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Dipp2 has been reported previously, but a detailed synthesis was not disclosed. We therefore present full details of its preparation and characterization in the Experimental Section.
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6)) are consistent with predominate isocyanide σ-donation concomitant with a minimal back bonding interaction. (a)
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As derived from metal hydrides, the covalent radii of Cu and Ag are tabulated as, 1.11 Å and 1.26 Å, respectively.
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2]OTf arises from the larger covalent radius of Ag(I) as compared to that of Cu(I). See the Supporting Information for representative spectra.
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2]OTf arises from the larger covalent radius of Ag(I) as compared to that of Cu(I). See the Supporting Information for representative spectra.
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56
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33947477539
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note
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3 that we prepare.
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81
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69549084443
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(CO) IR active frequencies. See ref 25.
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(CO) IR active frequencies. See ref 25.
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82
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5 complexes (M = Cr, Mo, W; sol = NCMe, THF)
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69549133391
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See the Supporting Information.
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See the Supporting Information.
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99
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69549107506
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Dipp2 units is firmly established. One component of the disorder model is depicted in Figure 11.
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Dipp2 units is firmly established. One component of the disorder model is depicted in Figure 11.
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100
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0011544130
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5.
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16844363448
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