NMR chemical shifts of common laboratory solvents as trace impurities

Journal of Organic Chemistry

Volumn 62, Issue 21, 1997, Pages 7512-7515

  Gottlieb, Hugo E ^a   Kotlyar, Vadim ^a   Nudelman, Abraham ^a  

^a BAR ILAN UNIVERSITY   (Israel)

Author keywords

[No Author keywords available]

Indexed keywords

NMR CHEMICAL SHIFTS; NON-POLAR SOLVENTS; TRACE IMPURITIES; WATER SIGNALS;

CHEMICAL SHIFT; HYDROGEN BONDS; METHANOL;

SOLVENTS;

EID: 84889582115     PISSN: 00223263     EISSN: 15206904     Source Type: Journal    
DOI: 10.1021/jo971176v     Document Type: Article

References (4)

1. For recommendations on the publication of NMR data, see: IUPAC Commission on Molecular Structure and Spectroscopy. Pure Appl. Chem. 1972, 29, 627;
2. 1976, 45, 217.
3. 2 groups (deuterated acetone, DMSO, acetonitrile), this signal is a 1:2:3:2:1 quintet with a splitting of ca. 2 Hz.
4. 13C spectra the solvent signal is due to the perdeuterated isotopomer, and the one-bond couplings to deuterium are always observable (ca. 20-30 Hz).