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Volumn , Issue 2, 2008, Pages 304-310

Chemistry of polyhalogenated nitrobutadienes, 6: A new ring-closure approach to perfunctionalized 5-nitropyrimidines

Author keywords

Halides; Nitro compounds; Nucleophilic substitution; Pyrimidines; Ring closure

Indexed keywords

NUCLEOPHILIC SUBSTITUTION; PYRIMIDINES; RING CLOSURE;

EID: 38849104330     PISSN: 00397881     EISSN: None     Source Type: Journal    
DOI: 10.1055/s-2007-990948     Document Type: Article
Times cited : (27)

References (32)
  • 6
    • 38849133720 scopus 로고    scopus 로고
    • All data of C10H12Cl2N4O 3 were collected on a Stoe IPDS-II single-crystal X-ray diffractometer with graphite monochromated MoKa radiation (λ, 0.71073 Å) at 223 K. The crystal structure was solved by direct methods and refined by full matrix leastsquares on F2 (SHELX-97) 4 in the triclinic space group P1 (Nr. 2, lattice parameters a, 921.5(3) pm, b, 1230.6(5) pm, c, 1369.6(6) pm, V, 1315.1(9) × 106 pm3, Z, 4, dcalc, 1.551 g cm-3, F(000, 632, absorption coefficient, 0.503 mm-1 using 4346 independent reflections and 439 parameters. R1, 0.0420, wR2, 0.1011 [I > 2σI, goodness of fit on F2, 1.082, residual electronic density, 0.463 and -0.341 e A-3. Crystallographic data have been deposited with th
    • -3. Crystallographic data have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-645171. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK (fax: +44(1223)336033, e-mail: fileserv@ccdc.ac.uk or http://www.ccdc.cam.ac.uk).
  • 7
    • 38849186192 scopus 로고    scopus 로고
    • Sheldrick, G. M. SHELX-97; University of Göttingen, 1997.
    • Sheldrick, G. M. SHELX-97; University of Göttingen, 1997.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.