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68049092497
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Crystal data for compound E-2a: C16H 17O4I, MW, 400.20, monoclinic, space group P2(1)/c, final R indices [I > 2σ(I, R1, 0.0332, wR2, 0.0847, R indices (all data, R1, 0.0394, wR2, 0.0878, a, 9.1568 (7) Å, b, 19.9575 (16) Å, c, 9.6108 (7) Å, α, 90°, β, 114.2340(1)°, γ, 90°, V, 1601.6 (2) Å3, T, 293(2) K, Z, 4, reflections collected/unique: 9277/3483 (R(int, 0.0446, number of observations [> 2σ(I, 2984, parameters 193. Supplementary crystallographic data have been deposited at the Cambridge Crystallographic Data Center as supplementary publication no. CCDC 694977. Copies of the data can be obtained free of charge on application toCCDC, 12 Union Road, Cambridge CB2 1EZ, UK Fax:, 44-1223/336- 033; E-mail: deposit@ccdc.cam.ac.uk
-
3, T = 293(2) K, Z = 4, reflections collected/unique: 9277/3483 (R(int) = 0.0446), number of observations [> 2σ(I)] 2984, parameters 193. Supplementary crystallographic data have been deposited at the Cambridge Crystallographic Data Center as supplementary publication no. CCDC 694977. Copies of the data can be obtained free of charge on application toCCDC, 12 Union Road, Cambridge CB2 1EZ, UK (Fax: + 44-1223/336- 033; E-mail: deposit@ccdc.cam.ac.uk).
-
-
-
-
76
-
-
68049098624
-
-
Crystal data for compound E-2b: C12H 17O4I, MW, 352.16, monoclinic, space group P2(1)/c, final R indices [I > 2σ(I, R1, 0.0416, wR2, 0.1048, R indices (all data, R1, 0.0460, wR2, 0.1075, a, 8.2163(9) Å, b, 13.1526(15) Å, c, 12.5835(14) Å, α, 90°, β, 95.994(2)°, γ, 90°, V, 1352.4 (3) Å3, T, 293(2) K, Z, 4, reflections collected/unique: 7777/2944 (R(int, 0.0900, number of observations [> 2σ(I, 2565, parameters 157. Supplementary crystallographic data have been deposited at the Cambridge Crystallographic Data Center as supplementary publication no. CCDC 694978. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK Fax:, 44-1223/336- 033; E-mail: deposit@ccdc.cam.ac.uk
-
3, T = 293(2) K, Z = 4, reflections collected/unique: 7777/2944 (R(int) = 0.0900), number of observations [> 2σ(I )] 2565, parameters 157. Supplementary crystallographic data have been deposited at the Cambridge Crystallographic Data Center as supplementary publication no. CCDC 694978. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK (Fax: + 44-1223/336- 033; E-mail: deposit@ccdc.cam.ac.uk).
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0001713670
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