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Crystal data for 3aa: C19H27NO, MW, 285.43, Monoclinic, space group P2 (1) /c, final R indices [I] 2σ (I, R1, 0.0377, wR2, 0.0881, a, 7.4333 (5) Å, b, 15.8825 (13) Å, c, 15.0972 (10) Å, α, 90°, β, 106.1198 (16) °, γ, 90°, V, 1712.3 (2) Å3, T, 296
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52
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