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Crystal data for 18: C28H22O 4S2, a, 915.15(18, b, 1266.3(3, c, 1315.2(3) pm, α, 108.78(3, β, 106.98(3, γ, 105.74(3)°, V, 1262.7(4) × 106 pm3; triclinic P1, Z, 2, ρcalcd, 1.2803 g cm -1, μ(Mo-Kα, 0.242 mm-1, STOE IPDS2, Mo-Kα radiation, λ, 0.71073 Å, T, 200 K, 2θmax, 52°, 5573 reflections measured, 3988 independent reflections (Rint, 0.0323, 2268 independent reflections with Fo > 4σ(Fo, The structure was solved by direct methods and refined by full-matrix least-square techniques against F2, 307 parameters S, O, C were refined anisotropically, H atoms calculated at ideal positions, R1, 0.0488, wR2
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-3. CCDC-662155 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.
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