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Wais, M.6
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13
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56649104339
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A mixture of Co(NO3)2·6H2O (55 mg, 0.19 mmol, H2oba (48 mg, 0.19 mmol, and bpmp (100 mg, 0.37 mmol) in 10 mL of H2O was heated at 120°C under autogenous pressure in an acid digestion bomb for 72 h. Small orange crystals of compound 1 (68 mg, 0.045 mmol, 71% yield) were isolated after washing with distilled water, ethanol, and acetone. IR (cm-1, powder, 2810(w, 1610(m, 1594(m, 1499(w, 1387(s, 1301(w, 1240(s, sh, 1232(s, 1160(m, 1129(w, 1067(w, 1011(m, 875(w, 853(w, 842(w, 794(w, 779(s, 766(w, 731(w, 694(w, 654(m, Anal. Calcd for C74H64CO 3N8O15 1, C, 59.97; H, 4.35; N, 7.56. Found: C, 59.39; H, 4.12; N, 7.62
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15 (1): C, 59.97; H, 4.35; N, 7.56. Found: C, 59.39; H, 4.12; N, 7.62.
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14
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56649093456
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-1, F(000) = 4590, R [I > 2σ(I)] = 0.0510, wR [I > 2σ(I)] = 0.1005, GOF = 0.856, T = 173(2) K, CCDC 689544.
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-1, F(000) = 4590, R [I > 2σ(I)] = 0.0510, wR [I > 2σ(I)] = 0.1005, GOF = 0.856, T = 173(2) K, CCDC 689544.
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16
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33745697785
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0000221522
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Blatov, V. A.; Shevchenko, A. P.; Serezhkin, V. N. J. Appl. Crystallogr. 2000, 33, 1193.
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Blatov, V.A.1
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19
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56649091857
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The long vertex symbol for this 8-connected network is 4.4.4.4.5.5.5 2.52.52.52.52.5 2.52.52.52.52.5 2.54.54.54.54.6 2.62.62.62.62.6 9.69
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9.
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20
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16244392144
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Ruiz-Valero, C.6
Iglesias, M.7
Gamez-Lor, B.8
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