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31
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23044448746
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note
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Phthalimide ketones are readily prepared from phthalimide and halide substituted ketone in the presence of potassium carbonate (see Supporting Information).
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32
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1242298809
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Ru-Catalyzed asymmetric hydrogenation of α-phthalimide ketones: (a) Lei, A.; Wu, S.; He, M.; Zhang, X. J. Am. Chem. Soc. 2004, 126, 1626.
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34
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23044468531
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note
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For preparation of complex, see Supporting Information.
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35
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23044457613
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note
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2 = 4/1/1). The absolute configuration of 2 was determined by measurement of its optical rotation and comparison to the literature value or by analogue.
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36
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0001113218
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TFE as a solvent stabilizes the active catalysts: (a) Milani, B.; Anzilutti, A.; Vicentini, L.; Santi, A. S.; Zangrando, E.; Geremia, S.; Mestroni, G. Organometallics 1997, 16, 5064.
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(b) Milani, B.; Corso, G.; Mestroni, G. Organometallics 2000, 19, 3435.
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Milani, B.1
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0344530801
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(b) Whitfield, H. J.; Griffin, R. J.; Hardcastle, I. R.; Henderson, A.; Meneyrol, J.; Mesguiche, V.; Sayle, K. L.; Golding, B. T. Chem. Commun. 2003, 2802.
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Golding, B.T.8
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