메뉴 건너뛰기




Volumn 74, Issue 2, 2010, Pages 377-387

Investigation into the intragranular structures of microcrystalline cellulose and pre-gelatinised starch

Author keywords

Atomic force microscopy (AFM); Granule structure; Microcrystalline cellulose (MCC); Nitrogen adsorption; Scanning electron microscopy (SEM); Small angle X ray scattering (SAXS); Starch 1500, pre gelatinised starch (PGS); Transmission electron microscopy (TEM); Wide angle X ray scattering (WAXS)

Indexed keywords

CELPHERE; MICROCRYSTALLINE CELLULOSE; NITROGEN; STARCH; STARCH 1500; UNCLASSIFIED DRUG;

EID: 75449094811     PISSN: 09396411     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.ejpb.2009.10.006     Document Type: Article
Times cited : (21)

References (53)
  • 3
    • 58349117904 scopus 로고    scopus 로고
    • The effect of processing parameters on pharmaceutical tablet properties
    • Sinka I.C., Motazedian F., Cocks A.C.F., and Pitt K.G. The effect of processing parameters on pharmaceutical tablet properties. Powder Technol. 189 (2009) 276-284
    • (2009) Powder Technol. , vol.189 , pp. 276-284
    • Sinka, I.C.1    Motazedian, F.2    Cocks, A.C.F.3    Pitt, K.G.4
  • 5
    • 0029375899 scopus 로고
    • On the cold compaction of powders
    • Fleck N.A. On the cold compaction of powders. J. Mech. Phys. Solids 43 (1995) 1409-1431
    • (1995) J. Mech. Phys. Solids , vol.43 , pp. 1409-1431
    • Fleck, N.A.1
  • 6
    • 34248192774 scopus 로고    scopus 로고
    • Local contact compliance relations at compaction of composite powders
    • Skrinjar O., Larsson P.-L., and Storåkers B. Local contact compliance relations at compaction of composite powders. J. Appl. Mech. 74 (2007) 164-168
    • (2007) J. Appl. Mech. , vol.74 , pp. 164-168
    • Skrinjar, O.1    Larsson, P.-L.2    Storåkers, B.3
  • 7
    • 0001559087 scopus 로고
    • Über die Berührung fester elastischer Körper (Concerning the contact of solid elastic bodies)
    • Hertz H. Über die Berührung fester elastischer Körper (Concerning the contact of solid elastic bodies). J. Reine Angew. Math. 92 (1882) 155-173
    • (1882) J. Reine Angew. Math. , vol.92 , pp. 155-173
    • Hertz, H.1
  • 8
    • 62549138222 scopus 로고    scopus 로고
    • Characterisation of granule structure and strength made in a high shear granulator
    • Rahmanian N., Ghadiri M., Jia X., and Stepanek F. Characterisation of granule structure and strength made in a high shear granulator. Powder Technol. 192 (2009) 184-194
    • (2009) Powder Technol. , vol.192 , pp. 184-194
    • Rahmanian, N.1    Ghadiri, M.2    Jia, X.3    Stepanek, F.4
  • 9
    • 55749115837 scopus 로고    scopus 로고
    • Three-dimensional analysis of macroporosity distributions in polyolefin particles using X-ray microtomography
    • Boden S., Bieberle M., Weickert G., and Hampel U. Three-dimensional analysis of macroporosity distributions in polyolefin particles using X-ray microtomography. Powder Technol. 188 (2008) 81-88
    • (2008) Powder Technol. , vol.188 , pp. 81-88
    • Boden, S.1    Bieberle, M.2    Weickert, G.3    Hampel, U.4
  • 10
    • 0037613447 scopus 로고    scopus 로고
    • Use of X-ray tomography to study the porosity and morphology of granules
    • Farber L., Tardos G., and Michaels J.N. Use of X-ray tomography to study the porosity and morphology of granules. Powder Technol. 132 (2003) 57-63
    • (2003) Powder Technol. , vol.132 , pp. 57-63
    • Farber, L.1    Tardos, G.2    Michaels, J.N.3
  • 11
    • 34547159349 scopus 로고    scopus 로고
    • Synthesis and characterization of polyamide powders for sorption of reactive dyes from aqueous solutions
    • Suteu D., Bilba D., and Dan F. Synthesis and characterization of polyamide powders for sorption of reactive dyes from aqueous solutions. J. Appl. Polym. Sci. 105 (2007) 1833-1843
    • (2007) J. Appl. Polym. Sci. , vol.105 , pp. 1833-1843
    • Suteu, D.1    Bilba, D.2    Dan, F.3
  • 12
    • 0034761360 scopus 로고    scopus 로고
    • The effect of shape and porosity on the compression behaviour and tablet forming ability of granular materials formed from microcrystalline cellulose
    • Johansson B., and Alderborn G. The effect of shape and porosity on the compression behaviour and tablet forming ability of granular materials formed from microcrystalline cellulose. Eur. J. Pharm. Biopharm. 52 (2001) 347-357
    • (2001) Eur. J. Pharm. Biopharm. , vol.52 , pp. 347-357
    • Johansson, B.1    Alderborn, G.2
  • 13
    • 0033053338 scopus 로고    scopus 로고
    • Tabletting behaviour of pellets of a series of porosities - a comparison between pellets of two different compositions
    • Nicklasson F., Johansson B., and Alderborn G. Tabletting behaviour of pellets of a series of porosities - a comparison between pellets of two different compositions. Eur. J. Pharm. Sci. 8 (1999) 11-17
    • (1999) Eur. J. Pharm. Sci. , vol.8 , pp. 11-17
    • Nicklasson, F.1    Johansson, B.2    Alderborn, G.3
  • 14
    • 0029982182 scopus 로고    scopus 로고
    • Degree of pellet deformation during compaction and its relationship to the tensile strength of tablets formed of microcrystalline cellulose pellets
    • Johansson B., and Alderborn G. Degree of pellet deformation during compaction and its relationship to the tensile strength of tablets formed of microcrystalline cellulose pellets. Int. J. Pharm. 132 (1996) 207-220
    • (1996) Int. J. Pharm. , vol.132 , pp. 207-220
    • Johansson, B.1    Alderborn, G.2
  • 15
    • 0028872408 scopus 로고
    • Compression behaviour and compactability of microcrystalline cellulose pellets in relationship to their pore structure and mechanical properties
    • Johansson B., Wikberg M., Ek R., and Alderborn G. Compression behaviour and compactability of microcrystalline cellulose pellets in relationship to their pore structure and mechanical properties. Int. J. Pharm. 117 (1995) 57-73
    • (1995) Int. J. Pharm. , vol.117 , pp. 57-73
    • Johansson, B.1    Wikberg, M.2    Ek, R.3    Alderborn, G.4
  • 16
    • 0032711132 scopus 로고    scopus 로고
    • Microcrystalline cellulose and its microstructure in pharmaceutical processing
    • Westermarck S., Juppo A.M., Kervinen L., and Yliruusi J. Microcrystalline cellulose and its microstructure in pharmaceutical processing. Eur. J. Pharm. Biopharm. 48 (1999) 199-206
    • (1999) Eur. J. Pharm. Biopharm. , vol.48 , pp. 199-206
    • Westermarck, S.1    Juppo, A.M.2    Kervinen, L.3    Yliruusi, J.4
  • 17
    • 63549108054 scopus 로고    scopus 로고
    • A small-angle X-ray scattering study of local variations within powder compacts
    • Laity P.R., and Cameron R.E. A small-angle X-ray scattering study of local variations within powder compacts. Powder Technol. 192 (2009) 287-297
    • (2009) Powder Technol. , vol.192 , pp. 287-297
    • Laity, P.R.1    Cameron, R.E.2
  • 18
    • 56549107748 scopus 로고    scopus 로고
    • A small-angle X-ray scattering study of powder compaction
    • Laity P.R., and Cameron R.E. A small-angle X-ray scattering study of powder compaction. Powder Technol. 188 (2008) 119-127
    • (2008) Powder Technol. , vol.188 , pp. 119-127
    • Laity, P.R.1    Cameron, R.E.2
  • 19
    • 33646734881 scopus 로고    scopus 로고
    • Experiments on corn pressure in silo cells - translation and comment of Janssen's paper from 1895
    • Sperl M. Experiments on corn pressure in silo cells - translation and comment of Janssen's paper from 1895. Granul. Matter 8 (2006) 59-65
    • (2006) Granul. Matter , vol.8 , pp. 59-65
    • Sperl, M.1
  • 20
    • 0037892514 scopus 로고    scopus 로고
    • Forces on bins: the effect of random friction
    • Pitman E.B. Forces on bins: the effect of random friction. Phys. Rev. E 57 (1998) 3170-3175
    • (1998) Phys. Rev. E , vol.57 , pp. 3170-3175
    • Pitman, E.B.1
  • 22
    • 0000158612 scopus 로고
    • Recent developments in polymer applications of small-angle neutron, X-ray and light scattering
    • Higgins J.S., and Stein R.S. Recent developments in polymer applications of small-angle neutron, X-ray and light scattering. J. Appl. Cryst. 11 (1978) 346-375
    • (1978) J. Appl. Cryst. , vol.11 , pp. 346-375
    • Higgins, J.S.1    Stein, R.S.2
  • 23
    • 75049083969 scopus 로고    scopus 로고
    • Changes in small-angle X-ray scattering during powder compaction - an explanation based on granule deformation
    • submitted for publication
    • P.R. Laity, R.E. Cameron, Changes in small-angle X-ray scattering during powder compaction - an explanation based on granule deformation, Powder Technology, submitted for publication.
    • Powder Technology
    • Laity, P.R.1    Cameron, R.E.2
  • 24
    • 0001155528 scopus 로고    scopus 로고
    • Calibration of rectangular atomic force microscope cantilevers
    • Sader J.E., Chon J.W.M., and Mulvaney P. Calibration of rectangular atomic force microscope cantilevers. Rev. Sci. Instrum. 70 (1999) 3967-3969
    • (1999) Rev. Sci. Instrum. , vol.70 , pp. 3967-3969
    • Sader, J.E.1    Chon, J.W.M.2    Mulvaney, P.3
  • 25
    • 32544455315 scopus 로고    scopus 로고
    • Determination of the surface free energy of crystalline and amorphous lactose by atomic force microscopy adhesion measurement
    • Zhang J., Ebbens S., Chen X., Jin Z., Luk S., Madden C., Patel N., and Roberts C.J. Determination of the surface free energy of crystalline and amorphous lactose by atomic force microscopy adhesion measurement. Pharm. Res. 23 (2006) 401-407
    • (2006) Pharm. Res. , vol.23 , pp. 401-407
    • Zhang, J.1    Ebbens, S.2    Chen, X.3    Jin, Z.4    Luk, S.5    Madden, C.6    Patel, N.7    Roberts, C.J.8
  • 26
    • 12444272525 scopus 로고
    • Adsorption of gases in multimolecular layers
    • Brunauer S., Emmett P.H., and Teller E. Adsorption of gases in multimolecular layers. J. Am. Chem. Soc. 60 (1938) 309-319
    • (1938) J. Am. Chem. Soc. , vol.60 , pp. 309-319
    • Brunauer, S.1    Emmett, P.H.2    Teller, E.3
  • 27
    • 0242523203 scopus 로고    scopus 로고
    • Fractal analysis of physical adsorption on material surfaces
    • Mahnke M., and Mögel H.J. Fractal analysis of physical adsorption on material surfaces. Col. Surf. A. Physicochem. Eng. Aspects 216 (2003) 215-228
    • (2003) Col. Surf. A. Physicochem. Eng. Aspects , vol.216 , pp. 215-228
    • Mahnke, M.1    Mögel, H.J.2
  • 28
    • 0342445773 scopus 로고
    • The determination of pore volume and area distributions in porous substances. I. Computations from nitrogen isotherms
    • Barrett E.P., Joyner L.G., and Halenda P.P. The determination of pore volume and area distributions in porous substances. I. Computations from nitrogen isotherms. J. Am. Chem. Soc. 73 (1951) 373-380
    • (1951) J. Am. Chem. Soc. , vol.73 , pp. 373-380
    • Barrett, E.P.1    Joyner, L.G.2    Halenda, P.P.3
  • 29
    • 0026244076 scopus 로고
    • Small-angle scattering studies of disordered, porous and fractal systems
    • Schmidt P. Small-angle scattering studies of disordered, porous and fractal systems. J. Appl. Cryst. 24 (1991) 414-435
    • (1991) J. Appl. Cryst. , vol.24 , pp. 414-435
    • Schmidt, P.1
  • 30
  • 31
    • 0031235505 scopus 로고    scopus 로고
    • SAXS measurements of the interface in polyacrylate and epoxy interpenetrating networks with fractal interfaces
    • Tan S., Zhang D., and Zhou E. SAXS measurements of the interface in polyacrylate and epoxy interpenetrating networks with fractal interfaces. Polymer 38 (1997) 4571-4575
    • (1997) Polymer , vol.38 , pp. 4571-4575
    • Tan, S.1    Zhang, D.2    Zhou, E.3
  • 32
    • 33749578590 scopus 로고    scopus 로고
    • Gelatinization of starch in excess water: beyond the melting of lamellar crystallites. A combined wide- and small-angle X-ray scattering study
    • Vermeylen R., Derycke V., Delcour J.A., Goderis B., Reynaers H., and Koch M.H.J. Gelatinization of starch in excess water: beyond the melting of lamellar crystallites. A combined wide- and small-angle X-ray scattering study. Biomacromolecules 7 (2006) 2624-2630
    • (2006) Biomacromolecules , vol.7 , pp. 2624-2630
    • Vermeylen, R.1    Derycke, V.2    Delcour, J.A.3    Goderis, B.4    Reynaers, H.5    Koch, M.H.J.6
  • 33
    • 0031347087 scopus 로고    scopus 로고
    • Interpretation of small angle X-ray scattering from starch on the basis of fractals
    • Suzuki T., Chiha A., and Yano T. Interpretation of small angle X-ray scattering from starch on the basis of fractals. Carbohydr. Polym. 34 (1997) 357-363
    • (1997) Carbohydr. Polym. , vol.34 , pp. 357-363
    • Suzuki, T.1    Chiha, A.2    Yano, T.3
  • 35
    • 75449086711 scopus 로고    scopus 로고
    • J.S. Lin, M-Y. Tang, J.F. Fellers, Fractal analysis of cotton cellulose as characterized by small-angle X-ray scattering, in: R.H. Atalla (Ed.), The Structures of Cellulose: Characterisation of the Solid State, ACS Symposium Series 340, 1987 (Chapter14).
    • J.S. Lin, M-Y. Tang, J.F. Fellers, Fractal analysis of cotton cellulose as characterized by small-angle X-ray scattering, in: R.H. Atalla (Ed.), The Structures of Cellulose: Characterisation of the Solid State, ACS Symposium Series 340, 1987 (Chapter14).
  • 36
    • 0008126156 scopus 로고
    • Variation in the lattice spacing of cellulose
    • Wellard H.J. Variation in the lattice spacing of cellulose. J. Polym. Sci. 13 (1954) 471-476
    • (1954) J. Polym. Sci. , vol.13 , pp. 471-476
    • Wellard, H.J.1
  • 37
    • 0001376995 scopus 로고
    • Crystallinity and crystallite size measurement in cellulose fibres: 1. Ramie and Fortisan
    • Hindeleh A.M., and Johnson D.J. Crystallinity and crystallite size measurement in cellulose fibres: 1. Ramie and Fortisan. Polymer 13 (1972) 423-430
    • (1972) Polymer , vol.13 , pp. 423-430
    • Hindeleh, A.M.1    Johnson, D.J.2
  • 38
    • 0016937944 scopus 로고
    • Determination of the structure of cellulose II
    • Kolpak F.J., and Blackwell J. Determination of the structure of cellulose II. Macromolecules 9 (1976) 273-278
    • (1976) Macromolecules , vol.9 , pp. 273-278
    • Kolpak, F.J.1    Blackwell, J.2
  • 39
    • 0026900113 scopus 로고
    • Tip-radius-induced artefacts in AFM images of protamine-complexed DNA fibres
    • Allen M.J., Hud N.V., Balooch M., Tench R.J., Siekhaus W.J., and Balhorn R. Tip-radius-induced artefacts in AFM images of protamine-complexed DNA fibres. Ultramicroscopy 42-44 Part 2 (1992) 1095-1100
    • (1992) Ultramicroscopy , vol.42-44 , Issue.PART 2 , pp. 1095-1100
    • Allen, M.J.1    Hud, N.V.2    Balooch, M.3    Tench, R.J.4    Siekhaus, W.J.5    Balhorn, R.6
  • 40
    • 0031168804 scopus 로고    scopus 로고
    • Phase imaging as an extension to tapping mode AFM for the identification of material properties on humidity-sensitive surfaces
    • Schmitz I., Schreiner M., Friedbacher G., and Grasserbauer M. Phase imaging as an extension to tapping mode AFM for the identification of material properties on humidity-sensitive surfaces. Appl. Surf. Sci. 115 (1997) 190-198
    • (1997) Appl. Surf. Sci. , vol.115 , pp. 190-198
    • Schmitz, I.1    Schreiner, M.2    Friedbacher, G.3    Grasserbauer, M.4
  • 43
    • 33846981178 scopus 로고    scopus 로고
    • Elastic modulus measurements from individual lactose particles using atomic force microscopy
    • Perkins M., Ebbens S.J., Hayes S., Roberts C.J., Madden C.E., Luk S.Y., and Patel N. Elastic modulus measurements from individual lactose particles using atomic force microscopy. Int. J. Pharm. 332 (2007) 168-175
    • (2007) Int. J. Pharm. , vol.332 , pp. 168-175
    • Perkins, M.1    Ebbens, S.J.2    Hayes, S.3    Roberts, C.J.4    Madden, C.E.5    Luk, S.Y.6    Patel, N.7
  • 44
    • 0034687574 scopus 로고    scopus 로고
    • Micro-scale measurement of the mechanical properties of compressed pharmaceutical powders. 1: the elasticity and fracture behavior of microcrystalline cellulose
    • Hancock B.C., Clas S.-D., and Christensen K. Micro-scale measurement of the mechanical properties of compressed pharmaceutical powders. 1: the elasticity and fracture behavior of microcrystalline cellulose. Int. J. Pharm. 209 (2000) 27-35
    • (2000) Int. J. Pharm. , vol.209 , pp. 27-35
    • Hancock, B.C.1    Clas, S.-D.2    Christensen, K.3
  • 45
    • 61849185901 scopus 로고    scopus 로고
    • Anisotropic elastic properties of cellulose measured using inelastic X-ray scattering
    • Diddens I., Murphy B., Krisch M., and Müller M. Anisotropic elastic properties of cellulose measured using inelastic X-ray scattering. Macromolecules 41 (2008) 9755-9759
    • (2008) Macromolecules , vol.41 , pp. 9755-9759
    • Diddens, I.1    Murphy, B.2    Krisch, M.3    Müller, M.4
  • 47
    • 0011836746 scopus 로고
    • Chemistry in non-integer dimensions between two and three. 1. Fractal theory of heterogeneous surfaces
    • Pfeifer P., and Avnir D. Chemistry in non-integer dimensions between two and three. 1. Fractal theory of heterogeneous surfaces. J. Chem. Phys. 79 (1983) 3558-3565
    • (1983) J. Chem. Phys. , vol.79 , pp. 3558-3565
    • Pfeifer, P.1    Avnir, D.2
  • 48
    • 0001345968 scopus 로고
    • Fractal BET and FHH theories of adsorption: a comparative study
    • Pfeifer P., Obert M., and Cole M.W. Fractal BET and FHH theories of adsorption: a comparative study. Proc. Roy. Soc. Lond. A 423 (1989) 169-188
    • (1989) Proc. Roy. Soc. Lond. A , vol.423 , pp. 169-188
    • Pfeifer, P.1    Obert, M.2    Cole, M.W.3
  • 49
    • 0345803800 scopus 로고    scopus 로고
    • Fractal dimension of cellulose powders analyzed by multilayer BET adsorption of water and nitrogen
    • Strømme M., Mihranyan A., Ek R., and Niklasson G.A. Fractal dimension of cellulose powders analyzed by multilayer BET adsorption of water and nitrogen. J. Phys. Chem. 107 (2003) 14378-14382
    • (2003) J. Phys. Chem. , vol.107 , pp. 14378-14382
    • Strømme, M.1    Mihranyan, A.2    Ek, R.3    Niklasson, G.A.4
  • 51
    • 0033888242 scopus 로고    scopus 로고
    • Determination of fractal dimensions of solid carbons from gas and liquid phase adsorption isotherms
    • Khalili N.R., Pan M., and Sandí G. Determination of fractal dimensions of solid carbons from gas and liquid phase adsorption isotherms. Carbon 38 (2000) 573-588
    • (2000) Carbon , vol.38 , pp. 573-588
    • Khalili, N.R.1    Pan, M.2    Sandí, G.3
  • 52
    • 34547954090 scopus 로고    scopus 로고
    • Porosity of microporous zeolites A, X and ZSM-5 studied by small angle X-ray scattering and nitrogen adsorption
    • Du X., and Wu E. Porosity of microporous zeolites A, X and ZSM-5 studied by small angle X-ray scattering and nitrogen adsorption. J. Phys. Chem. Solids 68 (2007) 1692-1699
    • (2007) J. Phys. Chem. Solids , vol.68 , pp. 1692-1699
    • Du, X.1    Wu, E.2
  • 53
    • 0028668666 scopus 로고
    • Welded tuff porosity characterization using mercury intrusion, nitrogen and ethylene glycol monoethyl ether sorption and epifluorescence microscopy
    • Reddy M.M., Claassen H.C., Rutherford D.W., and Chiou C.T. Welded tuff porosity characterization using mercury intrusion, nitrogen and ethylene glycol monoethyl ether sorption and epifluorescence microscopy. Appl. Geochem. 9 (1994) 491-499
    • (1994) Appl. Geochem. , vol.9 , pp. 491-499
    • Reddy, M.M.1    Claassen, H.C.2    Rutherford, D.W.3    Chiou, C.T.4


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.