Simultaneous extraction and cleanup method based on pressurized solvent extraction for multiresidue analysis of pesticides in complex feed samples

Journal of Agricultural and Food Chemistry

Volumn 57, Issue 10, 2009, Pages 3963-3973

  Fernandez Alvarez, Maria ^a   Llompart, Maria ^a   Lamas, J Pablo ^a   Lores, Marta ^a   Garci Jares, Carmen ^a   Garcia Chao, Maria ^b   Dagnac, Thierry ^b  

^a UNIVERSITY OF SANTIAGO DE COMPOSTELA   (Spain)

^b Centro de Investigacions Agrarias de Mabegondo   (Spain)

Author keywords

Cattle feed; Experimental design; Feed analysis; Organochlorine pesticides; Pesticides; Pressurized solvent extraction; Pyrethroids

Indexed keywords

ACETAMIDE DERIVATIVE; CHLORINATED HYDROCARBON; ORGANOPHOSPHORUS COMPOUND; PESTICIDE RESIDUE; PYRETHROID; SOLVENT;

ANIMAL; ANIMAL FOOD; ARTICLE; CATTLE; FOOD ANALYSIS; GAS CHROMATOGRAPHY; METHODOLOGY; PRESSURE;

ACETAMIDES; ANIMAL FEED; ANIMALS; CATTLE; CHROMATOGRAPHY, GAS; FOOD ANALYSIS; HYDROCARBONS, CHLORINATED; ORGANOPHOSPHORUS COMPOUNDS; PESTICIDE RESIDUES; PRESSURE; PYRETHRINS; SOLVENTS;

ANIMALIA; BOS;

EID: 66149117735     PISSN: 00218561     EISSN: None     Source Type: Journal    
DOI: 10.1021/jf9004252     Document Type: Article

References (33)

1. New Rules on Pesticide Residues in Food. In Directorate-General for Health and Consumers, European Commission: Brussels, Belgium, 2008. http://ec.europa.eu/food/plant/protection/pesticides/explanation-pesticide- residues.pdf
2. Directive 2002/32/EC of the European Parliament and of the Council of 7 May 2002 on undesirable substances in animal feed, Off. J. Eur. Comm., No. , 30 May 2002.
3. Regulation (EC) No 396/2005 of the European Parliament and of the Council of 23 February 2005 on maximum residue levels of pesticides in or on food and feed of plant and animal origin and amending Council Directive 91/414/EEC.
4. Commission Regulation (EC) No 839/2008 of 31 July 2008 amending Regulation (EC) No 396/2005 of the European Parliament and of the Council as regards Annexes II, III and IV setting maximum residue levels of pesticides in or on certain products.
5. United States Department of Agriculture (USDA), Foreign Agricultural Service, Maximum Residue Level Database. http://www. fas.usda.gov/htp/MRL.asp (last accessed Jan 2009).
6. Aulakh, R. S.; Gill, J. P. S.; Bedi, J. S.; Sharma, J. K.; Joia, B. S.; Ockerman, H. W. Organochlorine pesticide residues in poultry feed, chicken muscle and eggs at a poultry farm in Punjab, India. J. Sci. Food Agric. 2006, 86, 741-744.
7. van der Lee, M. K.; van der Weg, G.; Traag, W. A.; Mol, H. G. J. Qualitative screening and quantitative determination of pesticides and contaminants in animal feed using comprehensive two-dimensional gas chromatography with time-of-flight mass spectrometry. J. Chromatogr., A 2008, 1186, 325-339.
8. Gfrerer, M.; Chen, S.; Lankmayr, E. P.; Quan, X.; Yang, F. Comparison of different extraction techniques for the determination of chlorinated pesticides in animal feed. Anal. Bioanal. Chem. 2004, 378, 1861-1867.
9. Iglesias-García, I.; Barriada-Pereira, M.; González-Castro, M. J.; Muniategui-Lorenzo, S.; López-Mahía, P.; Prada-Rodríguez, D. Development of an analytical method based on microwave-assisted extraction and solid phase extraction cleanup for the determination of organochlorine pesticides in animal feed. Anal. Bioanal. Chem. 2008, 391, 745-752.
10. Walorczyk, S. Development of a multi-residue screening method for the determination of pesticides in cereals and dry animal feed using gas chromatography-triple quadrupole tandem mass spectrometry. J. Chromatogr., A 2007, 1165, 200-212.
11. Fernandez-Alvarez, M.; Llompart, M.; Lamas, J. P.; Lores, M.; Garcia-Jares, C.; Cela, R.; Dagnac, T. Development of a matrix solid-phase dispersion method for the simultaneous determination of pyrethroid and organochlorinated pesticides in cattle feed. J. Chromatogr., A 2009, 1216, 2832-2842.
12. EPA Method 3545, Pressurised Fluid Extraction. In Test Methods for Evaluating Solid Waste, Physical/Chemical Methods, 3rd ed., Final Update IV; EPA SW-846; U.S. GPO: Washington, DC, 2008.
13. Nieto, A.; Borrull, F.; Marce, R. M.; Pocurull, E. Pressurized liquid extraction of contaminants from environmental samples. Curr. Anal. Chem. 2008, 4, 157-167.
14. Adou, K.; Bontoyan, W. R.; Sweeney, P. J. Multiresidue method for the analysis of pesticide residues in fruits and vegetables by accelerated solvent extraction and capillary gas chromatography. J. Agric. Food. Chem. 2001, 49, 4153-4160.
15. Pang, G.-F.; Liu, Y.-M.; Fan, C.-L.; Zhang, J.-J.; Cao, Y.-Z.; Li, X.-M.; Li, Z.-Y.; Wu, Y.-P.; Guo, T.-T. Simultaneous determination of 405 pesticide residues in grain by accelerated solvent extraction then gas chromatography-mass spectrometry or liquid chromatographytandem mass spectrometry. Anal. Bioanal. Chem. 2006, 384, 1366-1408.
16. Nemoto, S.; Lehotay, S. J. Analysis of multiple herbicides in soybeans using pressurized liquid extraction and capillary electrophoresis. J. Agric. Food Chem. 1998, 46, 2190-2199.
17. Obana, H.; Kikuchi, K.; Okihashi, M.; Hori, S. Determination of organophosphorus pesticides in foods using an accelerated solvent extraction system. Analyst 1997, 122, 217-220.
18. Chen, S.; Gfrerer, M.; Lankmayr, E.; Quan, X.; Yang, F. Optimization of accelerated solvent extraction for the determination of chlorinated pesticides from animal feed. Chromatographia 2003, 58, 631-636.
19. Mendiola, J. A.; Herrero, M.; Cifuentes, A.; Ibañez, E. Use of compressed fluids for sample preparation: Food applications. J. Chromatogr., A 2007, 1152, 234-246.
20. Wilga, J.; Kot-Wasik, A.; Namiesnik, J. Comparison of extraction techniques of robenidine from poultry feed samples. Talanta 2007, 73, 812-819.
21. Syhre, M.; Hanschmann, G.; Heber, R. Cleanup procedure for monitoring chlorinated compounds in animal feed and crops. J. AOAC Int. 1998, 81, 513-517.
22. Argauer, R. J.; Lehotay, S. J.; Brown, R. T. Determining lipophilic pyrethroids and chlorinated hydrocarbons in fortified ground beef using ion-trap mass spectrometry. J. Agric. Food Chem. 1997, 45, 3936-3939.
23. Sporring, S.; Björklund, E. Selective pressurized liquid extraction of polychlorinated biphenyls from fat-containing food and feed samples. Influence of cell dimensions, solvent type, temperature and flush volume. J. Chromatogr., A 2004, 1040, 155-161.
24. Garrido Frenich, A.; Martínez Vidal, J. L.; Cruz Sicilia, A. D.; González Rodriguez, M. J.; Plaza Bolaños, P. Multiresidue analysis of organochlorine and organophosphorus pesticides in muscle of chicken, pork and lamb by gas chromatography-triple quadrupole mass spectrometry. Anal. Chim. Acta 2006, 555, 42-52.
25. Gómez-Ariza, J. L.; Bujalance, M.; Giráldez, I.; Velasco, A.; Morales, E. Determination of polychlorinated biphenyls in biota samples using simultaneous pressurized liquid extraction and purification. J. Chromatogr., A 2002, 946, 209-219.
26. Draisci, R.; Marchiafava, C.; Ferretti, E.; Palleschi, L.; Catellani, G.; Anastasio, A. Evaluation of musk contamination of freshwater fish in Italy by accelerated solvent extraction and gas chromatography with mass spectrometric detection. J. Chromatogr., A 1998, 814, 187-197.
27. Carabias-Martinez, R.; Rodriguez-Gonzalo, E.; Revilla-Ruiz, P.; Hernández-Méndez, J. Pressurized liquid extraction in the analysis of food and biological samples. J. Chromatogr., A 2005, 1089, 1-17.
28. Methods Optimization in Accelerated Solvent Extraction (ASE®); Technical Note 208; Dionex Corporation: Sunnyvale, CA, 2004.
29. Giergielewicz-Możajska, H.; Da̧browski, L.; Namieśnik, J. Accelerated solvent extraction (ASE) in the analysis of environmental solid samples-Some aspects of theory and practice. Crit. Rev. Anal. Chem. 2001, 31, 149-165.
30. Gfrerer, M.; Lankmayr, E. DDT degradation during enhanced solid-liquid extractions. A consideration. J. Chromatogr., A 2005, 1072, 117-125.
31. Extraction of Chlorinated Pesticides Using Accelerated Solvent Extraction (ASE®); Application Note 320 (Dionex); Dionex Corporation: Sunnyvale, CA, 2004.
32. Barriada-Pereira, M.; González-Castro, M. J.; Muniategui-Lorenzo, S.; López-Mahía, P.; Prada-Rodriguez, D.; Fernández- Fernández, E. Comparison of pressurized liquid extraction and microwave assisted extraction for the determination of organochlorine pesticides in vegetables. Talanta 2007, 71, 1345-1351.
33. Tuinstra, L. G. M. T.; Roos, A. H.; Griepink, B.; Maier, E. A. Certification of an animal feed reference material for the organochlorine pesticide contents: BCRCRM 115. Fresenius J. Anal. Chem. 1997, 357, 1035-1041.