메뉴 건너뛰기




Volumn 53, Issue 6, 2006, Pages 1517-1521

(2,2′-Bipyridine)palladiumdichloride derivatives as recyclable catalysts in heck reactions

Author keywords

Fluorous; Heck reaction; Homogeneous; Thermal stability; Vacuum distillation

Indexed keywords


EID: 34548572278     PISSN: 00094536     EISSN: None     Source Type: Journal    
DOI: 10.1002/jccs.200600198     Document Type: Article
Times cited : (19)

References (43)
  • 34
    • 85039230840 scopus 로고    scopus 로고
    • Analytical data of 2a: Yield 98, 1H NMR (500 MHz, d-Me2SO) 9.08 (2H, d, 32JHH, 5.9 Hz, H6, 8.37 (2H, s, H3, 7.74 (2H, d, 3JHH, 5.9 Hz, H5, 4.96 (4H, s, bpy-CH2, 4.42 (4H, t, 3JHF, 14.6 Hz, CF2CH 2, 19F NMR (470.5 MHz, d-Me2SO, 119.8 (2F, CH2CF2, 127.1 (2F, s, CH2CF 2CF2, 80.4 (3F, t, 3JHF, 9.2 Hz, CF3, 13C NMR (113 MHz, d-Me2SO) 71 (bpy-CH2, 65.5 (CH2CF2, 121.0, 124.7, 149.6, 152.1, 156.1 (bpy, 115∼119 (CF2CF2CF3, FT-IR (cm-1, 1623.4, 1559.5 (νbpy, m, 1232.4, 1196.6 (νCF2, vs, HR-MS FAB, M-Cl, C20N 2H
    • 37Cl calcd m/z 1186.9428, found m/z 1186.9421.
  • 40
    • 85039225253 scopus 로고    scopus 로고
    • 3, Z = 2, No of refln. = 4623 [R(int) = 0.0631], GoF = 0.610, R = 0.0365 [I > 2σ(I)], Rw = 0.0465.
    • 3, Z = 2, No of refln. = 4623 [R(int) = 0.0631], GoF = 0.610, R = 0.0365 [I > 2σ(I)], Rw = 0.0465.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.