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Volumn 7, Issue 3, 2004, Pages 437-439

Dehydrogenative coupling of 2,2′-bipyridine: Hydrothermal synthesis and crystal structure of a novel polyoxovanadate decorated with the 2,2′;6′,2″;6″,2‴-quaterpyridine ligand

Author keywords

Crystal structure; Dehydrogenative coupling; Hydrothermal synthesis; Polyoxovanadate

Indexed keywords

2,2' BIPYRIDINE; PYRIDINE DERIVATIVE; VANADIC ACID;

EID: 1242276296     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2004.01.001     Document Type: Article
Times cited : (46)

References (47)
  • 38
    • 33646669409 scopus 로고    scopus 로고
    • note
    • -1) for 1 (Fig. S6 ): 3433(bh), 3076(m), 1600(s), 1574(m), 1489(m), 1464(s), 1444(w), 1313(m), 1253(m), 1193(w), 1160(m), 1014(w), 995(m), 969(s), 912(s), 803(s), 771(w), 734(m), 664(s), 580(m), 524(w), 434(w). The TG curve of compound 1 (Fig. S5 ) exhibits three steps of weight losses, corresponding to the loss of nomadic water molecules, coordinated water molecules, quaterpy groups, respectively. The whole weight loss (63.10%) is in agreement with the calculated value (61.98%).
  • 43
    • 33646647025 scopus 로고    scopus 로고
    • note
    • int=0.0973) , 5837 observed with I>2σI) which were used in all refinements. The final R ( F ) was 0. 0642 for observed data.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.