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When 4- (N-benzylamino)-1-butyne was employed as a substrate, the reaction did not proceed and we could not observe desired product. In addition, the reaction of N-methy1-2-[ (trimethylsilyl)ethynyl]aniline, as one representative internal alkynyl substrate, did not take place.
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When 4- (N-benzylamino)-1-butyne was employed as a substrate, the reaction did not proceed and we could not observe desired product. In addition, the reaction of N-methy1-2-[ (trimethylsilyl)ethynyl]aniline, as one representative internal alkynyl substrate, did not take place.
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Whereas reactions of 1, 3- or 1, 4-aminoalkynes were postulated to proceed through the catalytic hydroamination route (Ref 6), those of 2-ethynylanilines are proposed here to form triazoles first followed by ring-opening process.
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