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c , the necessary rst step of using correctly TEM and other powerful, atomic-level microscopies. First, the sample needs to be as homogeneous to the eye and to lower power microscopies; the presence of multilayered samples or precipitates, for example bulk metal, virtually assures problems in obtaining representative micrographs in our experience. Next, a group of 10-20 randomly selected TEM micrographs at lower power (for example ≤100 K magnification) needs to be obtained, followed by any needed higher magnification micrographs. Restated, the particle counting software and resultant statistics used herein rely, of course, on one first obtaining truly representative micrographs of the system being examined;
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33745931444
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(b) The problem of obtaining a truly representative set of micrographs is what we like to call the "Avogadro's Number Problem" to remind us how far away, from an Avogadro's number collection of particles, the sample size being examined by TEM actually is.
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