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In the 31P{1H} NMR spectra of the crude reaction mixtures, besides the signals from 1b (δp, 2.1 ppm) and 2b (δp, 20.5 ppm) other low-intensity signals were detected: a singlet of diisopropyl phosphite at δp, 5.2 ppm, a singlet at δp, 2.8 ppm and a couple of doublets of equal intensity at δp, 2.1 (Jp,p, 39.6 Hz) and 15.9 ppm Jp,p, 39.6 Hz
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