Synthesis and stability of reactive salts of dodecafluoro-closo-dodecaborate(2-)

Journal of the American Chemical Society

Volumn 125, Issue 16, 2003, Pages 4694-4695

  Ivanov, Sergei V ^a   Miller, Susie M ^a   Anderson, Oren P ^a   Solntsev, Konstantin A ^b   Strauss, Steven H ^a  

^a Department of Environmental and Radiological Health Sciences   (United States)

^b KURNAKOV INSTITUTE OF GENERAL AND INORGANIC CHEMISTRY   (Russian Federation)

Author keywords

[No Author keywords available]

Indexed keywords

BORIC ACID; FLUORINE DERIVATIVE;

ARTICLE; CRYSTAL STRUCTURE; CRYSTALLIZATION; MASS SPECTROMETRY; MOLECULAR STABILITY; OXIDATION; OXIDATION REDUCTION REACTION; REACTION ANALYSIS; SYNTHESIS; THERMOGRAVIMETRY;

EID: 0037462077     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja0296374     Document Type: Article

References (39)

1. Pitochelli, A. R.; Hawthorne, M. F. J. Am. Chem. Soc. 1960, 82, 3228.
2. (a) Muetterties, E. L.; Knoth, W. H. Polyhedral Boranes; M. Dekker: New York, 1969.
3. (b) Hawthorne, M. F. Pure Appl. Chem. 1991, 63, 327.
4. (c) Hawthorne, M. F. Angew. Chem., Int. Ed. Engl. 1993, 32, 950.
5. (d) Hawthorne, M. F. Advances in Boron Chemistry, Special Publication No. 201: Royal Society of Chemistry: London, 1997: pp 261-272.
6. (e) Hawthorne, M. F. Mol. Med. Today 1998, 174-181.
7. (a) Knoth, W. H.; Miller, H. C.; England, D. C.; Parshall, G. W.; Muetterties, E. L. J. Am. Chem. Soc. 1962, 84, 1056.
8. (b) Knoth, W. H.; Miller, H. C.; Sauer, J. C.; Balthis, J. H.; Chia, V. T.; Muetterties, E. L. Inorg. Chem. 1964, 3, 159.
9. (c) Miller, H. C.; Muetterties, E. L. U.S. Patent 3, 551, 120, 1970.
10. (a) Peymann, T.; Knobler, C. B.; Hawthorne, M. F. J. Am. Chem. Soc. 1999, 121, 5601.
11. (b) Peymann, T.; Herzog, A.; Knobler, C. B.; Hawthorne, M. F. Angew. Chem., Int. Ed. 1999, 38, 1061.
12. (c) Peymann, T.; Knobler, C. B.; Hawthorne, M. F. Inorg. Chem. 2000, 39, 1163.
13. (d) Peymann, T.; Knobler, C. B.; Hawthome, M. F. Inorg. Chem. 2001, 40, 1291.
14. (e) Maderna, A.; Knobler, C. B.; Hawthorne, M. F. Angew. Chem., Int. Ed. 2001, 40, 1661.
15. (f) Peymann, T.; Knobler, C. B.; Khan, S. I.; Hawthorne, M. F. Angew. Chem., Int. Ed. 2001, 40, 1664.
16. (g) Thomas, J.; Hawthorne, M. F. Chem. Commun. 2001, 1884.
17. (h) Peymann, T.; Knobler, C. B.; Khan, S. I.; Hawthorne, M. F. J. Am. Chem. Soc. 2001, 123, 2182.
18. (a) Ivanova, S. M.; Ivanov, S. V.; Miller, S. M.; Anderson, O. P.; Solntsev, K. A.; Strauss, S. H. Inorg. Chem. 1999, 38, 3756.
19. (b) McLemore, D. K.; Dixon, D. A.; Strauss, S. H. Inorg. Chim. Acta 1999, 294, 193.
20. (c) Ivanov, S. V.; Rockwell, J. J.; Polyakov, O. G.; Gaudinski, C. M.; Anderson, O. P.; Solntsev, K. A.; Strauss, S. H. J. Am. Chem. Soc. 1998, 120, 4224.
21. (d) Strauss, S. H. In Contemporary Boron Chemistry; Davidson, M., Hughes, A. K., Marder, T. B., Wade, K., Eds.; Royal Society of Chemistry: Cambridge, U.K., 2000; p 44 and references therein.
22. Strauss, S. H. Chem. Rev. 1993, 93, 927.
23. (a) Metz, M. V.; Schwartz, D. J.; Stern, C. L.; Nickias, P. N.; Marks, T. J. Angew. Chem., Int. Ed. 2000, 39, 1312.
24. (b) Zhou, J.; Lancaster, S. J.; Walker, D. A.; Beck, S.; Thorton-Pett, M.; Bochmann, M. J. Am. Chem. Soc. 2001, 123, 223.
25. Solntsev, K. A.; Mebel, A. M.; Votinova, N. A.; Kuznetsov, N. T.; Charkin, O. P. Koord. Khim. 1992, 18, 340.
26. Wiersema, R. J.; Middaugh, R. L. Inorg. Chem, 1969, 8, 2074.
27. Synthetic details are given in the Supporting Information.
28. 2- anions are reported in: Solntsev, K. A.; Ivanov, S. V.; Sakharov, S. G.; Katser, S. B.; Chernyavskii, A. S.; Votinova, N. A.; Klyuchishche, E. A.; Kuznetsov, N. T. Russ. J. Coord. Chem. 1997, 23, 369.
29. Bochmann, M.; Sarsfield, M. J. Organometallics 1998, 17, 5908.
30. w = 0.125; GOF = 0.986.
31. Bondi, A. J. Phys. Chem. 1964, 68, 441.
32. (a) Bleasdale, C.; Clegg, W.; Ellwood, S. B.; Golding, B. T. Acta Crystallogr., Sect. C (Cr. Str. Comm.) 1991, 47, 550.
33. (b) Laube, T. Chem. Rev. 1998, 98, 1277.
34. Ehlert, T. C.; Hsia, M. M. J. Chem. Eng. Data 1972, 17, 18.
35. Ivanov, S. V.; Malinina, E. A.; Solntsev, K. A.; Kuznetsov, N. T. Koord. Khim. 1992, 18, 394.
36. Kongpricha, S.; Schroeder, H. Inorg. Chem. 1969, 8, 2449.
37. King, B. T.; Noll, B. C.; McKinley, A. J.; Michl, J. J. Am. Chem. Soc. 1996, 118, 10902.
38. A review of electrochemistry of polyhedral boron compounds is available: Morris, J. H.; Gysling, H. J.; Reed, D. Chem. Rev. 1985, 85, 51.
39. Peymann, T.; Knobler, C. B.; Hawthorne, M. F. Chem. Commun. 1999, 2039.