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The formation of the bisaldol byproduct was increased. 1st run, 7%; 2nd run, 10%; 3rd run, 16%; 4th run, 16%; 5th run, 20%; 6th run, 18%.
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No reaction or slow reactions were normally observed under heterogeneous conditions in less polar organic solvents such as ethyl ether, hexane, or toluene. See Supporting Information for details.
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