SCOPUS 정보 검색 플랫폼

Volumn 2, Issue 8, 2005, Pages 712-717

Solvothermal in situ ligand synthesis, crystal structure and fluorescent properties of a new heterocyclic compound 1, 1′-bis{3-(pyridin-2-yl)H-imidazo[1,5-α]pyridine}

(4) Liu, Cai Ming a Gao, Hong Yun a Zhang, De Qing a Zhu, Dao Ben a

a PEKING UNIVERSITY (China)

Author keywords

Crystal structure; Fluorescent property; Heterocyclic compound; Imidazo 1, 5 a pyridine compound; Iron(II) complex; Solvothermal synthesis

Indexed keywords

EID: 33947385349 PISSN: 15701786 EISSN: None Source Type: Journal
DOI: 10.2174/157017805774717427 Document Type: Review

Times cited : (12)

References (44)

1
- 0036300232
- For examples: a
- For examples: (a) Walton, R. I. Chem. Soc. Rev. 2002, 31, 230;
- (2002) Chem. Soc. Rev , vol.31 , pp. 230
- Walton, R.I.¹

2
- 0344822645
- (b) Cheetham, A. K.; Ferey, G.; Loiseau, T. Angew. Chem. Int. Ed. 1999,38, 3268;
- (1999) Angew. Chem. Int. Ed , vol.38 , pp. 3268
- Cheetham, A.K.¹ Ferey, G.² Loiseau, T.³

3
- 0033578735
- (c) Hagrman, P. J.; Hagrman, D.; Zubieta, J. Angew. Chem. Int. Ed. 1999,38, 2638;
- (1999) Angew. Chem. Int. Ed , vol.38 , pp. 2638
- Hagrman, P.J.¹ Hagrman, D.² Zubieta, J.³

4
- 1542665814
- (d) Stähler, R.; Mosel, B.-D.; Eckert, H., Bensch, W. Angew. Chem. Int. Ed. 2002, 41, 4487;
- (2002) Angew. Chem. Int. Ed , vol.41 , pp. 4487
- Stähler, R.¹ Mosel, B.-D.² Eckert, H.³ Bensch, W.⁴

5
- 0037112661
- (e) Paul, G.; Choudbury, A.; Sampathkumaran, E. V.; Rao, C. N. R. Angew. Chem. Int. Ed. 2002,41, 4297;
- (2002) Angew. Chem. Int. Ed , vol.41 , pp. 4297
- Paul, G.¹ Choudbury, A.² Sampathkumaran, E.V.³ Rao, C.N.R.⁴

6
- 0000945827
- (f) Khan, M. I.; Lee, Y.-S.; O'Connor, C. J.; Haushalker, R- C.; Zubieta, J. J. Am. Chem. Soc. 1994, 116, 4525;
- (1994) J. Am. Chem. Soc , vol.116 , pp. 4525
- Khan, M.I.¹ Lee, Y.-S.² O'Connor, C.J.³ Haushalker, R.C.⁴ Zubieta, J.⁵

7
- 0141761597
- (g) Wang, Y.; Yu, I.; Guo, M.; Xu, R. Angew. Chem. Int. Ed. 2003,42, 4089.
- (2003) Angew. Chem. Int. Ed , vol.42 , pp. 4089
- Wang, Y.¹ Yu, I.² Guo, M.³ Xu, R.⁴

8
- 0036073574
- For examples: a
- For examples: (a) Evans, O. R.; Lin, W. Acc. Chem. Res. 2002, 35, 511;
- (2002) Acc. Chem. Res , vol.35 , pp. 511
- Evans, O.R.¹ Lin, W.²

9
- 0042318534
- (b) Chae, H. K.; Kim, J.; Friedrichs, O. D.; O'Keeffe, M.; Yaghi, O. Angew. Chem. Int. Ed. 2003,42, 3907;
- (2003) Angew. Chem. Int. Ed , vol.42 , pp. 3907
- Chae, H.K.¹ Kim, J.² Friedrichs, O.D.³ O'Keeffe, M.⁴ Yaghi, O.⁵

10
- 0035906616
- (c) Gutschke, S. O. H.; Price, D. J.; Powell, A. K.; Wood, P. T. Angew. Chem. Int. Ed. 2001,40, 1920;
- (2001) Angew. Chem. Int. Ed , vol.40 , pp. 1920
- Gutschke, S.O.H.¹ Price, D.J.² Powell, A.K.³ Wood, P.T.⁴

11
- 1642269221
- (d) Su, C.-Y.; Goforth, A. M.; Smith, M. D.; Pellechia, P. J.; zur Loye, H.-C. J. Am. Chem. Soc. 2004, 126, 3576;
- (2004) J. Am. Chem. Soc , vol.126 , pp. 3576
- Su, C.-Y.¹ Goforth, A.M.² Smith, M.D.³ Pellechia, P.J.⁴ zur Loye, H.-C.⁵

12
- 0034608964
- (e) Lo, S. M.-F.; Chui, S. S.-Y.; Shek, L.-Y.; Lin, Z.; Zhang, X. X.; Wen, G.-H.; Williams, I. D. J. Am. Chem. Soc. 2000, 122, 6293;
- (2000) J. Am. Chem. Soc , vol.122 , pp. 6293
- Lo, S.M.-F.¹ Chui, S.S.-Y.² Shek, L.-Y.³ Lin, Z.⁴ Zhang, X.X.⁵ Wen, G.-H.⁶ Williams, I.D.⁷

13
- 0034665209
- (f) Liang, Y.; Cao, R.; Su, W.; Hong, M.; Zhang, W. Angew. Chem. Int. Ed. 2000,39, 3304;
- (2000) Angew. Chem. Int. Ed , vol.39 , pp. 3304
- Liang, Y.¹ Cao, R.² Su, W.³ Hong, M.⁴ Zhang, W.⁵

14
- 4644275297
- (g) Liu, C.-M.; Gao, S.; Zhang, D.-Q.; Huang, Y.-H.; Xiong, R.-G.; Liu, Z.-L.; Jiang, F.-C.; Zhu, D.-B. Angew. Chem. Int. Ed. 2004, 43, 990;
- (2004) Angew. Chem. Int. Ed , vol.43 , pp. 990
- Liu, C.-M.¹ Gao, S.² Zhang, D.-Q.³ Huang, Y.-H.⁴ Xiong, R.-G.⁵ Liu, Z.-L.⁶ Jiang, F.-C.⁷ Zhu, D.-B.⁸

15
- 0142214720
- (h) Liu, C.-M.; Zhang, D.-Q.; Luo, J.-L.; Wang, N.-L.; Hu, H.-M.; Zhu, D.-B. Eur. J. Inorg. Chem. 2003, 3618.
- (2003) Eur. J. Inorg. Chem , pp. 3618
- Liu, C.-M.¹ Zhang, D.-Q.² Luo, J.-L.³ Wang, N.-L.⁴ Hu, H.-M.⁵ Zhu, D.-B.⁶

16
- 0347899421
- (a) Zhang, J.-P.; Zheng, S.-L.; Huang, X.-C.; Chen, X.-M. Angew. Chem. Int. Ed. 2004,43, 206;
- (2004) Angew. Chem. Int. Ed , vol.43 , pp. 206
- Zhang, J.-P.¹ Zheng, S.-L.² Huang, X.-C.³ Chen, X.-M.⁴

17
- 16344388975
- and references therein
- (b) Zhang, X-M. Coord. Chem. Rev. 2005,249, 1201 and references therein.
- (2005) Coord. Chem. Rev , vol.249 , pp. 1201
- Zhang, X.-M.¹

18
- 0037151659
- For examples: a
- For examples: (a) Zheng, N.; Bu, X.; Feng, P. J. Am. Chem. Soc. 2002,124, 9688;
- (2002) J. Am. Chem. Soc , vol.124 , pp. 9688
- Zheng, N.¹ Bu, X.² Feng, P.³

19
- 0037131437
- (b) Xiong, R.-G.; Xue, X.; Zhao, H.; You, X.-Z.; Abrahams, B. F.; Xue, Z.-L. Angew. Chem. Int. Ed. 2002, 41, 3800;
- (2002) Angew. Chem. Int. Ed , vol.41 , pp. 3800
- Xiong, R.-G.¹ Xue, X.² Zhao, H.³ You, X.-Z.⁴ Abrahams, B.F.⁵ Xue, Z.-L.⁶

20
- 0037087715
- (c) Zhang, X.-M.; Tong, M.-L.; Chen, X.-M. Angew. Chem. Int. Ed. 2002,41, 1029;
- (2002) Angew. Chem. Int. Ed , vol.41 , pp. 1029
- Zhang, X.-M.¹ Tong, M.-L.² Chen, X.-M.³

21
- 0036083587
- (d) Tao, J.; Zhang, Y.; Tong, M.-L.; Chen, X.-M., Yuen, T.; Lin, C. L.; Huang, X.-Y.; Li, J. Chem. Commun. 2002, 1342;
- (2002) Chem. Commun , pp. 1342
- Tao, J.¹ Zhang, Y.² Tong, M.-L.³ Chen, X.-M.⁴ Yuen, T.⁵ Lin, C.L.⁶ Huang, X.-Y.⁷ Li, J.⁸

22
- 0035925836
- (e) Xiong, R.-G.; Zhang, J.; Chen, Z.-F.; You, X.-Z.; Che, C.-M.; Fun, H.-K. J. Chem. Soc., Dalton Trans. 2001, 780;
- (2001) J. Chem. Soc., Dalton Trans , pp. 780
- Xiong, R.-G.¹ Zhang, J.² Chen, Z.-F.³ You, X.-Z.⁴ Che, C.-M.⁵ Fun, H.-K.⁶

23
- 3042544380
- (f) Cheng, J.-K.; Yao, Y.-G.; Zhang, J.; Li, Z.-J.; Cai, Z.-W.; Zhang, X.-Y.; Chen, Z.-N.; Chen, Y.-B.; Kang, Y.; Qin, Y.-Y.; Wen, Y.-H. J. Am. Chem. Soc. 2004, 126, 7796;
- (2004) J. Am. Chem. Soc , vol.126 , pp. 7796
- Cheng, J.-K.¹ Yao, Y.-G.² Zhang, J.³ Li, Z.-J.⁴ Cai, Z.-W.⁵ Zhang, X.-Y.⁶ Chen, Z.-N.⁷ Chen, Y.-B.⁸ Kang, Y.⁹ Qin, Y.-Y.¹⁰ Wen, Y.-H.¹¹

24
- 0035823307
- (g) Liu, C.-M.; Gao, S.; Kou, H.-Z. Chem. Commun. 2001, 1670;
- (2001) Chem. Commun , pp. 1670
- Liu, C.-M.¹ Gao, S.² Kou, H.-Z.³

25
- 1242276296
- (h) Xiao, D.; Hou, Y.; Wang, E.; Lü, J.; Li, Y.; Xu, L.; Hu, C. Inorg. Chem. Commun. 2004, 7, 437;
- (2004) Inorg. Chem. Commun , vol.7 , pp. 437
- Xiao, D.¹ Hou, Y.² Wang, E.³ Lü, J.⁴ Li, Y.⁵ Xu, L.⁶ Hu, C.⁷

26
- 0007065057
- (i) Evans, O. R.; Lin, W. Cryst. Growth & Des. 2001, 1, 9;
- (2001) Cryst. Growth & Des , vol.1 , pp. 9
- Evans, O.R.¹ Lin, W.²

27
- 0346677844
- Lin, W, Evans, O. R, Cui, Y. Cryst. Growth & Des. 2002, 2, 409, Preparation A mixture of bpa (1.0 mmol, Fe(C104)2. 6H2O (1.0 mmol, NaN3 (2.0 mmol, H2O (0.5 cm3) and methanol (4.0 CM3, stirred for 20 min, was then transferred to a 20-cm3 polytetrafluoroethylene-lined stainless steel Parr bomb and kept at 100 °C for 4 days, 90 mg of yellow needle crystals of 1 (yield 46.3, by bpa) and 80 mg of red needle crystals of 2 (yield 24.5, by bpa) were obtained after, cooling at ambient temperature. 1: Anal. calcd for C24H16 N6, C, 74.21; H, 4.15; N, 21.64; found C, 74.16; H, 4.23; N,21.58. EI+-MS: m/z, 388 (100, M, 1H-NMR (400MHz, CDCI3, δ, 8.80(m, 2H, 8.69(m, 2H, 8.39(m, 2H, 8.00(m, 2H, 7.60(m, 2H, 7.40(m, 2H, 7.26(m, 2H, 7.03(m, 2H, 13 C-NMR 100NHz, CDC
- 3 are potentialy explosive and they should be handled with proper care!

28
- 0001863824
- (a) Renz, M.; Hemmert; C.; Donnadieu, B.; Meunier, B. Chem. Commun. 1998, 1635;
- (1998) Chem. Commun , pp. 1635
- Renz, M.¹ Hemmert, C.² Donnadieu, B.³ Meunier, B.⁴

29
- 0033022336
- (b) Meunier, B.; Hemmert; C.; Renz, M.; Gornitzka H.; Soulet, S. Chem. Eur. J. 1999, 5, 1766;
- (1999) Chem. Eur. J , vol.5 , pp. 1766
- Meunier, B.¹ Hemmert, C.² Renz, M.³ Gornitzka, H.⁴ Soulet, S.⁵

30
- 33749094800
- (c) Hemmert, C.; Renz, M.; Gornitzka, H.; Meunier, B. J. Chem. Soc., Dalton Trans. 1999, 3989;
- (1999) J. Chem. Soc., Dalton Trans , pp. 3989
- Hemmert, C.¹ Renz, M.² Gornitzka, H.³ Meunier, B.⁴

31
- 67650406878
- (d) Winterfeld, K; Franzke, H. Angew. Chem. Int. Ed. 1963, 2, 736;
- (1963) Angew. Chem. Int. Ed , vol.2 , pp. 736
- Winterfeld, K.¹ Franzke, H.²

32
- 37049065968
- (e) Bower, J. D.; Ramage, G. R. J. Chem. Soc. 1955, 2834;
- (1955) J. Chem. Soc , pp. 2834
- Bower, J.D.¹ Ramage, G.R.²

33
- 0018396269
- (f) Edgar, M. T.; Pettit, G. R.; Krupa, T. S. J. Org. Chem. 1979, 44, 396;
- (1979) J. Org. Chem , vol.44 , pp. 396
- Edgar, M.T.¹ Pettit, G.R.² Krupa, T.S.³

34
- 0010111049
- (g) Abushanab, E. Tetrahedron Lett. 1971,18, 1441;
- (1971) Tetrahedron Lett , vol.18 , pp. 1441
- Abushanab, E.¹

35
- 0000400082
- (h) Krapcho, A. P.; Powell, J. R. Tetrahedron Lett. 1986, 27, 3713;
- (1986) Tetrahedron Lett , vol.27 , pp. 3713
- Krapcho, A.P.¹ Powell, J.R.²

36
- 0010156255
- (i) Tachikawa, R.; Tanaka, S.; Terada, A. Heterocycles 1981, 15, 369.
- (1981) Heterocycles , vol.15 , pp. 369
- Tachikawa, R.¹ Tanaka, S.² Terada, A.³

37
- 0345145192
- Goleic, L.; Leban, I., Stanovinik, M.; Tisler, M.; Tomazic, A. Croat. Chem. Acta 1980,53, 435.
- (1980) Croat. Chem. Acta , vol.53 , pp. 435
- Goleic, L.¹ Leban, I.² Stanovinik, M.³ Tisler, M.⁴ Tomazic, A.⁵

38
- 4544274624
- (a) Morgan, G. T.; Burstall, F. H. J. Chem. Soc. 1932, 20;
- (1932) J. Chem. Soc , pp. 20
- Morgan, G.T.¹ Burstall, F.H.²

39
- 37049078606
- (b) Gillard, R. D.; Hall, D. P. J. J. Chem. Soc., Chem. Commun. 1988, 1163,
- (1988) J. Chem. Soc., Chem. Commun , pp. 1163
- Gillard, R.D.¹ Hall, D.P.J.²

40
- 11044221627
- 2 is the main product. Liu, C.-M.; Gao, S.; Zhang, D.-Q.; Liu, Z.-L.; Zhu, D.-B. Inorg. Chim. Acta 2005, 358, 834.
- 2 is the main product. Liu, C.-M.; Gao, S.; Zhang, D.-Q.; Liu, Z.-L.; Zhu, D.-B. Inorg. Chim. Acta 2005, 358, 834.

41
- 46149122212
- Crystal data for 1: C24H16N6: M, 388.42, monoclinic, space group P2/c,α, 12.059(2, b, 5.1639(10, c 15.236(3) Å, β, 100.79(3) V, 909.0(3) Å3, Z, 4, Pcalc, 1.419 g · cm-3, μ(MoKα) 0.089 mm-1,T, 293(2) K, R1 [I > 2σ(I, 0.0445, WR2[I > 2σ(I, 0.1173. 2031 indepencleat reflections, 1265 with > 2σ(1, Crystal data for 2: C48H52 C14Fe2 N12O16: M, 1306.52, triclinic, space group P1,α, 8.895(2, b, 11.836(2, c, 14.509(3)Å, α 83.57(3, β, 72.23(3, γ, 67.99(3) °, V, 1348.6(5) Å 3, Z 1, Pcalc, 1,609 g · cm-3, μMoKα, 0.818 mm
- 2 using SHELXL 97 program. All non-hydrogen atoms were refined anisotropically, all of the hydrogen atoms were introduced at calculated positions as riding on a bonded atom. CCDC-258922 and 258923.

42
- 0000262422
- Butcher, R. J.; Addison, A. W. Inorg. Chim. Acta 1989,158, 211.
- (1989) Inorg. Chim. Acta , vol.158 , pp. 211
- Butcher, R.J.¹ Addison, A.W.²

43
- 33751391663
- Glerup, J.; Goodson, P. A.; Hodgson, D. J.; Michelsen, K.; Nielsen, K. M.; Weihe, H. Inorg. Chem. 1992, 31, 4611.
- (1992) Inorg. Chem , vol.31 , pp. 4611
- Glerup, J.¹ Goodson, P.A.² Hodgson, D.J.³ Michelsen, K.⁴ Nielsen, K.M.⁵ Weihe, H.⁶

44
- 0035804412
- Loren, J. C.; Siegel, J. S. Angew. Chem. Int. Ed. 2001, 40, 754.
- (2001) Angew. Chem. Int. Ed , vol.40 , pp. 754
- Loren, J.C.¹ Siegel, J.S.²

* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.