ARTICLE; FATTY ACID ANALYSIS; FOOD ANALYSIS; GAS CHROMATOGRAPHY; QUANTITATIVE ANALYSIS; SOXHLET EXTRACTION; TRANSESTERIFICATION;

EID: 77950593460     PISSN: 03088146     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.foodchem.2010.02.018     Document Type: Article

References (26)

1. AOAC. Official method 996.06 official methods of analysis of AOAC. 17th ed. (2000), AOAC International Press, Gaithersburg, Maryland, USA
2. Aparicio R., and Aparicio-Ruiz R. Authentication of vegetable oils by chromatographic techniques. Journal of Chromatographic Science 881 (2000) 93-104
3. Bell J.G., Tocher D.R., Farndele B.M., Cox D.I., McKinnley R.W., and Sargent J.R. The effects of dietary lipids on polyunsaturated fatty acid metabolism in Atlantic salmon undergoing parr-smolt transformation. Lipids 32 (1997) 515-525
4. Chapkin, R. S. (2000). Reappraisal of essential fatty acids. In C.K. Chow (Ed.), Fatty acid in foods and their health implications (2nd ed.). New York: Marcel Dekker.
5. Chow C.K. Fatty acid in foods and their health implications. 2nd ed. (2000), Marcel Dekker, New York
6. Dayhuff L.-E., and Wells M.J.M. Identification of fatty acids in fishes collected from the Ohio River using gas chromatography-mass spectrometry in chemical ionization and electron impact modes. Journal of Chromatography, A 1098 (2005) 144-149
7. de Geus H.-J., Aidos I., de Boer J., Luten J.B., and Brinkman U.A.Th. Characterization of fatty acids in biological oil samples using comprehensive multidimensional gas chromatography. Journal of Chromatography, A 910 (2001) 95-103
8. European Pharmacopoeia. (2005). 2.4.22, EDQM (5th ed., Vol. 1). Strasbourg, France: Council of Europe.
9. Hajimahmoodi M., Vander Hayden Y., Sadeghi N., Jannat B., Oveisi M.R., and Shahbazian S. Gas-chromatographic fatty-acid fingerprints and partial least squares modeling as a basis for the simultaneous determination of edible oil mixtures. Talanta 66 (2005) 1108-1116
10. Huang Z., Wang B., and Crenshow A.A. A simple method for the analysis of trans fatty acid with GC-MS and AT-Silar-90 capillary column. Food Chemistry 98 (2006) 593-598
11. ICH. (1996). Validation of analytical procedures: methodology, harmonized tripartite guideline, topic Q2B. UK.
12. ISO 1443. (1973). Meat and meat products - Determination of total fat content.
13. ISO 5508. (1999). Animal and vegetable fats and oils - Analysis by gas chromatography of methyl esters of fatty acids.
14. ISO 5509. (2000). Animal and vegetable fats and oils - Preparation of methyl esters of fatty acids.
15. Jalali-Heravi M., and Vosough M. Characterization and determination of fatty acids in fish oil using gas chromatography-mass spectrometry coupled with chemometric resolution techniques. Journal of Chromatography, A 1024 (2004) 165-176
16. Kritchevsky, D. (2002). Fats and oils in human health. In C. C. Akoh, D. B. Min (Eds.), Food lipids: Chemistry, nutrition and biotechnology (2nd ed.). New York: Marcel Dekker.
17. Lehotay S.J., and Hajšlova J. Application of gas chromatography in food analysis. Trends in Analytical Chemistry 21 (2002) 686-697
18. Maduko C.O., and Park Y.W. Modification of fatty acid and sterol composition of caprine milk for use as infant formula. International Diary Journal 17 (2007) 1434-1440
19. McKenzie D.J. Effects of dietary fatty acids on respiratory and cardiovascular physiology of fish. Comparative Biochemistry and Physiology, A: Comparative Physiology 128 (2001) 607-621
20. Mendez Antolin E., Marrero Delange D., and Gonzalez Canavaciolo V. Evaluation of five methods for derivatization and GC determination of a mixture of very long chain fatty acids. Journal of Pharmaceutical and Biomedical Analysis 46 (2008) 194-199
21. Mondello L., Tranchida P.Q., Dugo P., and Dugo G. Rapid, microscale preparation and very fast gas chromatographic separation of cod liver oil fatty acid methyl esters. Journal of Pharmaceutical and Biomedical Analysis 41 (2006) 1566-1570
22. O'Keefe, S. F. (2002). Nomenclature and classification of lipids. In C. C. Akoh, D. B. Min (Eds.), Food lipids: chemistry, nutrition and biotechnology (2nd ed.). New York: Marcel Dekker.
23. Ramadan M.F., Sharanabasappa G., Seetharam Y.N., Seshagiri M., and Moersel J.-T. Characterization of fatty acids and bioactive compounds of kachnar (Bauhinia purpurea L.) seed oil. Food Chemistry 98 (2006) 359-365
24. Seppanen-Laakso T., Laakso I., and Hiltunen R. Analysis of fatty acids by gas chromatography, and its relevance to research on health and nutrition. Analytica Chimica Acta 465 (2002) 39-62
25. Stransky K., Zarevucka M., and Wimmer Z. Gas chromatography analysis of blackcurrant oil in relation to its stability. Food Chemistry 92 (2005) 569-573
26. Vijver L.P.L., Kardinaal A.F.M., Couet C., Aro A., Kafatos A., and Steingrimsdottir L. Association between trans fatty acid intake and cardiovascular risk factors in Europe: The Transfair study. European Journal of Clinical Nutrition 54 (2000) 126-135