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Single-Crystal X-ray Diffraction Data of Compound 4 C 34H52Br4N4O2Zn 4·0.5 (toluene, 1175.98, Stoe IPDS 2T, space group C2/c (No. 15) with a, 29.1063 (12) Å, b, 17.2017 (7) Å, c, 22.2739 (9) Å, β, 126.790 (2)° at 200 K, Z, 8, V, 8931.0(6) Å3, ρ, 1.749 g cm -3, 2cmax, 50°, 7865 reflections collected, 6354 unique reflections (Rint, 0.0860, The structure was solved by Patterson methods (SHELXS-97 and SHELXL-97) and refined by full-matrix least-square techniques with I > 2σ(I) to R 1, 0.0483 and wR2, 0.1190. Single-Crystal X-ray Diffraction Data of Compound 9 C34H56N 4O2Zn4 814.31, Oxford Diffraction Xcalibur S Sapphire, space group P
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2 = 0.0812. Positional parameters, hydrogen-atom parameters, thermal parameters, bond lengths and angles have been deposited as Supporting Information; CCDC-689633 (4) and 689634 (9).
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