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-1) for 1 (Fig. S6 ): 3433(bh), 3076(m), 1600(s), 1574(m), 1489(m), 1464(s), 1444(w), 1313(m), 1253(m), 1193(w), 1160(m), 1014(w), 995(m), 969(s), 912(s), 803(s), 771(w), 734(m), 664(s), 580(m), 524(w), 434(w). The TG curve of compound 1 (Fig. S5 ) exhibits three steps of weight losses, corresponding to the loss of nomadic water molecules, coordinated water molecules, quaterpy groups, respectively. The whole weight loss (63.10%) is in agreement with the calculated value (61.98%).
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note
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int=0.0973) , 5837 observed with I>2σI) which were used in all refinements. The final R ( F ) was 0. 0642 for observed data.
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