Novel heterometallic 3d-4f metal-azido complex of mixed ligands with unprecedented structure type: Synthesis, structure, and magnetic properties

Inorganic Chemistry

Volumn 45, Issue 16, 2006, Pages 6129-6131

  Liu, Fu Chen ^a   Zeng, Yong Fei ^a   Jiao, Jiao ^a   Li, Jian Rong ^a   Bu, Xian He ^a   Ribas, Joan ^b   Batten, Stuart R ^c  

^a NANKAI UNIVERSITY   (China)

^b UNIVERSITY OF BARCELONA   (Spain)

^c MONASH UNIVERSITY   (Australia)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 33748264392     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic060773+     Document Type: Article

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28. 2O in the ratio of 1:2:2:5:2000 was sealed in a Teflon-lined autoclave and heated to 140°C for 2 days. The crystals were obtained in ca. 30% yield based on Ni. Elemental analysis is satisfactory. Caution! Azide complexes are potentially explosive. Only a small amount of the materials should be prepared and handled with care.
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