-
1
-
-
0040174477
-
-
(a) Kaberdin, R. V.; Potkin, V. I.; Zapol'skii, V. A. Russ. Chem. Rev. 1997, 66, 827.
-
(1997)
Russ. Chem. Rev
, vol.66
, pp. 827
-
-
Kaberdin, R.V.1
Potkin, V.I.2
Zapol'skii, V.A.3
-
2
-
-
2942562101
-
-
(b) Zapol'skii, V. A.; Namyslo, J. C.; Adam, A. E. W.; Kaufmann, D. E. Heterocycles 2004, 63, 1281.
-
(2004)
Heterocycles
, vol.63
, pp. 1281
-
-
Zapol'skii, V.A.1
Namyslo, J.C.2
Adam, A.E.W.3
Kaufmann, D.E.4
-
3
-
-
33748773088
-
-
(c) Zapol'skii, V. A.; Nutz, E.; Namyslo, J. C.; Adam, A. E. W.; Kaufmann, D. E. Synthesis 2006, 2927.
-
(2006)
Synthesis
, pp. 2927
-
-
Zapol'skii, V.A.1
Nutz, E.2
Namyslo, J.C.3
Adam, A.E.W.4
Kaufmann, D.E.5
-
4
-
-
33845966730
-
-
(d) Zapol'skii, V. A.; Namyslo, J. C.; Blaschkowski, B.; Kaufmann, D. E. Synlett 2006, 3464.
-
(2006)
Synlett
, pp. 3464
-
-
Zapol'skii, V.A.1
Namyslo, J.C.2
Blaschkowski, B.3
Kaufmann, D.E.4
-
5
-
-
33947430159
-
-
(e) Zapol'skii, V. A.; Namyslo, J. C.; Gjikaj, M.; Kaufmann, D. E. ARKIVOC 2007, (i), 76.
-
(2007)
ARKIVOC
, vol.1
, pp. 76
-
-
Zapol'skii, V.A.1
Namyslo, J.C.2
Gjikaj, M.3
Kaufmann, D.E.4
-
7
-
-
0031352643
-
-
Zapol'skii, V. A.; Potkin, V. I.; Nechai, N. I.; Kaberdin, R. V.; Pevzner, M. S. Russ. J. Org. Chem. 1997, 33, 1461.
-
(1997)
Russ. J. Org. Chem
, vol.33
, pp. 1461
-
-
Zapol'skii, V.A.1
Potkin, V.I.2
Nechai, N.I.3
Kaberdin, R.V.4
Pevzner, M.S.5
-
8
-
-
34347373301
-
-
Crystal Data for 7 have been deposited with the Cambridge Crystallographic Data Center (CCDC 632420) and may be obtained free of charge from The Director
-
Crystal Data for 7 have been deposited with the Cambridge Crystallographic Data Center (CCDC 632420) and may be obtained free of charge from The Director, CCDC, 12 Union Road, Cambridge, CB2 1EZ, UK [fax:+44 (1223)336033; e-mail: fileserv@ccdc.ac.uk or www.ccdc.cam.ac.uk].
-
CCDC, 12 Union Road, Cambridge, CB2 1EZ, UK [fax:+44 (1223)336033; e-mail: Fileserv@ccdc.ac.uk or
-
-
-
9
-
-
34250228583
-
-
Molchanov, L. V.; Kadyrov, C. S.; Ayupova, A. T. Chem. Nat. Compd. 1981, 17, 357.
-
(1981)
Chem. Nat. Compd
, vol.17
, pp. 357
-
-
Molchanov, L.V.1
Kadyrov, C.S.2
Ayupova, A.T.3
-
10
-
-
34347404317
-
-
(a) Hirai, K.; Ishiba, T.; Sugimoto, H. Chem. Pharm. Bull. 1972, 20, 1711.
-
(1972)
Chem. Pharm. Bull
, vol.20
, pp. 1711
-
-
Hirai, K.1
Ishiba, T.2
Sugimoto, H.3
-
11
-
-
2442739934
-
-
(b) Schaumann, E.; Scheiblich, S.; Wriede, U.; Adiwidjaja, G. Chem. Ber. 1988, 121, 1165.
-
(1988)
Chem. Ber
, vol.121
, pp. 1165
-
-
Schaumann, E.1
Scheiblich, S.2
Wriede, U.3
Adiwidjaja, G.4
-
12
-
-
0000874570
-
-
(c) Shibuya, I.; Taguchi, Y.; Tsuchiya, T.; Oishi, A.; Katoh, E. Bull. Chem. Soc. Jpn. 1994, 67, 3048.
-
(1994)
Bull. Chem. Soc. Jpn
, vol.67
, pp. 3048
-
-
Shibuya, I.1
Taguchi, Y.2
Tsuchiya, T.3
Oishi, A.4
Katoh, E.5
-
13
-
-
0032532807
-
-
(d) Terang, N.; Mehta, B.; Ila, H.; Junjappa, H. Tetrahedron 1998, 54, 12973.
-
(1998)
Tetrahedron
, vol.54
, pp. 12973
-
-
Terang, N.1
Mehta, B.2
Ila, H.3
Junjappa, H.4
-
15
-
-
84993869127
-
-
(b) Takahashi, M.; Zheng, M.; Oshida, T.; Narahara, K. J. Heterocycl. Chem. 1994, 31, 205.
-
(1994)
Heterocycl. Chem
, vol.31
, pp. 205
-
-
Takahashi, M.1
Zheng, M.2
Oshida, T.3
Narahara, K.J.4
-
16
-
-
1342332607
-
-
(c) Chowdhury, S. K. D.; Sarkar, M.; Mahalanabis, K. K. J. Chem. Res., Synop. 2003, 11, 746.
-
(2003)
Chem. Res., Synop
, vol.11
, pp. 746
-
-
Chowdhury, S.K.D.1
Sarkar, M.2
Mahalanabis, K.K.J.3
-
17
-
-
84948492933
-
-
(a) Chattaway, F. D.; Lye, R. J. Proc R. Soc. London, Ser. A 1932, 135, 282.
-
(1932)
Proc R. Soc. London, Ser. A
, vol.135
, pp. 282
-
-
Chattaway, F.D.1
Lye, R.J.2
-
21
-
-
34250119874
-
-
(b) Saloutin, V. I.; Fomin, A. N.; Pashkevich, K. I. Bull. Acad. Sci. USSR Div. Chem. Sci. (Engl. Transl.) 1985, 34, 135.
-
(1985)
Bull. Acad. Sci. USSR Div. Chem. Sci. (Engl. Transl.)
, vol.34
, pp. 135
-
-
Saloutin, V.I.1
Fomin, A.N.2
Pashkevich, K.I.3
-
22
-
-
13444266910
-
-
(c) Penning, T. D.; Talley, J. J.; Bertenshaw, S. R.; Carter, J. S.; Collins, P. W.; Docter, S.; Graneto, M. J.; Lee, L. F.; Malecha, J. W.; Miyashiro, J. M.; Rogers, R. S.; Rogier, D. J.; Yu, S. S.; Anderson, G. D.; Burton, E. G.; Cogburn, J. N.; Gregory, S. A.; Koboldt, C. M.; Perkins, W. E.; Seibert, K.; Veenhuizen, A. W.; Zhang, Y. Y.; Isakson, P. C. J. Med. Chem. 1997, 40, 1347.
-
(1997)
J. Med. Chem
, vol.40
, pp. 1347
-
-
Penning, T.D.1
Talley, J.J.2
Bertenshaw, S.R.3
Carter, J.S.4
Collins, P.W.5
Docter, S.6
Graneto, M.J.7
Lee, L.F.8
Malecha, J.W.9
Miyashiro, J.M.10
Rogers, R.S.11
Rogier, D.J.12
Yu, S.S.13
Anderson, G.D.14
Burton, E.G.15
Cogburn, J.N.16
Gregory, S.A.17
Koboldt, C.M.18
Perkins, W.E.19
Seibert, K.20
Veenhuizen, A.W.21
Zhang, Y.Y.22
Isakson, P.C.23
more..
-
23
-
-
0030955273
-
-
(d) Tsuji, K.; Konishi, N.; Spears, G. W.; Ogino, T.; Nakamura, K.; Tojo, T.; Ochi, T.; Shimojo, F.; Senoh, H.; Matsuo, M. Chem. Pharm. Bull. 1997, 45, 1475.
-
(1997)
Chem. Pharm. Bull
, vol.45
, pp. 1475
-
-
Tsuji, K.1
Konishi, N.2
Spears, G.W.3
Ogino, T.4
Nakamura, K.5
Tojo, T.6
Ochi, T.7
Shimojo, F.8
Senoh, H.9
Matsuo, M.10
-
24
-
-
0141586472
-
-
(e) Filyakova, V. I.; Karpenko, N. S.; Kuznetsova, O. A.; Pashkevich, K. I. Russ. J. Org. Chem. 1998, 34, 381.
-
(1998)
Russ. J. Org. Chem
, vol.34
, pp. 381
-
-
Filyakova, V.I.1
Karpenko, N.S.2
Kuznetsova, O.A.3
Pashkevich, K.I.4
-
25
-
-
0347517818
-
-
(f) Li, J.; DeMello, K. M. L.; Cheng, H.; Sakya, S. M.; Bronk, B. S.; Rafka, R. J.; Jaynes, B. H.; Ziegler, C. B.; Kilroy, C.; Mann, D. W.; Nimz, E. L.; Lynch, M. P.; Haven, M. L.; Kolosko, N. L.; Minich, M. L.; Li, C.; Dutra, J. K.; Rast, B.; Crosson, R. M.; Morton, B. J.; Kirk, G. W.; Callaghan, K. M.; Koss, D. A.; Shavnya, A.; Lund, L. A.; Seibel, S. B.; Petras, C. F.; Silvia, A. Bioorg. Med. Chem. Lett. 2004, 14, 95.
-
(2004)
Bioorg. Med. Chem. Lett
, vol.14
, pp. 95
-
-
Li, J.1
DeMello, K.M.L.2
Cheng, H.3
Sakya, S.M.4
Bronk, B.S.5
Rafka, R.J.6
Jaynes, B.H.7
Ziegler, C.B.8
Kilroy, C.9
Mann, D.W.10
Nimz, E.L.11
Lynch, M.P.12
Haven, M.L.13
Kolosko, N.L.14
Minich, M.L.15
Li, C.16
Dutra, J.K.17
Rast, B.18
Crosson, R.M.19
Morton, B.J.20
Kirk, G.W.21
Callaghan, K.M.22
Koss, D.A.23
Shavnya, A.24
Lund, L.A.25
Seibel, S.B.26
Petras, C.F.27
Silvia, A.28
more..
-
26
-
-
0346513076
-
-
Kagabu, S.; Moriya, K.; Shibuya, K.; Hattori, Y.; Tsuboi, S.; Shiokawa, K. Biosci. Biotechnol. Biochem. 1992, 56, 362.
-
(1992)
Biosci. Biotechnol. Biochem
, vol.56
, pp. 362
-
-
Kagabu, S.1
Moriya, K.2
Shibuya, K.3
Hattori, Y.4
Tsuboi, S.5
Shiokawa, K.6
-
27
-
-
0037142378
-
-
(a) Zhang, N.; Tomizawa, M.; Casida, J. E. J. Med. Chem. 2002, 45, 2832.
-
(2002)
Med. Chem
, vol.45
, pp. 2832
-
-
Zhang, N.1
Tomizawa, M.2
Casida, J.E.J.3
-
28
-
-
0001303576
-
-
(b) Shiokawa, K.; Moriya, K.; Shibuya, K.; Hattori, Y.; Tsuboi, S.; Kagabu, S. J. Biosci. Biotechnol. Biochem. 1992, 56, 1364.
-
(1992)
Biosci. Biotechnol. Biochem
, vol.56
, pp. 1364
-
-
Shiokawa, K.1
Moriya, K.2
Shibuya, K.3
Hattori, Y.4
Tsuboi, S.5
Kagabu, S.J.6
-
29
-
-
0036011062
-
-
(c) Kagabu, S.; Nishiwaki, H.; Sato, K.; Hibi, M.; Yamaoka, N.; Nakagawa, Y. Pest Manage. Sci. 2002, 58, 483.
-
(2002)
Pest Manage. Sci
, vol.58
, pp. 483
-
-
Kagabu, S.1
Nishiwaki, H.2
Sato, K.3
Hibi, M.4
Yamaoka, N.5
Nakagawa, Y.6
-
30
-
-
34347390249
-
-
Fischer, R, Jeschke, P, Erdelen, C, Lösel, P, Reckmann, U, Kaufmann, D, Zapol'skii, V, Bayer AG, WO 03/040129A1, 2003
-
(d) Fischer, R.; Jeschke, P.; Erdelen, C.; Lösel, P.; Reckmann, U.; Kaufmann, D.; Zapol'skii, V. (Bayer AG); WO 03/040129A1, 2003.
-
-
-
-
31
-
-
33947292785
-
-
(a) Soulen, R. L.; Clifford, D. B.; Crim, F. F.; Johnston, J. A. J. Org. Chem. 1971, 36, 3386.
-
(1971)
Org. Chem
, vol.36
, pp. 3386
-
-
Soulen, R.L.1
Clifford, D.B.2
Crim, F.F.3
Johnston, J.A.J.4
-
32
-
-
0026017374
-
-
(b) Belen'kii, L. I.; Brokhovetskii, D. B.; Krayushkin, M. M. Tetrahedron 1991, 47, 447.
-
(1991)
Tetrahedron
, vol.47
, pp. 447
-
-
Belen'kii, L.I.1
Brokhovetskii, D.B.2
Krayushkin, M.M.3
-
33
-
-
0035904861
-
-
(c) Garuti, L.; Roberti, M.; Pession, A.; Leoncini, E.; Hrelia, S. Bioorg. Med. Chem. Lett. 2001, 11, 3147.
-
(2001)
Bioorg. Med. Chem. Lett
, vol.11
, pp. 3147
-
-
Garuti, L.1
Roberti, M.2
Pession, A.3
Leoncini, E.4
Hrelia, S.5
-
35
-
-
37049111132
-
-
(e) Hall, R. H.; Jordaan, A.; Malherbe, M. J. Chem. Soc., Perkin Trans. 1 1980, 126.
-
(1980)
Chem. Soc., Perkin Trans. 1
, pp. 126
-
-
Hall, R.H.1
Jordaan, A.2
Malherbe, M.J.3
-
36
-
-
1642532512
-
-
(f) Khlebnikov, A. F.; Novikov, M. S.; Kusei, E. Yu.; Kopf, J.; Kostikov, R. R. Russ. J. Org. Chem. 2003, 39, 559.
-
(2003)
Russ. J. Org. Chem
, vol.39
, pp. 559
-
-
Khlebnikov, A.F.1
Novikov, M.S.2
Kusei, E.Y.3
Kopf, J.4
Kostikov, R.R.5
-
37
-
-
34347377595
-
-
(g) Kosinskaya, I. M.; Pinchuk, A. M.; Shevchenko, V. I. J. Gen. Chem. USSR (Engl. Transl.) 1971, 41, 101.
-
(1971)
J. Gen. Chem. USSR (Engl. Transl.)
, vol.41
, pp. 101
-
-
Kosinskaya, I.M.1
Pinchuk, A.M.2
Shevchenko, V.I.3
-
39
-
-
34347400006
-
-
Experimental Details 1H NMR and 13C NMR spectra were obtained on a BRUKER Avance 400. Proton spectra were referenced to TMS; 13C NMR spectra refer to the solvent signal at δ, 77.0 ppm. Spectra in DMSO-d6 were referenced to δ, 2.50 ppm (1H) and 39.7 ppm (13C, respectively. High-resolution mass spectra were measured with a Bruker Daltonik APEX IV FT Ion Cyclotron Resonance mass spectrometer with electrospray ionization. 1-(2-Chloro-5- pyridylmethyl)-2-(2,3,3-trichloro-1-nitroallylidene)imidazolidine (3) To a solution of 7.19 g (38.7 mmol) N-(2-chloro-5-pyridylmethyl)ethane-1,2- diamine in 30 mL MeOH was added a solution of 5.00 g (18.4 mmol) 1,1,2,4,4-pentachloro-3-nitro-1,3-butadiene (1) in 5 mL MeOH at -40°C within 5 min. The resulting mixture was kept at -40°C for 1 h, then 1 h at r.t. The precipitate was sucked off, washed with H2O (3 x 20 mL, MeOH 1 x 10
-
+:...
-
-
-
-
41
-
-
0001700558
-
-
Kagabu, S.; Yokoyama, A. K.; Iwaya, K.; Tanaka, M. Biosci. Biotechnol. Biochem. 1998, 62, 1216.
-
(1998)
Biosci. Biotechnol. Biochem
, vol.62
, pp. 1216
-
-
Kagabu, S.1
Yokoyama, A.K.2
Iwaya, K.3
Tanaka, M.4
|