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33749008256
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note
-
Attempts to prepare salts 1 with doubly charged anions by precipitation from an aqueous solution of 1 × 4Br upon addition of excess disodium sulphate, oxalate, terephthalate, isophthalate, or phthalate led to only partial substitution of bromide. The precipitated salts kept up to two bromide anions.
-
-
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49
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33749038670
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note
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About the importance of ion pairing with initial counterions in electrostatic self-assembly, see ref 16.
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52
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33749039514
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note
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2+), respectively.
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53
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33749016820
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note
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4 were practically impossible due to the very easy stoppering of the nano needle.
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54
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0039501785
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Due to a different volatility, charge, protonation ability, stability, etc. of the species, the intensity of the signals in the mass spectra is dependent on many unknowns and, consequently, gives only qualitative information. For details, see: Oshovsky, G. V.; Verboom, W.; Fokkens, R. H.; Reinhoudt, D. N. Chem.-Eur. J. 2004, 10, 2739-2748.
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