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For a detailed description of the isolation, purification, and yield and purity determination of PEG-supported compounds, see the Experimental Section of ref 6b or the Supplementary Information.
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The catalyst employed in reaction 10 when recovered by precipitation and filtration contained undetermined amounts of NaOH and was used as such in reactions 12-14 (see Supplementary Information). These were carried out on the same scale as reaction 10.
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