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In comparison, Paterson's synthesis of 1 involved 27 steps for the longest linear sequence in 3.8% yield (ref 7a). Curran's 34 steps afforded 1% yield (ref 7b), and the 26-step longest sequence by Phillips yielded ∼1% (ref 8).
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13C NMR of our sample (1.5 mg) matched with those reported in the literature (refs 7 and 8).
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13C NMR of our sample (1.5 mg) matched with those reported in the literature (refs 7 and 8).
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41
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