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A precise monitoring of the evolution of the film thickness during the grafting for the given sample was not possible since the set-up for in situ ellipsometric measurements is not compatible with rather demanding polymerization conditions (air- and water-sensitivity, low temperature). The reaction course, therefore, was monitored for series of samples by the termination of the grafting process after a respective time.
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1H NMR.
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67849103087
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pS(i) = 232 × 1.33 × (38.5-7.5) 168 × 2.0 × 7.5 = 3.8.
-
pS(i) = 232 × 1.33 × (38.5-7.5) 168 × 2.0 × 7.5 = 3.8.
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