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Volumn 46, Issue 46, 2007, Pages 8880-8882

Carbon extrusion/cluster contraction: Synthesis of the fluorinated cyano-closo-undecaborate K2[3-NC-closo-B11F10]

Author keywords

Carboranes; Cluster compounds; Cyanoborates; NMR spectroscopy; Structure elucidation

Indexed keywords

AMINO ACIDS; LIGANDS; NEGATIVE IONS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SYNTHESIS (CHEMICAL);

EID: 36749064386     PISSN: 14337851     EISSN: None     Source Type: Journal    
DOI: 10.1002/anie.200703385     Document Type: Article
Times cited : (27)

References (38)
  • 12
    • 36749053948 scopus 로고    scopus 로고
    • S. H. Strauss, S. V. Ivanov, A. J. Lupinetti, Colorado State University Research Foundation, WO 98/43983, 1998
    • S. H. Strauss, S. V. Ivanov, A. J. Lupinetti, (Colorado State University Research Foundation), WO 98/43983, 1998.
  • 14
  • 17
    • 34548280245 scopus 로고    scopus 로고
    • Angew. Chem. Int. Ed. 2007, 46, 6346.
    • (2007) Chem. Int. Ed , vol.46 , pp. 6346
    • Angew1
  • 20
    • 17644399514 scopus 로고    scopus 로고
    • Angew. Chem. Int. Ed. 2005, 44, 2220.
    • (2005) Chem. Int. Ed , vol.44 , pp. 2220
    • Angew1
  • 26
    • 36749016118 scopus 로고    scopus 로고
    • unpublished results
    • M. Finze, unpublished results.
    • Finze, M.1
  • 32
    • 36749034185 scopus 로고    scopus 로고
    • Crystal structure of K2[NCB11F10, CB11F10K2N, Mr, 413.13, STOE-IPDS, MoKa radiation (λ, 0.71073 Å, temperature 120K. Colorless crystals (0.30×0.15×0.15 mm3, obtained from CH3CN/Et2O/CH2C12, monoclinic, space group C2/c (no. 15, a, 23.935(8, b, 9.903(2, c, 14.367(6) Å, β, 126.17(3)°, V, 2749.1(16) Aring;3, Z, 8, ρcalcd, 1.996 Mgm-3, μ(MoKa, 0.791 mm-1, F(000, 1568, 14557 measured reflections (5.12 < θmax < 25.00°, structure solution by direct methods and structure refinement based on F2 with 2405 independent reflections (1276 independent reflections with I > 2σ(I, 231 variables SHELXS-97
    • -3. CCDC-653913 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.
  • 33
    • 36749093333 scopus 로고    scopus 로고
    • Gaussian03 (Revision D.01): M.J. Frisch et al., see the Supporting Information.
    • Gaussian03 (Revision D.01): M.J. Frisch et al., see the Supporting Information.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.