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Journal of Chemical Research

Volumn , Issue 4, 2007, Pages 195-199

A new way to quinazolines, perimidines and dibenzo[d,f][1,3]diazepines

(4) Zaleska, Barbara a Karelus, Marcin a Trzewik, Bartosz a Serda, Pawet b

a JAGIELLONIAN UNIVERSITY (Poland)

b Regional Laboratory of Physicochemical Analyses and Structural Research (Poland)

Author keywords

Fused 1,3 diazepines; Perimidines; Quinazolines; Rearrangements

Indexed keywords

EID: 34547313491 PISSN: 03082342 EISSN: None Source Type: Journal
DOI: 10.3184/030823407X203387 Document Type: Article

Times cited : (4)

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- Compound 5a with formula C22H19N 3OS crystallises in the monoclinic system, space group P2 1/a, with unit cell parameters a, 794.48(3, b, 1439.97(5, c, 1639.56(5) pm, β= 93.217(2)°, V, 1872.8(1) 106 pm3, Z, 4. A total of 2774 independent reflections (R(int, 0.098) were collected on a sample of size 0.35 × 0.20× 0.15 mm using Kappa CCD diffractometer and MoKa radiation. The structure was solved by direct methods with SHELXS9713 and refined by the full-matrix least-squares method on F2 using SHELXL9714 program.Final discrepancy indices for 1884 reflections with I>2σ(I) were equal Rl, 0.055, wR2, 0.105 and R1, 0.094, wR2, 0.123 for ail 2774 data. The final difference Fourier map of electron density was featureless with the largest peak and hole of 0.27 and -0.23-10-6 e-pnv-3, respectively. All calcul
- 15 The structural data were deposited at the Cambridge Crystallographic Data Centre. These data can be obtained free of charge via www.ccdc.cam.ac.uk/conts/retrieving. html (or from the CCDC, 12 Union Road, Cambridge CB2 IEZ, UK; fax: + 44 1223 336033; E-mail: deposit@ccdc.cam.ac.uk) under reference number CCDC 623593.

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* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.