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62649128124
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-1): 3201w br, 2287m, 2228m, 2162s, 1618m, 1565w, 1426w, 1363m, 1350m, 1336m, 1303w, 1271w, 1225w, 1144w, 1120m, 1072w, 1013m, 992m, 947w, 911w, 852m, 839m, 801s, 677m.
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-1): 3201w br, 2287m, 2228m, 2162s, 1618m, 1565w, 1426w, 1363m, 1350m, 1336m, 1303w, 1271w, 1225w, 1144w, 1120m, 1072w, 1013m, 992m, 947w, 911w, 852m, 839m, 801s, 677m.
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62649115129
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Crystal data for 1: [Co(dca)2(4-bpmp)2(H2O)2]n, M, 495.40 g mol-1, monoclinic, space group P21/c, a, 9.5916(11) Å, b, 13.4429(15) Å, c, 18.149(2) Å, β, 102.920(1, V, 2280.9(4) Å3, Z, 4. Refinement of 156 parameters on 2643 independent reflections out of 12,542 measured reflections (Rint, 0.0281) led to R1, 0.0320, wR2, 0.0753 (all data) and S, 1.073. The hydrogen atoms bound to the aqua ligand were found by Fourier map. See supporting data for more detailed crystallographic information
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2 = 0.0753 (all data) and S = 1.073. The hydrogen atoms bound to the aqua ligand were found by Fourier map. See supporting data for more detailed crystallographic information.
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